Synthesis and Characterization of Various Amino Acids Complexes ...

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ADim ..lL @rt irhS u idlo grelp Hydrut!relirc md Ptuli@. Tlc mino &id! qhich csot be st h.siad by rhc body @ ar.gorized a.sn.l di.o.cids $iich ircludc n rhidiE, phdy'ddie, thMiilc, ltuiE, iel.ucinc, l$iie, fyltophd, rdii., s4 i! @ly infdcy, nididin . How.v.r, &n of th. diio &idr re clrsificd a ndeti.l, od d b. syn$6isd d&lgrdsly by th. body s Fr Anim &i
i! eit seg6's 6gdn 0-tll|@2, 4-dinito bqE .) lal. 'Irtc @sor urdeac @nd€nslior Eelio Nilh tu€ Mino greup3 in @ld dd nildly .lkdin. $ludon, Ar th. @jdiry of di@ &ids do na Sow 6ogh (ry lb$Drim .l drc Nd Mv€ldgths (250 to 280 m} . di@t ealysis s4i not p6sibl.. Anothd pomisi.g tpFqh b ddiwrizr1iu of rh. oirc &id\ pbviding luit Uc rMing @npound, beloF e.ltsk, nt. liiedtu@ Gviff sho*Ed Ihat, a Nnba of&rirEtizi.g qgaB l@ cmptoyed fd tbe d.r.minari6 ofdino *idr itr biologic.l tluids. A fluooneFi. hetlod for d.tdniratio! of oho 4ids i. biologiol tluids w d.velop.d iI ou l.bo..toy, Faisly l5l. Daiw$atid % pafom.d with oxim in @idic ndi. after h.rtilg foi l0 ninutes ar ! ortrolled r.npRtr. (60oC} Ilc p.l. yellN l{lduds obt itEd, s@ na&d in difft.6r sp6t!6copic Fgios !r. *arc lagrhs dgq 100 to 380m fo. qci6ti6 $'hil.dission int nsiti.s wft obswd !r 410 !o 480,n for dififfit &rivs'tiv6 of @ino eid5. It. pEpa.d €SGnl wd ! nd dc ed ws not E on d in li.f.nd Aiolhs *uk E oncd by ou crelp 16l, w Fhr.! wirh Mi.o.cids dcdvariv6 of niiltddi, e ihpovddts ii thc Fs.dw w3 mad. i! arldition ro mct l ioN $ch B zin , coDDd, cadnih, strDitium clc in rh. hi.o eid $lurio, Th.s. nerli ions fom . mnplq, *lich givc ! b3rhahMi. shift &d \e Elrriv.ly m@ 5r.bl.. Anino rclds as Llgrd! Thc lese sl. lppl'€liolr ofligeds rLrieed fron di.o rcids is a Dopuld subjet i. orSdoncr.llic .hcmisty 11. A rmbs of iqq n.r.l ios, srch s Cu':, Co", Mn*., Fc'1, etc. @npl*6 eirh mino sids i! ettich boib @tboxyl 6d olhd lroups, sh 6 -NH1 b.l Jl|. e involvd, nsv. b.d rcponed Ior .bple:
Page 1 and 2: Synthesis and Characterization of V
Page 4 and 5: CERTIFICATE "Syntheals and Characte
Page 6 and 7: I d litcdlly ideh.d !o Di Nr.iD. M@
Page 8 and 9: Anino ai.ls @ t!. diftt uilof.v.ry
Page 10 and 11: o tl "4o N r.rn.dEtu P!qo..d nldEdd
Page 12 and 13: Tirlc t2 1,3 1.t 1,7 LE 1,9 Amino r
Page 14 and 15: 43 4.1 A.hoAdtL 5.4 R.$lrr rd DiMio
Page 17 and 18: L 4. 5 6. List of Original Publicat
Page 19 and 20: l€*orhcna aromic 'bsQlloi speftn
Page 21 and 22: Chapten* t
Page 23: Ch.rit rdor of^biro Adb MoloDiro Do
Page 27 and 28: 2-Mclhyl-8-ttydroxyquirolir. ole c.
Page 29 and 30: \z\.\z* San
Page 31 and 32: cgins ro fibcdd a ! cltdyrl. Th s.
Page 33 and 34: oE@D. [41], Ihis prcvidq dr sole of
Page 35 and 36: streng inluae of 3ulfusntlining him
Page 37 and 38: eith ltsrin. dd th. .rt llzing crpl
Page 39 and 40: 13, F- P, Dwya dd D. !. Mill6 "Cldd
Page 41 and 42: 37. Z, Guo ed P, J, Sadld,,{ n84. C
Page 43 and 44: 6a F. Wq, , D.{r ,. rL Eid d F. I $
Page 45 and 46: Anlno Acids Det rmi!.uoD Literatu?e
Page 47 and 48: ihis cnt@c.d efrer of dlllysit vaio
Page 49 and 50: ne ndhod @ b. us.d for $e Egid deim
Page 51 and 52: sm. mino sid5 glycine *dinq vdin. d
Page 53 and 54: Cbol*teroLAriro Ad& Compldg Litdtur
Page 55 and 56: nly beon. a Esrdini.g f&!or fo. nen
Page 57 and 58: Anino eids dons virh tn ir d.dvadvs
Page 59 and 60: 16. T. Tdleuhi md T. Mira. Ktunatos
Page 61 and 62: 45. S. A.l3irc, s. K. N!6, C- is Mi
Page 63 and 64: dt R. Ioro.i S. Hdildi, "nn-ro,nr,r
Page 65 and 66: Cfi.apter- 3 ADino Acids Compleres
Page 67 and 68: Fluomm.tdc Study Results aod Dbcuss
Page 69 and 70: tl3 t (a! ttE {6r dqdr..ald..' Er*-
Page 71 and 72: T l. l. (b) h4tior LiEits or C}3l.l
Page 73 and 74: E. c-o f: eQ h. eo eQ rtln 3 (.)! F
Page 75 and 76:
Tt @DFrali* ladt of nur6c. in Gny o
Page 77 and 78:
7 r.95 1.35 r.3 l.?t : !.25 3.5 3.1
Page 79 and 80:
FE E (bl cdlFrlt € lody of alst3&
Page 81 and 82:
TGA / DTA Sludie. A4rnic Acid-2-Mdh
Page 83 and 84:
E.; A I d i! 533t Po I ;r E -=; 60
Page 85 and 86:
q s sa!, {,32 5. I rs8 EI Fi!P -9 l
Page 87 and 88:
t I : Eer er *; -9 r ,P1 9?! xi3 rl
Page 89 and 90:
Tlbl. q Infred rpst al b6nd $ignn n
Page 91 and 92:
.th 10, hnlr.d s!€t"lb€d Nignn.
Page 93 and 94:
.bk1l. tntdcd sp@t6t bard Nirnncn$
Page 95 and 96:
Trbl. lt" hfnrcd spd..l tqd \sigMor
Page 97 and 98:
Trbl. 13. Nucl6 n.grElic EsMe sp.!t
Page 99 and 100:
8,21,8.0, 7-?8, t.?5 ed 7,O ppm wi$
Page 101 and 102:
thc ovedl e4mdiElio. p.um of th. ed
Page 103 and 104:
2-Mclhyl+hydroxyquidolir. -.3p.!tic
Page 105 and 106:
2.Mcahyt+tydmryqlirolir. -cF!.lnc C
Page 107 and 108:
15- O.B.trin, lbrlrd. rEL3126t0994)
Page 109 and 110:
Amitro Acids Derivrtives of Cholcst
Page 111 and 112:
Geftnl Synatealc Proedure for AmiDo
Page 113 and 114:
Syrrtgh olcbol€t rJl r.lb@!i!.i.
Page 115 and 116:
Aolm AcXr D.dvrtiv.. ofchol.st rol
Page 117 and 118:
Clol.ddyl sgi.id. B ob66ed b h.E 75
Page 119 and 120:
Thern'rl Amblis IIGA / DTA studi€
Page 121 and 122:
Ttbl. 3. TGA / DTA studid ofcnobsro
Page 123 and 124:
T.t te 5. TGA / DTA StldiB of Chol.
Page 125 and 126:
Mrss 3F.trcnclric ttudy ofrmino rci
Page 127 and 128:
F g. 7. Mss sp.doneoic atudica of c
Page 129 and 130:
Cl.ldr.oHcqi@ d.riutiE(Ch.L.ic!yl L
Page 131 and 132:
4fi=26o4 426-06% Pr.Doied mE!& of c
Page 133 and 134:
. I l. Ms +€.tonet b sdi6 of ctoL
Page 135 and 136:
Chapter - 5
Page 137 and 138:
Introducrion Rn. Pd, Pt, Ru od simi
Page 139 and 140:
Preprrrllotr ofthe OS(ID conplerei
Page 141 and 142:
Fin d wirh Esed loitl ion-hydro€e
Page 143 and 144:
Fig 1. ThG mleule strlcte of , with
Page 145 and 146:
$c X-ny dift& on dslysis of . singl
Page 147 and 148:
Ncvenhelds, b€cous of th€.ndtid
Page 149 and 150:
i .dat d in 3!ch ! wy, tn@urn (u ir
Page 151 and 152:
Ci.b6d€tiv. Eydnsd-Tlrllf.r R.d!.
Page 153 and 154:
fa*i dngly. ctrloFrrimnc, ac{uiFd b
Page 155 and 156:
(e) M.A. Eidel!!" M.P. Gai4 A.M. Lt
Page 157 and 158:
_synmdy_ell_slnin! f icliric s)m.ry
Page 159 and 160:
R.6l1@d of Fr^ alajd ALL ERdiG. TtF
Page 161 and 162:
Os0,02451(6)0.03135(7)0.02422{6)0.0
Page 163 and 164:
cl4 os cro 67,80(7) , , ? cll O!clo
Page 165 and 166:
Cry.trlhSr.phichfonmtiotr F .s(CIF3
Page 167 and 168:
_difirn EfB rv_R_.ldvilsa 0 0375 _d
Page 169 and 170:
Hr H 0.5472 0.m02 0.990. 0.169 ue r
Page 171 and 172:
c r3 0. r00l9r 0 03E9r 0 o92{t rJ 0
Page 173 and 174:
le_&3h_#.r@y-t _lr.m-dd.-ft_rrfrey
Page 175 and 176:
l@_Eid_e,tE_lrbd_l ldn_6io_@-3ic-Lh
Page 177 and 178:
Conclusion PEDadion dd @npl.le €h
Page 179 and 180:
Re5earah Artide Synthesis, structur
Page 181 and 182:
H lrhm!]lJlor^ft!@pbn@'Ls ; *dr*.a.
Page 183 and 184:
him Fdsdtrlc of onnrfi0 19 ffi ffi#
Page 185 and 186:
Sy'nthesis and X-Ray Structural Stu
Page 187 and 188:
cryidr o rryk r tur tulP. M Issn m$
Page 189 and 190:
ffi ETSEVIER Av.]|'bbonh.n0w'sh€d
Page 191 and 192:
ELSEVIER Etratugtion of statur of t
Page 193 and 194:
vs&nE^ii@Hd4drHd!, iLrt Evrluation
Page 195 and 196:
ELSE\'IER Determinadon of cadmlum l
Page 197 and 198:
il EISEVIER 1;' ftienceDirect A mul
Page 199 and 200:
: Edu.tim or ltuu b s.run od:f,ln;l
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Synthesis and Characterization of Various Amino Acids Complexes ...

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