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Synthesis and Characterization of Various Amino Acids Complexes ...

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m dd .nission 45oin. [tv.loted nethod s suNtutlv lpPlicd ro lne salvsis <strong>of</strong><br />

tl'proPha in a D@led huma eNn.<br />

Dctcdinario <strong>of</strong> tliPhlric 6ino &lb in sdn ws sicd oul bv HILC wilh<br />

fllmn ric da.dor, 6ins @-i@biliz.d dztm Fcror (Nobddhi et al ' l9' 0ll' A<br />

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*M by HPLC, wnh d.tddon bv cinrobil'ed llein' dehvdegd&&uci'e<br />

dehydd8@ by po51 olum r@tion sd nu@m€r€r' TIF *Ptntion s &hidcd bv<br />

n $t ODS @lunn *nh .Mion *i1h ph$ph . bufd (!tl ?0) The svstem 8!vc x'@<br />

6p6e sd detetioh lini$ al I +2M ld.h.<br />

Flrconetu d.tdni..tior <strong>of</strong> tFtlionirc 6 &hid'd bv oxire (Kui '1 al ' 1994)<br />

Il2t. MalFnire M @f,d.ns.d with oxin. uDdq low ldpF$t al 6d in aq@us D'di4<br />

The Ou@$fll peduct ws studied tpdronuoronelri@llv as w'll 6 bv oin'r dd,tical<br />

rehniquas. The d.retion limil <strong>of</strong>mdionin. ws *hi4'd dds !o nnol ld'l<br />

A tludoneuj. studv <strong>of</strong> naPhlhalcnc2,lnicabqvtldchvd' (NDA) s a Fhrial<br />

dedvalizing ssql for $c fluoromeEio d.telid <strong>of</strong> min4 ed nho &ids in $e Drcsene<br />

<strong>of</strong> payclod.rrinw@ wLd (Aninuddin dd Mill6, |994) lrll Exp€'indr'tl condilio6<br />

including pH <strong>of</strong> $e ncdim. l* optjniad fd th' flndid <strong>of</strong> rh' flunsl NDA-<br />

ChonarognPnic da@indion <strong>of</strong> dino &i& w4 Gpon'd b, (Aninuddin dd<br />

Milh, l99a) lr4. A P.Ecd'pne HILC pF.!dE, 6ing a flwlge<br />

lined for th. sinsle sd qldtitaliv€ {tetemi.clio <strong>of</strong>da@ hounB <strong>of</strong> mino rcids in lhc ng/L<br />

6gp, by pEslMh d.riv.tizltion si$ mPhh.loe'2,lnic{bo*ldehvde l was obseNed<br />

in4 nl@s..G {t€r..don <strong>of</strong> thc d.tivlris hls tdv&tsg6 ova rhc Uvn'rdion svffi<br />

26

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