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3.5<br />
3.0<br />
2.5<br />
Wt. % H desorbed<br />
2.0<br />
1.5<br />
1.0<br />
0.5<br />
0.0<br />
-0.5<br />
0 1000 2000 3000 4000 5000 6000 7000<br />
corrected time (s)<br />
Figure 12: Percent hydrogen desorbed for dehydriding of Mg 2 Ni.<br />
Ball milled Mg 2 Ni reacted at lower temperatures and H 2 pressures to react than<br />
previously reported values [23]. The amount of H absorbed, 3.04 %, (Mg 2 NiH 3.23 ) was<br />
lower than the reported value of 3.60 % (Mg 2 NiH 4 ). The uptake reaction was complete in<br />
about 15 minutes.<br />
3.1.2. VTiNi<br />
V, Ti and Ni were alloyed using the Spex8000 Mixer Mill. Since the starting<br />
materials were pure elements, a relatively long milling time, 90 minutes, was used. The<br />
40