Synthesis and Characterization of Various Amino Acids Complexes ...

More documents

Recommendations

Info

CERTIFICATE "Syntheals and Characte zation of Vadous Anino Aci& Comptgxo€ Using Different Analytical Techniiues" under my su;dance ed supeNision in thc labonlories of National Cenre of Excellence jn Analltical Ch€misFy, Univ€rsity of Sindh, Janshoro-Pakistan. His rcsearch work is original, irnovative and thesis is worrhy ofpreseniation io the University of Sindh for dre award of degree of Dodor of Philosophy in Chemhtry. This is to cenify that, Mi RAJA ADIL SARFRAZ s/o Raja Sr.frrz Akht.r has canied our his Res€arch and Experimental work on the topic (Prot Dr, Tasneem Gul Kirl) SupeIvisor Nation l Cfttc of Exellcne in Anal}lical Chemi$ry. Univ€siry oi Sindh, Jmshoo, Pali$an.
ACKNOWLEDGEMENTS I bow oy held b.foE AlEthq Ahh, The omnipotent thc onnipEs! lhe n.lciful, lh. nosl gtuiols, th€ @np4;or5lq rhe b.nefic.nt, who b tlE dln ..d only sole or d.ry *nowlcdgc dd wisdon sdo$€d to narLnd ud wno bbs*n m. wnh rh. ability 10 do ihis work sd g'nr MuhrDerd (Sellalldro Alaihe Waallm) wno gav. u th. spim ro 18. h is lnc blsing ol Alnigbry AId od Eir Pmp!.r (Sdhll.ho Alaib. Wasallmr fiar have enrbld me @ malc my eifotu d:uas. I rculd liLe to lllc this opportunfy to @v.y my @rdial gdnud. ud app@idjon b ny vodr, eleend, dd Ealol supeFief Pret Dr Tcrtren Cul Ksi, wnhoul vh@ @n51ol help, dF, inLGt .nd vi8ilDa sull$e, rhe @ntleton of tiis d6is would nor h.vc ben possible. I sm euy ind.bt d to ho fo hd .@omod.rivc atiirudc, lhoughl povoldns guida.ce, inh.r int lletl.l input, p.1i.M, symp.lh.tic bdt.vior dd adninhtrative dedure in Foviding m. all rhc f.ciliries r.qlircd 1o complere $b piece of I m !.ally indebt d to Prof. Di MuhuEad Iqbd 8n.r8.., Dn€ctor National Cote of Exellae in AMlydc.l Ch.oist y, Univdity of Sin
Page 1 and 2: Synthesis and Characterization of V
Page 6 and 7: I d litcdlly ideh.d !o Di Nr.iD. M@
Page 8 and 9: Anino ai.ls @ t!. diftt uilof.v.ry
Page 10 and 11: o tl "4o N r.rn.dEtu P!qo..d nldEdd
Page 12 and 13: Tirlc t2 1,3 1.t 1,7 LE 1,9 Amino r
Page 14 and 15: 43 4.1 A.hoAdtL 5.4 R.$lrr rd DiMio
Page 17 and 18: L 4. 5 6. List of Original Publicat
Page 19 and 20: l€*orhcna aromic 'bsQlloi speftn
Page 21 and 22: Chapten* t
Page 23 and 24: Ch.rit rdor of^biro Adb MoloDiro Do
Page 25 and 26: i! eit seg6's 6gdn 0-tll|@2, 4-dini
Page 27 and 28: 2-Mclhyl-8-ttydroxyquirolir. ole c.
Page 29 and 30: \z\.\z* San
Page 31 and 32: cgins ro fibcdd a ! cltdyrl. Th s.
Page 33 and 34: oE@D. [41], Ihis prcvidq dr sole of
Page 35 and 36: streng inluae of 3ulfusntlining him
Page 37 and 38: eith ltsrin. dd th. .rt llzing crpl
Page 39 and 40: 13, F- P, Dwya dd D. !. Mill6 "Cldd
Page 41 and 42: 37. Z, Guo ed P, J, Sadld,,{ n84. C
Page 43 and 44: 6a F. Wq, , D.{r ,. rL Eid d F. I $
Page 45 and 46: Anlno Acids Det rmi!.uoD Literatu?e
Page 47 and 48: ihis cnt@c.d efrer of dlllysit vaio
Page 49 and 50: ne ndhod @ b. us.d for $e Egid deim
Page 51 and 52: sm. mino sid5 glycine *dinq vdin. d
Page 53 and 54:
Cbol*teroLAriro Ad& Compldg Litdtur
Page 55 and 56:
nly beon. a Esrdini.g f&!or fo. nen
Page 57 and 58:
Anino eids dons virh tn ir d.dvadvs
Page 59 and 60:
16. T. Tdleuhi md T. Mira. Ktunatos
Page 61 and 62:
45. S. A.l3irc, s. K. N!6, C- is Mi
Page 63 and 64:
dt R. Ioro.i S. Hdildi, "nn-ro,nr,r
Page 65 and 66:
Cfi.apter- 3 ADino Acids Compleres
Page 67 and 68:
Fluomm.tdc Study Results aod Dbcuss
Page 69 and 70:
tl3 t (a! ttE {6r dqdr..ald..' Er*-
Page 71 and 72:
T l. l. (b) h4tior LiEits or C}3l.l
Page 73 and 74:
E. c-o f: eQ h. eo eQ rtln 3 (.)! F
Page 75 and 76:
Tt @DFrali* ladt of nur6c. in Gny o
Page 77 and 78:
7 r.95 1.35 r.3 l.?t : !.25 3.5 3.1
Page 79 and 80:
FE E (bl cdlFrlt € lody of alst3&
Page 81 and 82:
TGA / DTA Sludie. A4rnic Acid-2-Mdh
Page 83 and 84:
E.; A I d i! 533t Po I ;r E -=; 60
Page 85 and 86:
q s sa!, {,32 5. I rs8 EI Fi!P -9 l
Page 87 and 88:
t I : Eer er *; -9 r ,P1 9?! xi3 rl
Page 89 and 90:
Tlbl. q Infred rpst al b6nd $ignn n
Page 91 and 92:
.th 10, hnlr.d s!€t"lb€d Nignn.
Page 93 and 94:
.bk1l. tntdcd sp@t6t bard Nirnncn$
Page 95 and 96:
Trbl. lt" hfnrcd spd..l tqd \sigMor
Page 97 and 98:
Trbl. 13. Nucl6 n.grElic EsMe sp.!t
Page 99 and 100:
8,21,8.0, 7-?8, t.?5 ed 7,O ppm wi$
Page 101 and 102:
thc ovedl e4mdiElio. p.um of th. ed
Page 103 and 104:
2-Mclhyl+hydroxyquidolir. -.3p.!tic
Page 105 and 106:
2.Mcahyt+tydmryqlirolir. -cF!.lnc C
Page 107 and 108:
15- O.B.trin, lbrlrd. rEL3126t0994)
Page 109 and 110:
Amitro Acids Derivrtives of Cholcst
Page 111 and 112:
Geftnl Synatealc Proedure for AmiDo
Page 113 and 114:
Syrrtgh olcbol€t rJl r.lb@!i!.i.
Page 115 and 116:
Aolm AcXr D.dvrtiv.. ofchol.st rol
Page 117 and 118:
Clol.ddyl sgi.id. B ob66ed b h.E 75
Page 119 and 120:
Thern'rl Amblis IIGA / DTA studi€
Page 121 and 122:
Ttbl. 3. TGA / DTA studid ofcnobsro
Page 123 and 124:
T.t te 5. TGA / DTA StldiB of Chol.
Page 125 and 126:
Mrss 3F.trcnclric ttudy ofrmino rci
Page 127 and 128:
F g. 7. Mss sp.doneoic atudica of c
Page 129 and 130:
Cl.ldr.oHcqi@ d.riutiE(Ch.L.ic!yl L
Page 131 and 132:
4fi=26o4 426-06% Pr.Doied mE!& of c
Page 133 and 134:
. I l. Ms +€.tonet b sdi6 of ctoL
Page 135 and 136:
Chapter - 5
Page 137 and 138:
Introducrion Rn. Pd, Pt, Ru od simi
Page 139 and 140:
Preprrrllotr ofthe OS(ID conplerei
Page 141 and 142:
Fin d wirh Esed loitl ion-hydro€e
Page 143 and 144:
Fig 1. ThG mleule strlcte of , with
Page 145 and 146:
$c X-ny dift& on dslysis of . singl
Page 147 and 148:
Ncvenhelds, b€cous of th€.ndtid
Page 149 and 150:
i .dat d in 3!ch ! wy, tn@urn (u ir
Page 151 and 152:
Ci.b6d€tiv. Eydnsd-Tlrllf.r R.d!.
Page 153 and 154:
fa*i dngly. ctrloFrrimnc, ac{uiFd b
Page 155 and 156:
(e) M.A. Eidel!!" M.P. Gai4 A.M. Lt
Page 157 and 158:
_synmdy_ell_slnin! f icliric s)m.ry
Page 159 and 160:
R.6l1@d of Fr^ alajd ALL ERdiG. TtF
Page 161 and 162:
Os0,02451(6)0.03135(7)0.02422{6)0.0
Page 163 and 164:
cl4 os cro 67,80(7) , , ? cll O!clo
Page 165 and 166:
Cry.trlhSr.phichfonmtiotr F .s(CIF3
Page 167 and 168:
_difirn EfB rv_R_.ldvilsa 0 0375 _d
Page 169 and 170:
Hr H 0.5472 0.m02 0.990. 0.169 ue r
Page 171 and 172:
c r3 0. r00l9r 0 03E9r 0 o92{t rJ 0
Page 173 and 174:
le_&3h_#.r@y-t _lr.m-dd.-ft_rrfrey
Page 175 and 176:
l@_Eid_e,tE_lrbd_l ldn_6io_@-3ic-Lh
Page 177 and 178:
Conclusion PEDadion dd @npl.le €h
Page 179 and 180:
Re5earah Artide Synthesis, structur
Page 181 and 182:
H lrhm!]lJlor^ft!@pbn@'Ls ; *dr*.a.
Page 183 and 184:
him Fdsdtrlc of onnrfi0 19 ffi ffi#
Page 185 and 186:
Sy'nthesis and X-Ray Structural Stu
Page 187 and 188:
cryidr o rryk r tur tulP. M Issn m$
Page 189 and 190:
ffi ETSEVIER Av.]|'bbonh.n0w'sh€d
Page 191 and 192:
ELSEVIER Etratugtion of statur of t
Page 193 and 194:
vs&nE^ii@Hd4drHd!, iLrt Evrluation
Page 195 and 196:
ELSE\'IER Determinadon of cadmlum l
Page 197 and 198:
il EISEVIER 1;' ftienceDirect A mul
Page 199 and 200:
: Edu.tim or ltuu b s.run od:f,ln;l
show all

Synthesis and Characterization of Various Amino Acids Complexes ...

Create successful ePaper yourself

Delete template?

Save as template?