Thesis - Oztek_Muzaffer_T_200508_MA

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LIST OF REFERENCES 1. Rosso, M. J. and Golben, P. M., Journal of the Less Common Metals, 1987. 131(1-2): p. 283-292. 2. Hampton, M. D. and Slattery, D. K., Metal Hydrides for Hydrogen Separation, Recovery and Purification, Annual Report for NASA Hydrogen Research at Florida Universities. 2005, University of Central Florida, Florida Solar Energy Center. 3. Kesting, R. E. and Fritzsche, A. K., 1993. Polymeric Gas Separation Membranes, New York: John Wiley and Sons. 4. Schweitzer, P. A., Handbook of Separation Techniques for Chemical Engineers 3 rd ed. 1996, New York: Mc Graw Hill. 5. Liu, B.S. and Au, C. T., Catalysis Letters, 2001. 77(1-3): p. 67-74. 6. Jordal, K., Bredesen, R., Kvamsdal, H.M., and Bolland, O., Energy, 2004. 29: p. 1269-1278. 7. Oyama, S. T., Lee, D., Sugiyama, S., Fukuki, K., and Iwasawa, Y., Journal of Materials Science, 2001. 36: p. 5213-5217. 8. Chiou, J. S. and Paul, D.R., Ind. Eng. Chem. Res., 1988. 27: p. 2161-2164. 9. Shanin, Y. I., Proc. NATO Advanced Research Workshop on Hydrogen Materials Science and Chemistry of Metal Hydrides, 2001: p. 313-320. 10. Maeland, A.J., in Hydrides for Energy Storage, Andersen, A.F., Editor. 1978, Pergamon Press: U.K. p. 19-31. 11. Akiba, E., Current Opinion in Solid State and Materials Science, 1999. 4: p. 267- 272. 12. Fukai, Y., The Metal-Hydrogen System, Basic Bulk Properties. 1993, Heidelberg: Springer-Verlag. 13. Fromm, E., Kinetics of Metal-gas Interactions at Low Temperatures. 1998, Heidelberg: Springer Verlag. 14. Mintz, M. H. and Bloch, J., Progress in Solid State Chemistry, 1985. 16: p. 163- 194. 15. Bloch, J., Brill, M., Ben-Eliahu, By., and Gavra, Z., Journal of Alloys and Compounds, 1998. 267: p. 158-166. 84
16. Van-Vucht, J.H.N., Kuijpers, F.A., and Bruning, H.C.A.M., Philips Research Reports, 1970. 25: p. 133-140. 17. Mohammed, I.S. and Dakka, A., International Journal of Hydrogen Energy, 2000. 25: p. 773-777. 18. Sandrock, G., S. Suda, and Schlapbach, L., Applications, in Hydrogen in Intermetallic Compounds II, Schlapbach, L., Editor. 1992, Springer-Verlag: Heidelberg. p. 197-258. 19. Mitsuishi, N., Sato, S., and Fukada, S., Fusion Engineering and Design, 1995. 28: p. 362-366. 20. Yukawa, H., Yamashita, D., Ito, S., Morinaga, M., and Yamaguchi, S., Journal of Alloys and Compounds, 2003. 356-357: p. 45-49. 21. Percheron-Guegan, A. and Welter, J-M., Preparation of Intermetallics and Hydrides, in Hydrogen in Intermetallic Compounds I, Schlapbach, L., Editor. 1992, Springer-Verlag: Heidelberg. 22. Libowitz, G.G., in Hydrides for Energy Storage, A.F. Andersen, A.J.M., Editor. 1978, Pergamon Press: U.K. 23. Reilly, J.J. and Jr., R.H. Wiswall, Inorganic Chemistry, 1968. 7(11): p. 2254- 2256. 24. Hampton, M.D., Juturu, R., and Lomness, J.K., International Journal of Hydrogen Energy, 1999. 24: p. 981-988. 25. Hampton, M.D. and Lomness, J.K., International Journal of Hydrogen Energy, 1999. 24: p. 175-187. 26. Tsushio, Y. and Akiba, E., Journal of Alloys and Compounds, 1998. 267: p. 246- 251. 27. Tanaka, S., Clewley, J.D., and Flanagan, T.B., Journal of the Less Common Metals, 1997. 56: p. 137-139. 28. Boser, O., Journal of the Less Common Metals, 1976. 46: p. 91-99. 29. Nomura, K. and Akiba, E., Journal of Alloys and Compounds, 1995. 231: p. 513- 517. 30. Lomness, J.K., Hampton, M.D., and Giannuzzi, L.A., International Journal of Hydrogen Energy, 2002. 27: p. 915-920. 85
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RECOVERY OF HYDROGEN AND HELIUM FRO
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ABSTRACT Waste streams of hydrogen
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I dedicate this work to my family m
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I also would like to cheer for my f
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2.2.2.1. Hydriding and Dehydriding
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LIST OF FIGURES Figure 1. Pressure-
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Figure 34. Pressure profiles under
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1. INTRODUCTION The focus of this s
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ecause of the difference in partial
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hydrides by dissolving large amount
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hydrogen storage alloy has a specif
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• Insensitivity to poisoning by i
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hydrogen capacity was not reproduci
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showed the lowest plateau pressure
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grain boundaries increases the tota
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These parameters are generally inte
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Figure 4. CaCu5-type P6/mmm structu
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In this study, the addition of Al t
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2. EXPERIMENTAL 2.1.Chemicals and R
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Figure 5. The high energy Spex 8000
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2.2.1.1. Hydriding and Dehydriding
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approximately 5 atm, and heating th
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determined by the start and end of
Page 47 and 48: 450 400 coating thickness (Å) 350
Page 49 and 50: 3. RESULTS AND DISCUSSIONS 3.1. Hyd
Page 51 and 52: DSC 111 heat flow/mW Exo 300 Figure
Page 53 and 54: The thermogram associated with the
Page 55 and 56: total time was broken into three 30
Page 57 and 58: The VTiNi sample was subjected to d
Page 59 and 60: solid solution of hydrogen rather t
Page 61 and 62: DSC 111 Heat Flow/mW 180 Exo Figure
Page 63 and 64: 100 rpm setting, the milling vial w
Page 65 and 66: BPR, 400 rpm, 5 minutes) did not re
Page 67 and 68: Table 1: Effects of various milling
Page 69 and 70: Due to the fast kinetics observed a
Page 71 and 72: The mole % Al after milling was les
Page 73 and 74: Figure 24: Percent hydrogen capacit
Page 75 and 76: the start of the heating period, wh
Page 77 and 78: However, it was noted that the part
Page 79 and 80: percent hydrogen was decreased. The
Page 81 and 82: 3.2.2.4. AuPd and Pt Coating on LaN
Page 83 and 84: 1.0 0.8 (a) (b) Wt. % H absorbed 0.
Page 85 and 86: After dehydriding by the sample, th
Page 87 and 88: 19 18 P (atm) 17 16 15 14 0.74 %Al
Page 89 and 90: GC output, arbitrary units 0 5 10 1
Page 91 and 92: sample was LaNi 5 . This may indica
Page 93 and 94: 30 min. 15 min. Intensity (arb. uni
Page 95 and 96: After milling the percentages of Al
Page 97: 4. CONCLUSIONS This study has been
Page 101 and 102: 47. Suryanarayana, C., Progress in
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