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March 22, 1988<br />

I . Ciifton W. Davenport<br />

California Department of Health Services<br />

5850 Sheilmound, Suite 100<br />

Emeryville, CA 94608<br />

Dear Mr. Davenport:<br />

Draft Final Report<br />

Bay Area Drum<br />

Expedited Response Action<br />

Canonie Envlronmentai Sewices Corp.<br />

1825 South Grant Sheet<br />

Suite 260<br />

San Matea, California 94402<br />

Mione: 415-573 8012<br />

Enclosed is one copy of <strong>the</strong> Draft Final Report, Bay Area Drum Expedited<br />

Response Action, for your review.<br />

If you have any questions, please contact us at (415) 573-8012.<br />

Very truly yours,<br />

Claude Carlos White, Jr.<br />

Assistant Project Engineer<br />

Richard J. Ereenwood, P.E.<br />

Project Manager<br />

Enc.


LIST OF TABLES<br />

LIST OF FIGURES<br />

LIST OF APPENDICES<br />

1.0 EXECUTIVE SUMMARY<br />

1.1 Introduction<br />

1.2 Site Background<br />

1.3 Implementation<br />

2.0 IMPLEMENTATION<br />

2.1 Mobilization and Site Setup<br />

2.1.1 Mobilization<br />

2.1.2 Site Setup<br />

2.1.3 Daily Records<br />

TABLE OF CONTENTS<br />

2.2 Phase I Demolition and Drum Yard Preparation<br />

2.2.1 Demolition<br />

2.2.2 Additional Excavation and Drum Removal<br />

2.2.3 Utility Protection<br />

2 .2.4 Site Grading and Surface Preparation<br />

2.2.4.1 Soil Excavation<br />

2.2.4.2 Drainage Ditch Excavation<br />

2.2.4.3 Equipment Decontamination<br />

2.2.4.4 Placement of Cover<br />

2.2.4.5 Orphan Drums<br />

2.2.4.6 Preparation of Roll-Off Boxes<br />

PAGE<br />

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TABLE OF CONTENTS<br />

(Cont i nued)<br />

2.3 Removal of Liquids and Sludges<br />

2.3.1 Sludge Tank<br />

2.3.2 Boiler Tank<br />

2.3.3 Sump and Dip Tanks<br />

2.3.4 Worker Protection<br />

2.4 Phase I1 Demo1 ition and Residential Yard Preparation<br />

2.4.1 Demolition<br />

2.4.2 Surface Preparation<br />

2.5 Soil Excavation and Backfill Placement<br />

2.5.1 Site Clearing and Grading<br />

2.5.2 Excavation<br />

2.5.3 Loading, Transportation and Disposal<br />

2.5.4 Backfill Placement<br />

2.6 Cap Construction<br />

Liner Placement<br />

Concrete Placement<br />

Drainage Pipe<br />

Permeable Sand<br />

Geotextile Pi acement<br />

Gravel Placement<br />

Paving of <strong>the</strong> Driveway and Surface Chip Seal<br />

2.7 Fence Reconstruction<br />

2.8 Drum Hand1 ing and Disposal<br />

2.9 Compatibility Testing<br />

2.10 Winterization and Demobilization<br />

- PAGE<br />

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TABLE OF CONTENTS<br />

(Continued)<br />

- PAGE<br />

3.0 TRANSPORTATION PLAN 23<br />

3.1 Introduction 23<br />

3.2 Implementation 23<br />

4.0 SITE AND COMMUNITY HEALTH AND SAFETY 24<br />

4.1 Introduction 24<br />

4.2 Revisions to <strong>the</strong> Health and Safety Plan 24<br />

4.3 Key Personnel and Their Responsibilities 24<br />

4.4 Job Hazard Analysis 26<br />

4.4.1 Physical Hazards 26<br />

4.4.1.1 Noise 27<br />

4.4.1.2 Heat Stress 27<br />

4.4.1.3 Construction Equipment 2 7<br />

4.4.1.4 Uneven Terrain 2 7<br />

4.4.1.5 Unstable Stacking of Containers 28<br />

4.4.1.6 Manual Material Handling 28<br />

4.4.1.7 Confined Spaces 28<br />

4.4.2 Chemical Hazards 28<br />

4.5 Air Monitoring 29<br />

4.5.1 Air Monitoring During Liquid Removal Activities 29<br />

4.5.2 Air Monitoring During Soil Excavation Activities 33<br />

4.5.2.1 Summary of Excavation Activities 33<br />

4.5.2.2 Direct Reading Instrumentation 34<br />

4.5.2.3 Integrated Sample Collection and Analysis 38<br />

4.6 Personal Protective Equipment 39


REFERENCES<br />

TABLES<br />

FIGURES<br />

APPENDIX A<br />

APPENDIX B<br />

APPENDIX C<br />

APPENDIX D<br />

4.7 Decontamination Procedures<br />

TABLE OF CONTENTS<br />

(Continued)<br />

4.7.1 Personal Decontamination<br />

4.7.2 Equipment Decontamination<br />

4.8 General Site Health and Safety and Work Rules<br />

4.9 Training<br />

4.10 Medical Monitoring<br />

4.11 Work Zone and Site Security<br />

4.11.1 Exclusion Area<br />

4.11.2 Decontamination Area<br />

4.11.3 Support Area<br />

4.11.4 Site Security<br />

4.12 Community Health and Safety<br />

- PAGE<br />

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TABLE<br />

NUMBER<br />

LIST OF TABLES<br />

Subcontractor List<br />

Summary of Hazardous Waste Disposal<br />

Employee Air Monitoring Coll ection Summary<br />

Ambient Air Monitoring Collection Summary<br />

Employee Air Monitoring Analytical Results<br />

Ambient Air Monitoring Analytical Results


-<br />

-<br />

LIST OF FIGURES<br />

FIGURE DRAWING<br />

NUMBER NUMBER TITLE<br />

1 87-035-E8 Project Schedule<br />

2 87-035-E5 Phase I Staging and Site Working Area<br />

3 87-035-E6 Phase I1 Staging and Site Working Area<br />

4 87-035-B10 Drum Hand1 i ng Site Plan


APPENDIX A<br />

APPENDIX B<br />

APPENDIX C<br />

APPENDIX D<br />

LIST OF APPENDICES<br />

As-Built Construction Drawings<br />

Test Results for Compliance with<br />

Technical Specifications<br />

Laboratory Test Results<br />

HDPE and Geotextile Fabric Instal 1 ation<br />

Procedures


The goal of <strong>the</strong> ERA was to rapidly reduce and mitigate public and<br />

environmental exposure to potentially harmful contaminants. The California<br />

Department of Health Services (DHS) had determined, based on <strong>the</strong> Public<br />

Health and Environmental Risk Assessment (PHERA), that <strong>the</strong> ERA was<br />

necessary to protect <strong>the</strong> public health and to limit risks of continued<br />

exposure due to potential time delays from <strong>the</strong> Remedial Investigation/<br />

Feasibility Study (RI/FS) and Remedial Planning Process. The objectives of<br />

<strong>the</strong> ERA were <strong>the</strong> following:<br />

1. Reduce potential direct contact of people with contaminated soil<br />

in residential and vacant lots on <strong>the</strong> south and east sides of <strong>the</strong><br />

site and within <strong>the</strong> drum yard;<br />

2. Reduce potential future environmental degradation from<br />

contaminated surface water runoff;<br />

3. Remove contaminated materials, tanks, and drums that might have<br />

presented <strong>the</strong> potential for future off-site contamination or<br />

fur<strong>the</strong>r degradation of <strong>the</strong> environment;<br />

4. Reduce <strong>the</strong> hazard of potentially contaminated airborne dust;<br />

5. Reduce <strong>the</strong> potential for fur<strong>the</strong>r degradation of <strong>the</strong> groundwater<br />

beneath <strong>the</strong> site from infiltration of precipitation or runoff.<br />

1.3 Imolementation<br />

The work required to implement <strong>the</strong> ERAS was performed by Canonie's contract<br />

team or <strong>the</strong>ir subcontractors. A list of subcontractors is provided in<br />

Table 1. The actual progression of activities and <strong>the</strong> schedule for any<br />

remaining activities are provided as Figure 1.


The work performed included nine major components:<br />

1. Mobilization and site setup;<br />

2. Demol i tion and disposal of drums, tanks, miscellaneous scrap<br />

metal, fencing, and debris from <strong>the</strong> drum yard;<br />

3. Excavation, grading, and placement of soil cover within <strong>the</strong> drum<br />

yard;<br />

4. Demol ition and disposal of fencing, sheds, concrete, and o<strong>the</strong>r<br />

miscellaneous debris from <strong>the</strong> residential lots;<br />

5. Excavation and disposal of soil from residential lots;<br />

6. Backfill and compaction of excavated areas;<br />

7. Construction of site cap and construction of surface drain system<br />

and retaining structures;<br />

8. Reconstruction of wood fencing;<br />

9. Winterization of site.<br />

The work was performed under <strong>the</strong> direction and supervision of DHS. During<br />

<strong>the</strong> course of <strong>the</strong> site activities, numerous additional activities were<br />

required to enhance <strong>the</strong> construction work and to fur<strong>the</strong>r protect <strong>the</strong> public<br />

from health risks due to exposure. These additional activities included:<br />

1. Increased levels of personal protective equipment by workers;<br />

2. Removal of buried drums and debris;<br />

3. Excavation of additional contaminated soil ;


4. Additional testing of drums and contaminated soil;<br />

5. Working overtime hours to complete critical work tasks;<br />

6. Mobilization of additional equipment and supplies necessary to<br />

meet <strong>the</strong> additional project requirements;<br />

7. Air monitoring and air sample testing;<br />

8. Construction of additional surface water control and drainage<br />

features.<br />

Although <strong>the</strong> time required to complete <strong>the</strong> work increased due to wea<strong>the</strong>r<br />

conditions and increased work activities, <strong>the</strong> project was completed in a<br />

timely fashion and fulfilled <strong>the</strong> goal and purpose of <strong>the</strong> ERA.


2.0 IMPLEMENTATION<br />

As presented in Section 1.0 of this report, <strong>the</strong> work covered under <strong>the</strong><br />

scope of activities included nine major components. The work required by<br />

<strong>the</strong>se components was carried out in accordance with <strong>the</strong> technical<br />

specifications, <strong>the</strong> procedures outlined in Section 2.0, <strong>the</strong> Transportation<br />

Requirements of Section 3.0, and <strong>the</strong> Health and Safety Requirements of<br />

Section 4.0.<br />

Some of <strong>the</strong> specifications and procedures presented in <strong>the</strong> technical<br />

specifications and work plan were modified as required by field conditions.<br />

These modifications were made after <strong>the</strong> necessity for change was determined<br />

by <strong>the</strong> Construction Superintendent and after approval was given by <strong>the</strong><br />

Project Manager. All modifications were authorized by <strong>the</strong> DHS Project<br />

Officer.<br />

2.1 Mobilization and Site Setuo<br />

2.1.1 Mobilization<br />

Mobilization of personnel, equipment, materials, and supplies was carried<br />

out as was necessary to meet <strong>the</strong> requirements of <strong>the</strong> technical<br />

specifications and included <strong>the</strong> specific items and personnel identified and<br />

presented in <strong>the</strong> work plan and reported in <strong>the</strong> financial reports of <strong>the</strong><br />

project. Mobilization of <strong>the</strong>se items was performed just before use.<br />

Transportation of equipment, materials, and supplies to <strong>the</strong> site was along<br />

<strong>the</strong> local routes specified in Section 3.0 of <strong>the</strong> Work Plan.<br />

Delivery dates and arrivals for equipment, materials, supplies, and<br />

personnel were based upon work progress. Materials and supplies were<br />

stored prior to use within <strong>the</strong> site building in <strong>the</strong> areas indicated on<br />

Figure 2. Equipment was stored within <strong>the</strong> fenced area near <strong>the</strong> work being<br />

performed by that equipment.


2.1.2 Site Setuo<br />

During site setup procedures, portions of <strong>the</strong> fencing within <strong>the</strong><br />

residential lots were removed and temporary fencing was placed at <strong>the</strong><br />

approximate locations shown in Figure 3. In addition, temporary fencing<br />

was placed around <strong>the</strong> perimeter of <strong>the</strong> site and a pedestrian walkway was<br />

constructed outside of <strong>the</strong> primary site security fencing. The excavation<br />

was sealed off from <strong>the</strong> residential lots by using temporary fencing lined<br />

with visquene.<br />

Because of <strong>the</strong> temporary nature of <strong>the</strong> site fencing and <strong>the</strong> risk of public<br />

exposure, full time security was maintained at <strong>the</strong> site. These security<br />

measures were necessary to prevent access to <strong>the</strong> site by non-authorized<br />

personnel and <strong>the</strong>reby reduce public exposure and protect onsite supplies<br />

and equipment.<br />

During setup procedures, <strong>the</strong> office areas within <strong>the</strong> building, areas used<br />

by construction personnel, and areas used for material/supply storage were<br />

cleaned. Cleaning of <strong>the</strong> office consisted of boxing all materials, papers,<br />

and debris for future DHS review. All debris, equipment parts, and tanks<br />

outside <strong>the</strong> office and within <strong>the</strong> area required for storage were moved to<br />

o<strong>the</strong>r portions of <strong>the</strong> building outside <strong>the</strong> storage area. These materials<br />

were handled under <strong>the</strong> same level of protection as presented in Section 4.0<br />

of this report.<br />

During preparation of <strong>the</strong> work plan and during site setup activities, <strong>the</strong><br />

City of San Francisco was contacted for <strong>the</strong> purpose of determining permit<br />

procedures and requirements. Due to <strong>the</strong> nature of <strong>the</strong> work (hazardous<br />

waste removal) normal permit procedures did not apply, and confusion<br />

developed concerning <strong>the</strong> type of permitting that would be required.<br />

Because of <strong>the</strong> permit conditions and requirements, delays to <strong>the</strong> project<br />

and increased work requirements resulted. The changes to <strong>the</strong> schedule are


shown in <strong>the</strong> project schedule (Figure 1). Costs associated with <strong>the</strong>se<br />

activities and remobil ization costs are reflected in <strong>the</strong> project financial<br />

reports.<br />

2.1.3 Dailv Records<br />

A daily record of activities of <strong>the</strong> work performed was prepared and<br />

submitted periodically to <strong>the</strong> DHS Project Officer. The reports gave <strong>the</strong><br />

number and type of personnel, <strong>the</strong> equipment used, and a description of <strong>the</strong><br />

work performed. These forms were available for inspection by <strong>the</strong> DHS<br />

Project Officer between submittals.<br />

2.2 Phase I Demo1 ition and Drum Yard Preoaration<br />

2.2.1 Demolition<br />

This section covers <strong>the</strong> work performed to clear and remove all concrete,<br />

rubble, weeds, debris, timbers, scrap metal, fencing, posts, sheet metal,<br />

gates and drums within <strong>the</strong> drum yard. This work was performed as required<br />

by Sections 02020, 02102, and 01037 of <strong>the</strong> technical specifications or as<br />

described herein.<br />

Prior to implementation of <strong>the</strong> ERAS by Canonie, DHS contacted <strong>the</strong> former<br />

operator of <strong>the</strong> BAD facility and arranged to remove many of <strong>the</strong> drums and<br />

equipment from <strong>the</strong> drum yard area. This work was performed before final<br />

pricing of <strong>the</strong> Canonie work, and reduced costs were reflected in <strong>the</strong><br />

authorized amount in <strong>the</strong> task order.<br />

All material within <strong>the</strong> drum yard with <strong>the</strong> exception of <strong>the</strong> boiler tank and<br />

<strong>the</strong> open-top sludge tank was collected by laborers, operators and a Case<br />

580 backhoe. The backhoe was equipped with a backhoe arm and bucket and a<br />

1 oader bucket.


All materials not resting on <strong>the</strong> ground surface were removed from <strong>the</strong>ir<br />

existing locations with <strong>the</strong> backhoe arm and bucket. The backhoe loader<br />

bucket <strong>the</strong>n picked up <strong>the</strong>se materials and placed <strong>the</strong>m into roll-off boxes.<br />

Materials which could not be picked up with <strong>the</strong> backhoe were picked up by<br />

hand and <strong>the</strong>n loaded into <strong>the</strong> backhoe loader bucket for placement into <strong>the</strong><br />

roll-off boxes. Occasionally, due to <strong>the</strong> size and shape of <strong>the</strong> debris,<br />

hand loading into <strong>the</strong> roll-off boxes was required. After <strong>the</strong>se loading<br />

operations were completed, <strong>the</strong> surface of <strong>the</strong> drum site was scraped with<br />

<strong>the</strong> backhoe bucket and small bulldozer, and small debris and rubble was<br />

collected and loaded into a roll-off box.<br />

All personnel performed <strong>the</strong> demolition work under <strong>the</strong> level of protection<br />

specified in Section 4.7 of this report. Before any activity for debris<br />

removal and site grading, <strong>the</strong> ground surface was moistened to reduce <strong>the</strong><br />

creation of and exposure to dust.<br />

2.2.2 Additional Excavation and Drum Removal<br />

During demo1 ition of <strong>the</strong> wood fencing dividing <strong>the</strong> drum yard and <strong>the</strong> vacant<br />

lot, several drums were uncovered beneath <strong>the</strong> surface of <strong>the</strong> drum yard.<br />

Upon fur<strong>the</strong>r investigation (excavation along <strong>the</strong> fence1 ine) additional<br />

drums were found with capacities of about 30 gallons and filled with fluids<br />

and gravel. These drums were excavated using <strong>the</strong> Case 580 backhoe, placed<br />

in empty 55-gallon drums, and <strong>the</strong>n stored inside <strong>the</strong> building.<br />

During excavation of <strong>the</strong> drums Health and Safety personal protective<br />

equipment was upgraded to Level B protection. In addition to <strong>the</strong> drum<br />

removal, additional contaminated soil within this area was also removed.<br />

2.2.3 Utility Protection<br />

The utilities identified within <strong>the</strong> drum yard were above ground power<br />

poles, <strong>the</strong>ir guide wires, monitoring wells, and an underground gas 1 ine.<br />

During site construction activities, equipment maintained a safe distance


from all power 1 ines, monitoring wells, guy wires, and gas lines. All work<br />

performed near any utilities was done by hand, if it was felt that safe<br />

distances could not be maintained with construction equipment. In<br />

addition, a protective casing made of cinder blocks was placed around <strong>the</strong><br />

monitoring well in <strong>the</strong> vacant lot to prevent damage during fill operations.<br />

During <strong>the</strong> course of <strong>the</strong> work, one gas line not previously located was<br />

uncovered and struck by <strong>the</strong> backhoe bucket. PG&E was notified, and after<br />

an inspection, indicated that no damage to <strong>the</strong> line had occurred.<br />

Accordingly PG&E authorized completion of <strong>the</strong> backfill operation.<br />

2.2.4 Site grad in^ and Surface Preoaration<br />

The site grading and surface preparation within <strong>the</strong> drum yard was performed<br />

concurrent with demolition operations and as was required by Section 02232<br />

of <strong>the</strong> technical specifications or as specified herein. Activities for<br />

site grading included:<br />

o Excavation of soil required to bring <strong>the</strong> existing surface of <strong>the</strong> drum<br />

yard to grade;<br />

o Excavation of drainage ditch areas;<br />

o Equipment decontamination;<br />

o Placement and compaction of three inches of cover material;<br />

o Placement and lining of roll-off boxes.<br />

Subgrade preparation and protection complied with Section 02232,<br />

Subsections 3.1 and 3.3 of <strong>the</strong> technical specifications.<br />

2.2.4.1 Soil Excavation<br />

The excavation of soil in <strong>the</strong> drum yard needed to bring <strong>the</strong> surface to <strong>the</strong><br />

required grade was performed using <strong>the</strong> Case 580 bucket and a CAT D-3<br />

bulldozer (equivalent).


A grid system was established along <strong>the</strong> curbs and <strong>the</strong> building, and <strong>the</strong><br />

surface of <strong>the</strong> yard was surveyed periodically to control elevation<br />

requirements. Surveying was performed after excavation, subgrade<br />

preparation, and backfilling. Excess material over that required to grade<br />

<strong>the</strong> site was stockpiled on <strong>the</strong> surface of <strong>the</strong> drum yard. This stockpiled<br />

material was loaded into trucks during removal of residential soils and in<br />

accordance with <strong>the</strong> procedures presented in Section 2.5 of <strong>the</strong> Work Plan.<br />

Drums containing drill cuttings, which had been transferred from <strong>the</strong> drum<br />

yard to <strong>the</strong> building, were brought back out to <strong>the</strong> stockpile, opened and<br />

dumped into <strong>the</strong> pile. The emptied drums were <strong>the</strong>n carried back into <strong>the</strong><br />

building. The emptied contents were disposed with <strong>the</strong> residential soils.<br />

2.2.4.2 Drainaqe Ditch Excavation<br />

Excavation of <strong>the</strong> drainage ditch areas conformed to Section 2200, and to<br />

<strong>the</strong> As-built Construction Drawings in Appendix A of this implementation<br />

report. The position of <strong>the</strong> ditch along Thomas Street was altered slightly<br />

to accommodate two monitoring wells. This excavation was performed with<br />

<strong>the</strong> backhoe and dozer. Grade was checked and controlled by periodic<br />

surveying.<br />

All materials excavated in <strong>the</strong> drainage ditch area were stockpiled for<br />

disposal along with <strong>the</strong> residential soils. Use of hand tools and labor was<br />

required to protect utilities during construction.<br />

2.2.4.3 Eouipment Decontamination<br />

Equipment used during Phase I work was decontaminated when this equipment<br />

was required to cross between contaminated areas and noncontaminated areas,<br />

and when site grading operations were completed.<br />

The decontamination was performed by placing plastic in an area between <strong>the</strong><br />

contaminated area and <strong>the</strong> noncontaminated area. The equipment was <strong>the</strong>n<br />

driven slowly onto <strong>the</strong> plastic, steam cleaned, and <strong>the</strong>n driven slowly onto<br />

<strong>the</strong> noncontaminated area. The steam cleaning water was allowed to drain


off <strong>the</strong> plastic onto <strong>the</strong> drum yard. This water helped in dust suppression<br />

and contributed to moisture content for compaction. All workers wore<br />

safety glasses, PVC rain pants or polycoated Tyveks, and rubber boots<br />

during steam cleaning operations.<br />

2.2.4.4 Placement of Cover<br />

After <strong>the</strong> site grading and drainage ditch excavation, a three-inch<br />

(compacted thickness) lift of fill material was placed over <strong>the</strong> drum yard.<br />

This cover was graded by Esquivel Grading and Paving and was compacted by<br />

Canonie personnel. The fill was placed to provide a clean surface for<br />

operation of equipment and personnel, to cover any sharp objects or o<strong>the</strong>r<br />

protrusions which might affect <strong>the</strong> performance of <strong>the</strong> liner, and to provide<br />

a roadway surface between <strong>the</strong> vacant lot and <strong>the</strong> drum yard. The cover<br />

material was dumped in <strong>the</strong> vacant lot and <strong>the</strong>n spread with <strong>the</strong> dozer to <strong>the</strong><br />

required thickness. The cover material met <strong>the</strong> specifications for fine<br />

fill of Section 2200, Subsection 2.5 of <strong>the</strong> technical specifications. The<br />

results of compliance testing are provided in Appendix B.<br />

Once <strong>the</strong> cover material had reached <strong>the</strong> drum yard, a test section for<br />

compaction was constructed. The purpose of <strong>the</strong> test section was to verify<br />

that <strong>the</strong> compaction required by Section 02200, Subsection 1.4.1 could be<br />

achieved by compacting <strong>the</strong> cover surface.<br />

2.2.4.5 Orphan Drums<br />

During this phase of implementation, fifteen 55-gallon drums were left in<br />

<strong>the</strong> street outside <strong>the</strong> Hawes Street gate. These drums were brought into<br />

<strong>the</strong> drum yard where <strong>the</strong>y were inspected by <strong>the</strong> DHS Enforcement Division.<br />

The drums were <strong>the</strong>n moved inside <strong>the</strong> building. Samples were taken from <strong>the</strong><br />

drums, tested by Canonie and profiled by CWM, or sent to DHS laboratories.


2.2.4.6 Preoaration of Roll-Off Boxes<br />

The roll-off boxes were lined with 5-mil thick plastic sheets before<br />

placement of any waste materi a1 s.<br />

2.3 Removal of Liauids and Sludqes<br />

To expedite <strong>the</strong> removal process, samples of <strong>the</strong> liquid and sludge materials<br />

for <strong>the</strong> on-site tanks and <strong>the</strong> sump were obtained before implementation of<br />

<strong>the</strong> work plan. The samples were obtained and tested for compatibility and<br />

chemical content. Chemical compatibility testing conformed to <strong>the</strong> testing<br />

requirements as outlined in Section 2.10. Chemical content testing was<br />

performed as required for <strong>the</strong> determination of <strong>the</strong> disposal profile and for<br />

acceptance by <strong>the</strong> Kettleman Hills disposal facility. The results of <strong>the</strong>se<br />

tests are provided in Appendix C.<br />

2.3.1 Sludae Tank<br />

The liquids were removed from <strong>the</strong> sludge tank by being pumped into 55-<br />

gallon drums. After pumping, solids and sludges were removed and placed<br />

into 55-gallon drums using <strong>the</strong> Case 580 backhoe with a twelve-inch bucket.<br />

The outside surface of <strong>the</strong> 55-gallon drums were shea<strong>the</strong>d in plastic so that<br />

this surface would be kept clean. The drums were placed in a berm<br />

constructed of plastic sheeting and absorbant in case spillage occurred.<br />

Residual sol ids were removed by hand excavations. After cleaning, <strong>the</strong> tank<br />

was loaded with yard debris, placed on a flatbed truck, and transported to<br />

<strong>the</strong> Kettleman Hills disposal facility. The tank was picked up by a crane<br />

with steel cables wrapped around each end of <strong>the</strong> tank and connected in <strong>the</strong><br />

middle. The cables were <strong>the</strong>n secured to <strong>the</strong> lifting arm of <strong>the</strong> crane and<br />

<strong>the</strong> tank was lifted onto <strong>the</strong> truck.<br />

2.3.2 Boiler Tank<br />

The 1 iquid from <strong>the</strong> boiler tank was collected into 55-gallon drums. The<br />

liquid was drained through a valve at <strong>the</strong> bottom of <strong>the</strong> tank and into 5-


gallon buckets. These buckets were <strong>the</strong>n emptied into 55-gallon drums.<br />

After <strong>the</strong> liquids from <strong>the</strong> boiler tank had been removed, <strong>the</strong> boiler tank<br />

was lifted onto a truck and transported to Levin Scrap for metal salvage.<br />

2.3.3 Sumo and Dio Tanks<br />

The liquids from <strong>the</strong> sump area and dip tanks (inside <strong>the</strong> building) were<br />

removed in <strong>the</strong> same way as liquids from <strong>the</strong> sludge tank.<br />

2.3.4 Worker Protection<br />

During liquid removal operations and cleaning of <strong>the</strong> inside<br />

materials/supply storage areas and sump areas, all workers wore protection<br />

equipment as required by Section 4.7 of this report. In addition, all work<br />

was performed under <strong>the</strong> direction of a construction supervisor with<br />

demonstrated experience in similar operations.<br />

2.4 Phase I1 Demo1 ition and Residential Yard Preoaration<br />

2.4.1 Demolition<br />

This section covers <strong>the</strong> work that was required to clear and remove all<br />

concrete rubble, weeds, debris, timbers, scrap metal, fencing, posts,<br />

trees, shrubs, and <strong>the</strong> structure (woodshed) within <strong>the</strong> work area. This<br />

work was performed as required by Sections 02020, 02102, and 01037 of <strong>the</strong><br />

technical specifications or as described herein.<br />

All material within <strong>the</strong> residential lots was handled or o<strong>the</strong>rwise collected<br />

using laborers, operators and a Case 580 backhoe. The backhoe was equipped<br />

with a backhoe arm and bucket and a loader bucket.<br />

All materials not resting on <strong>the</strong> ground surface, with <strong>the</strong> exception of <strong>the</strong><br />

trees, shrubs, and weeds, were removed from <strong>the</strong>ir existing location by <strong>the</strong><br />

backhoe arm. The material was <strong>the</strong>n picked up by hand and loaded into <strong>the</strong><br />

loader bucket. The backhoe <strong>the</strong>n transported <strong>the</strong> materials to <strong>the</strong> roll-off


ox marked "nonhazardous materials" (prepared according to Section 2.2.3).<br />

Any materials that were stained or o<strong>the</strong>rwise considered hazardous were<br />

separated from nonhazardous materials and loaded into roll-off boxes marked<br />

as "hazardous materials. " Table 2 provides a summary of <strong>the</strong> hazardous<br />

materials which were transported off-site.<br />

Trees and shrubs were cut flush with <strong>the</strong> ground surface, loaded into <strong>the</strong><br />

loader bucket, and placed into <strong>the</strong> nonhazardous roll -off boxes. All<br />

personnel performed <strong>the</strong> demo1 i tion work under levels of protection required<br />

by Section 4.7. Before performing any activities during debris removal and<br />

excavation operations, <strong>the</strong> surface of <strong>the</strong> ground was moistened to reduce<br />

creation of and exposure to dust.<br />

2.4.2 Surface Preoaration<br />

After demolition operations, a three-inch lift of fill material was placed<br />

by Canonie and graded by Esquivel Grading and Paving over <strong>the</strong> drum yard<br />

surface. The material was placed to provide a clean surface for operation<br />

of equipment and personnel. An additional thickness of fill was placed as<br />

required to produce a level surface for operation of excavation equipment.<br />

The cover material was dumped in <strong>the</strong> vacant lot and spread by <strong>the</strong> bulldozer<br />

until <strong>the</strong> required thickness and a level surface were achieved. The<br />

surface of <strong>the</strong> fill was compacted only as necessary to allow operation of<br />

equipment over <strong>the</strong> surface.<br />

2.5 Soil Excavation and Backfill Placement<br />

2.5.1 Site Clearinq and Gradinq<br />

Site clearing and grading was performed before excavation ofdesignated<br />

soils with procedures similar to those outlined in Section 2.2. This work<br />

was performed using equipment and personnel as presented in Section 5.0 of<br />

<strong>the</strong> Work Plan or as shown in <strong>the</strong> project financial reports.


2.5.2 Excavation<br />

The excavation of designated soils and buried debris was performed to meet<br />

<strong>the</strong> requirements of Section 02200, Subsection 3.1 of <strong>the</strong> technical<br />

specifications, or as specified herein. Equipment used to perform <strong>the</strong> work<br />

is listed in Section 5.0 of <strong>the</strong> Work Plan and/or in <strong>the</strong> project financial<br />

reports, and as is outlined in this section. The soil was excavated and<br />

placed directly into waiting dump trucks and transported to <strong>the</strong> disposal<br />

facility along <strong>the</strong> route presented in Section 3.0. Soils were dampened as<br />

necessary to reduce <strong>the</strong> potential for exposure to dust particles during<br />

excavation operations.<br />

Cut slopes within <strong>the</strong> excavated areas were maintained at slopes no steeper<br />

than 1H:lV or as was required by safety and as designated by <strong>the</strong> on-site<br />

engineer and approved by <strong>the</strong> site Health and Safety Officer.<br />

The excavation began in Yard 3. To prevent spillage, <strong>the</strong> backhoe excavated<br />

<strong>the</strong> soil keeping <strong>the</strong> bucket not more than three-quarters full of soil. The<br />

backhoe rotated in a counter clockwise direction (toward <strong>the</strong> drum yard) and<br />

placed <strong>the</strong> material in <strong>the</strong> truck.<br />

The truck was backed up directly beside <strong>the</strong> backhoe to limit <strong>the</strong> distance<br />

<strong>the</strong> material was carried before placement. Once <strong>the</strong> truck was loaded, <strong>the</strong><br />

plastic 1 iner (placed in <strong>the</strong> truck before loading) was folded over <strong>the</strong><br />

material and securely tied down. The truck would <strong>the</strong>n leave <strong>the</strong> area<br />

through <strong>the</strong> drum yard as shown on Figure 3.<br />

The excavation proceeded away from Yard 3. When <strong>the</strong>re was no longer enough<br />

room for <strong>the</strong> trucks to maneuver behind <strong>the</strong> backhoe, <strong>the</strong> trucks entered by<br />

<strong>the</strong> Hawes Street entrance and parked alongside <strong>the</strong> backhoe as shown on<br />

Figure 3. When <strong>the</strong> backhoe reached <strong>the</strong> edge of <strong>the</strong> building, it turned and<br />

proceeded into <strong>the</strong> vacant lot. Any areas of contaminated soil which could<br />

not be excavated with <strong>the</strong> backhoe were removed by hand.


After <strong>the</strong> excavation had been completed, <strong>the</strong> bucket areas of <strong>the</strong> backhoe<br />

arm that came in contact with <strong>the</strong> contaminated soil were steam cleaned over<br />

a plastic berm. This rinsate was collected in a 55-gallon drum. Air<br />

monitoring was performed prior to and during <strong>the</strong> excavation operation. The<br />

procedures and results of <strong>the</strong> air monitoring are provided in Section 4.5.<br />

2.5.3 Loadinq. Transoortation and Disoosal<br />

Excavated soil was loaded directly into waiting dump trucks (as described<br />

in Section 2.5.2) for transportation to <strong>the</strong> disposal facility. The<br />

equipment and personnel used to perform <strong>the</strong>se tasks were as provided for in<br />

Section 5.0 of <strong>the</strong> Work Plan and/or listed in <strong>the</strong> project financial<br />

reports. Transportation of loaded soils was carried out in accordance with<br />

<strong>the</strong> transportation plan provided in Section 3.0 of <strong>the</strong> Work Plan.<br />

During <strong>the</strong> excavation activities, <strong>the</strong> presence of vinyl chloride was<br />

suspected because of air monitoring results. Increased Health and Safety<br />

precautions, project standby time, and o<strong>the</strong>r delays resulted during <strong>the</strong><br />

period that <strong>the</strong> presence or absence of vinyl chloride was being evaluated.<br />

The procedures and results of <strong>the</strong> air monitoring for vinyl chloride are<br />

presented in Section 4.5.<br />

Laboratory analyses on <strong>the</strong> soils for determination of vinyl chloride are<br />

provided in Appendix C.<br />

2.5.4 Backfill Placement<br />

Backfill operations were performed as required by Section 02200 of <strong>the</strong><br />

technical specifications or as described herein.<br />

Backfilling began in <strong>the</strong> vacant lot, where <strong>the</strong> deep PCB pit was first<br />

brought up to <strong>the</strong> same grade as <strong>the</strong> excavation in <strong>the</strong> residential lot.<br />

Backfill soil in <strong>the</strong> vacant lot was placed in 8-inch thick lifts and


compacted with <strong>the</strong> backhoe bucket and by wheel rolling. Compaction near<br />

foundations and monitoring wells was performed with a hand-held Wacker<br />

rammer-type compactor.<br />

From <strong>the</strong> vacant lot <strong>the</strong> backfill operations proceeded into Yard #1, and<br />

<strong>the</strong>n into Yards #2 and #3. The backfill soil was pushed in front of <strong>the</strong><br />

backhoe so that <strong>the</strong> backhoe was only in contact with <strong>the</strong> clean imported<br />

soil .<br />

In <strong>the</strong> vacant lot and in <strong>the</strong> residential lots, <strong>the</strong> backfill soil below a<br />

depth of two feet from finish grade was common fill, as described in<br />

Section 02200, Subsection 2.4. Between <strong>the</strong> depths of 1 foot and 2 feet,<br />

<strong>the</strong> backfill soil was topsoil as described in Section 02200, Subsection<br />

2.1, compacted by wheel rolling. At depths from finish grade to 1 foot,<br />

<strong>the</strong> backfill was uncompacted topsoil.<br />

The trench separating <strong>the</strong> vacant lot from <strong>the</strong> drumyard was backfilled using<br />

common fill. This soil was placed in 12-inch lifts and was compacted by<br />

using <strong>the</strong> backhoe bucket and by wheel rolling.<br />

2.6 Cao Construction<br />

The placement of <strong>the</strong> HDPE Syn<strong>the</strong>tic Membrane was performed as required by<br />

Sections 02200, 02232, 02400, 03300, and 07114 of <strong>the</strong> technical<br />

specifications except that <strong>the</strong> precleaning of <strong>the</strong> existing concrete slab<br />

and sump areas was performed before final site grading and cap placement.<br />

The concrete slab shown in Figure 2 was scraped with <strong>the</strong> Case 580 backhoe<br />

and was <strong>the</strong>n steam cleaned. Steam cleaning water was allowed to flow onto<br />

<strong>the</strong> ground surface.<br />

2.6.1 Liner Placement<br />

The syn<strong>the</strong>tic 1 iner was supplied and <strong>the</strong> instal lation supervised by Nilex<br />

USA, Inc. All submittals required by Section 07114, Subsection 1.5 and


1.6, Section 07115, Subsection 1.4 and 1.5, specific methodology for liner<br />

placement field scanning, and placement of boots for monitoring wells,<br />

telephone poles, guide wires, fence posts, and o<strong>the</strong>r structures penetrating<br />

<strong>the</strong> liner were prepared by Canonie with cooperation and information from<br />

Nilex. This information was submitted to DHS two weeks before liner<br />

installation and is included as Appendix D.<br />

Upon delivery, <strong>the</strong> HDPE liner was stored in <strong>the</strong> area shown on Figure 4.<br />

When it was determined that <strong>the</strong> drum yard subgrade was completed, <strong>the</strong> liner<br />

was removed from <strong>the</strong> storage area and placed onto <strong>the</strong> drum yard using an<br />

extended arm crane. The 1 iner was rolled out and placed into position by<br />

laborers. A Nilex field technician <strong>the</strong>n fused <strong>the</strong> sheets of HDPE toge<strong>the</strong>r<br />

as per <strong>the</strong> working details that Nilex had provided. Nilex suggested that a<br />

better seal around <strong>the</strong> monitoring wells could be achieved if <strong>the</strong> concrete<br />

utility boxes were replaced with sono tubes. This would allow <strong>the</strong><br />

performed pipe boots to be used instead of using a field weld. This method<br />

was determined to be acceptable by Canonie, DHS, and CH2M HILL so long as<br />

<strong>the</strong> utility boxes were replaced and accessiblity to <strong>the</strong> monitoring wells<br />

maintained. Plans were made for utility box replacement so that <strong>the</strong> sono<br />

tubes could be used.<br />

Field vacuum testing and laboratory destructive testing of <strong>the</strong> liner seams<br />

were performed. Any seams that proved to be inadequately welded were re-<br />

welded and tested again to insure <strong>the</strong>ir integrity.<br />

2.6.2 Concrete Placement<br />

The placement of <strong>the</strong> concrete curb and catch basin conformed to Section<br />

03300 of <strong>the</strong> Construction Specifications and as is shown on <strong>the</strong><br />

construction drawings. The concrete curb was placed and allowed to cure<br />

five days before placement of final subsurface cover material and HDPE<br />

liner. The existing curb around <strong>the</strong> sump was removed and <strong>the</strong> sump<br />

backfilled with concrete so that <strong>the</strong> newly constructed curb could be<br />

extended over <strong>the</strong> sump. After <strong>the</strong> curb had been cured, <strong>the</strong> HDPE liner was<br />

fastened to <strong>the</strong> curb with Hilti concrete anchorages.


The concrete catch basin was purchased from <strong>the</strong> Santa Rosa Cast Products<br />

Company. The catch basin was installed after <strong>the</strong> placement of <strong>the</strong> liner.<br />

Tommy Lee of <strong>the</strong> San Francisco Department of Public Works (SFDPW) was<br />

present during <strong>the</strong> placement of <strong>the</strong> basin and approved <strong>the</strong> basin connection<br />

to <strong>the</strong> city sewer system.<br />

2.6.3 Drainaqe Pioe<br />

The drainage pipe was installed after completion of <strong>the</strong> liner installation.<br />

All pipe was installed as required by <strong>the</strong> construction drawings and<br />

according to Section 02400 of <strong>the</strong> technical specifications, except for <strong>the</strong><br />

length of pipe running parallel to Thomas Street. Because of <strong>the</strong> position<br />

of <strong>the</strong> monitoring wells, this section of pipe was positioned five feet from<br />

<strong>the</strong> curb instead of <strong>the</strong> three feet as originally provided by <strong>the</strong> plans.<br />

2.6.4 Permeable Sand<br />

Samples of <strong>the</strong> sand required for placement above <strong>the</strong> liner were obtained<br />

and tested as required by Section 02200 of <strong>the</strong> technical specifications.<br />

The results of <strong>the</strong>se tests were provided to DHS before delivery of <strong>the</strong> sand<br />

to <strong>the</strong> site and are included in Appendix B.<br />

The sand was end-dumped in <strong>the</strong> vacant lot and spread (full thickness) with<br />

<strong>the</strong> backhoe. The sand was completely spread over <strong>the</strong> liner but compaction<br />

was not completed until winter rains had subsided and <strong>the</strong> sand had dried.<br />

After <strong>the</strong> sand had dried sufficiently, <strong>the</strong> grade was checked and some<br />

additional sand was added and distributed with a Bobcat where needed.<br />

Compaction of <strong>the</strong> sand was performed with hand-held vibrating plate<br />

compactors. Water was added as necessary to achieve <strong>the</strong> compaction<br />

required.<br />

In order to prevent subgrade ponding at <strong>the</strong> drain inlet prior to <strong>the</strong><br />

completion of <strong>the</strong> cap seal coat, holes were drilled into <strong>the</strong> side of <strong>the</strong><br />

drain box beneath <strong>the</strong> drain box inlet and above <strong>the</strong> syn<strong>the</strong>tic membrane.


2.6.5 Geotextile Placement<br />

Geotextile fabric was placed as required by Section 07115 of <strong>the</strong> technical<br />

specifications and as described herein. Correspondence from <strong>the</strong><br />

manufacturer provided additional instructions regarding storage, handling<br />

and installation, and is included in Appendix D (James M. Cramer, Vice<br />

President, Nilex USA Inc., California Branch, letter dated February 13,<br />

1988). Following <strong>the</strong> manufacturer's instructions, <strong>the</strong> seams of <strong>the</strong><br />

geotextile were not bonded, but were overlapped two feet to provide proper<br />

continuity of <strong>the</strong> fabric.<br />

2.6.6 Gravel Placement<br />

The Class 2 aggregate base layer for <strong>the</strong> top 6 inches of <strong>the</strong> cap was placed<br />

as required by Section 02200 of <strong>the</strong> technical specifications. The<br />

aggregate was dumped and spread with a Massey Ferguson loader and compacted<br />

with a Bomag 100 roller. Moisture was added as required to achieve proper<br />

compaction. The base was spread and compacted so that <strong>the</strong> trucks always<br />

ran over <strong>the</strong> compacted base and did not disturb <strong>the</strong> liner. Compaction<br />

around <strong>the</strong> wells, fence tubes and Christy boxes was achieved with a hand-<br />

held Wacker rammer-type compactor.<br />

2.6.7 Pavinq of <strong>the</strong> Drivewav and Surface chi^ Seal<br />

Paving of <strong>the</strong> driveway and installation of <strong>the</strong> chip seal coating on <strong>the</strong> cap<br />

was performed as required by Sections 02510 and 02605 of <strong>the</strong> technical<br />

specifications. Inspection of <strong>the</strong> site after rainfall indicated that<br />

drainage from <strong>the</strong> site was working effectively and no ponding was evident.<br />

Some additional work was performed to protect <strong>the</strong> DHS monitoring wells on<br />

site and provide ease of access to <strong>the</strong>se wells. Christy boxes were<br />

installed around five monitoring wells within <strong>the</strong> cap area, flush with <strong>the</strong><br />

final grade. Structural concrete was used to cement inside <strong>the</strong> box and<br />

bring <strong>the</strong> well grout back up to final grade.


O<strong>the</strong>r additional work was performed to control drainage and prevent surface<br />

runoff from getting under <strong>the</strong> liner at <strong>the</strong> edge of <strong>the</strong> drum yard. Asphalt<br />

concrete berms were installed at several locations. These included <strong>the</strong><br />

following: adjacent to <strong>the</strong> Bay Area Drum and machine shop/plating shop<br />

buildings; across <strong>the</strong> former driveway and across <strong>the</strong> asphalt walkways by<br />

<strong>the</strong> building and machine shop; and between <strong>the</strong> drum yard and <strong>the</strong> vacant<br />

1 ot.<br />

2.7 Fence Reconstruction<br />

Because of rain delays, only Phase I of <strong>the</strong> fence reconstruction was<br />

performed. Phase I reconstruction included replacing <strong>the</strong> fences in <strong>the</strong><br />

residential lots and placing <strong>the</strong> sono tubes in <strong>the</strong> drum yard area. This<br />

work was performed after placement of <strong>the</strong> three inches of cover over <strong>the</strong><br />

drum yard and <strong>the</strong> excavation and backfilling of <strong>the</strong> residential lots.<br />

Phase I fencing was provided and installed by With Fencing, Inc. according<br />

to Section 02445 of <strong>the</strong> technical specifications.<br />

Sono tubes were placed using a hand auger or <strong>the</strong> Case 580 backhoe.<br />

Excavated soils were collected and disposed of with <strong>the</strong> residential soils.<br />

The excavated area around each sono tube was backfilled with fine soil and<br />

compacted with a hand-held Wacker rammer-type compactor.<br />

Final permanent fencing work is expected to be completed in <strong>the</strong> near<br />

future.<br />

2.8 Drum Handlina and Disoosal<br />

Drum handling and disposal will be performed at a later I date.<br />

2.9 Comoatibilitv Testinq<br />

Compatibility testing will be performed at a later date.


2.10 Winterization and Demobilization<br />

Winterization of <strong>the</strong> site was performed to prevent rain damage to <strong>the</strong> site<br />

during <strong>the</strong> seasonal rains.<br />

Site winterization consisted of sealing <strong>the</strong> site against rainwater<br />

infiltration, securing <strong>the</strong> site against outside intrusion, and removing<br />

rainwater that had collected in <strong>the</strong> building.<br />

To protect <strong>the</strong> site from rain, visquene was placed over <strong>the</strong> street curb to<br />

liner joint, <strong>the</strong> HDPE liner was completely covered with sand, <strong>the</strong> sono<br />

tubes were sealed with visquene and duct tape, and plywood was propped over<br />

<strong>the</strong> gap between <strong>the</strong> building and <strong>the</strong> concrete containment curb.<br />

The site perimeter was secured by placing temporary fencing along <strong>the</strong><br />

backyard of <strong>the</strong> Madison residence, by wiring shut <strong>the</strong> gap in <strong>the</strong> Shafter<br />

Street access gate, and by securely locking all site doors and gates.<br />

Samples of water were collected from <strong>the</strong> drum storage area inside <strong>the</strong><br />

building and sent to DHS laboratories for chemical analyses. These results<br />

have been forwarded to Tommy Lee of <strong>the</strong> SFDPW. A temporary sump pump has<br />

been placed in <strong>the</strong> drum storage area, and Mr. Lee has approved <strong>the</strong><br />

discharge of any water collected into <strong>the</strong> city sewer system.


3.1 Introduction<br />

3.0 TRANSPORTATION PLAN<br />

The transportation phase of <strong>the</strong> Bay Area Drum ERA was critical in that it<br />

represented <strong>the</strong> portion of <strong>the</strong> project which had, although limited, <strong>the</strong><br />

greatest potential for public exposure outside of <strong>the</strong> immediate project<br />

area. Therefore, Canonie had developed a plan for loading and<br />

transportation of <strong>the</strong> hazardous waste to <strong>the</strong> Kettleman Hills disposal<br />

facility with <strong>the</strong> assistance of Chemical Waste Management, Enrac Division<br />

(CWM) and DHS. In <strong>the</strong> development of this plan, Canonie had considered<br />

issues of personnel and pub1 ic safety, regulatory compliance, and<br />

operational efficiency. The plan was presented in Section 3.0 of <strong>the</strong> Work<br />

Plan.<br />

3.2 Imolementation<br />

During implementation of <strong>the</strong> ERA for Bay Area Drum, <strong>the</strong> transportation plan<br />

was followed. No spill or need for emergency response occurred during <strong>the</strong><br />

performance of <strong>the</strong> work.


4.1 Introduction<br />

4.0 SITE AND COMMUNITY HEALTH AND SAFETY<br />

The work performed in implementing <strong>the</strong> Health and Safety Plan was designed<br />

as a practical approach to accomplishing <strong>the</strong> ERA activities considering <strong>the</strong><br />

occupational and public health hazards anticipated at <strong>the</strong> site. The Health<br />

and Safety procedures applied to all site activities carried out under <strong>the</strong><br />

Expedited Response Action (ERA) at <strong>the</strong> BAD site.<br />

All on-si te personnel, enforcement agency personnel, and visitors were<br />

required to familiarize <strong>the</strong>mselves with and comply with provisions of <strong>the</strong><br />

Health and Safety Plan. Canonie provided health and safety equipment for<br />

Canonie employees and subcontractors. All o<strong>the</strong>r personnel provided equal<br />

or greater levels of protection for <strong>the</strong>mselves.<br />

4.2 Revisions to <strong>the</strong> Health and Safety Plan<br />

Because conditions varied, <strong>the</strong> original plan presented in Section 4.0 of<br />

<strong>the</strong> work plan was upgraded and downgraded, as appropriate, depending on<br />

site conditions. All changes to <strong>the</strong> Health and Safety Plan were determined<br />

or approved by <strong>the</strong> site Health and Safety Officer and discussed with <strong>the</strong><br />

Project Officer.<br />

4.3 Kev Personnel and Their Res~onsi bil ities<br />

The following list names <strong>the</strong> key personnel who were assigned to <strong>the</strong> project<br />

for implementation of <strong>the</strong> ERA. Details of <strong>the</strong>ir experience and technical<br />

levels were provided in Appendix C of <strong>the</strong> work plan. Additional personnel<br />

required to implement <strong>the</strong> ERA were determined after approval of <strong>the</strong> work<br />

plan and pricing proposal and before performance of <strong>the</strong> work required by<br />

such personnel.


1. Richard J. Greenwood, P.E.: Mr. Greenwood was <strong>the</strong> Canonie project<br />

manager; he was responsible for <strong>the</strong> overall project management<br />

including <strong>the</strong> Health and Safety Plan.<br />

2. Jack Isley: Mr. Isley was <strong>the</strong> project construction manager and<br />

was responsible for technical assistance during handling of<br />

hazardous materi a1 s.<br />

3. Keith Pushaw: Mr. Pushaw was <strong>the</strong> project construction<br />

superintendent and was responsible for review of profiling and<br />

disposal procedures and for verification of all work in accordance<br />

with state and Federal requirements for disposal of hazardous<br />

wastes. Mr. Pushaw was also responsible for preparation and<br />

review of drum handling and compatibility testing procedures.<br />

4. Arlen Saxton: Mr. Saxton was <strong>the</strong> project construction supervisor<br />

and was responsible for on-site activities including handling of<br />

hazardous materials; he was directly responsible for personnel<br />

compliance with <strong>the</strong> Health and Safety Plan; Mr. Saxton is<br />

certified in first aid and CPR and was designated as agent to<br />

notify paramedics and <strong>the</strong> fire department in <strong>the</strong> event of an<br />

emergency.<br />

5. Brian Hickam and Mike Endicott: Mr. Hickam and Mr. Endicott were<br />

<strong>the</strong> project construction foremen. They were responsible for<br />

assisting <strong>the</strong> project work, for directing project laborers, and<br />

for taking over <strong>the</strong> responsibilities of <strong>the</strong> project supervisor in<br />

<strong>the</strong> event that Mr. Saxton was not available.<br />

6. Michael Strebeck: Mr. Strebeck is a Level 3 professional and<br />

assisted in <strong>the</strong> project during <strong>the</strong> course of <strong>the</strong> work. Mr.<br />

Strebeck's responsibilities were to act as <strong>the</strong> agent for <strong>the</strong><br />

project manager in <strong>the</strong> event that <strong>the</strong> project manager was not<br />

available.


James Babcock: Mr. Babcock is a Level 4 professional and assisted<br />

in <strong>the</strong> project during winterization activities and completion of<br />

<strong>the</strong> site cap. Mr. Babcock's responsibilities were to act as <strong>the</strong><br />

agent for <strong>the</strong> project manager in <strong>the</strong> event that <strong>the</strong> project<br />

manager was not available.<br />

Susan Walker: Certified Industrial Hygienist (CIH) : Ms. Walker<br />

was <strong>the</strong> site Health and Safety Officer; she was responsible for<br />

implementation and management of <strong>the</strong> site Health and Safety Plan.<br />

Kurt Ahlich: Mr. Ahlich was responsible for on-site quality<br />

control, maintaining site records, and engineering activities<br />

required during field activities.<br />

Albert Elizondo: Mr. Elizondo is a Level 2 professional and<br />

assisted in <strong>the</strong> project during winterization activities and<br />

completion of <strong>the</strong> cap. Mr. Elizondo's responsibilities were to<br />

assist in completion of <strong>the</strong> work and assist Mr. Ahlich in his<br />

responsibilities.<br />

Michael Klein: Mr. Klein is a Level 1 professional and assisted<br />

in <strong>the</strong> project during <strong>the</strong> course of <strong>the</strong> work. Mr. Klein's<br />

responsibilities were to assist Mr. Ahlich in his<br />

responsibilities.<br />

4.4 ~ o Hazard b Analysis<br />

4.4.1 Phvsical Hazards<br />

The major physical hazards at <strong>the</strong> site included <strong>the</strong> following:<br />

1. Noise<br />

2. Potential heat stress<br />

3. Construction equipment<br />

4. Uneven terrain


5. Unstable stacking of containers (inside building)<br />

6. Manual material handl ing<br />

7. Drum handl ing<br />

8. Drum overpacking operations<br />

9. Potential exposure to vinyl chloride<br />

4.4.1.1 Noise<br />

Where excessive noise was encountered, employees were provided with E.A.R.<br />

ear plugs.<br />

4.4.1.2 Heat Stress<br />

All on-site personnel were instructed in <strong>the</strong> symptoms of heat stress.<br />

Where site conditions warranted, <strong>the</strong> site Health and Safety Officer<br />

monitored for heat stress. Potable water was available on-site, and<br />

Gatorade was provided as needed.<br />

4.4.1.3 Construction Eouioment<br />

Trucks, excavation equipment, and drum handl ing equipment were issued at<br />

<strong>the</strong> site. On-site personnel were made aware of <strong>the</strong> presence of this<br />

equipment. All personnel operating such equipment were made aware of <strong>the</strong><br />

presence of o<strong>the</strong>r site personnel. Backup alarms and roll -over protection<br />

were used, as appropriate. The excavation area was examined by a utilities<br />

locator.<br />

Personnel operating construction equipment were experienced in <strong>the</strong><br />

operation of such equipment and continuous supervision was provided during<br />

<strong>the</strong> operation of that equipment.<br />

4.4.1.4 Uneven Terrain<br />

All open excavations and ground openings were protected from inadvertent<br />

entry. Any openings left open overnight were barricaded and covered to


prevent entry by off-site personnel. Security guards were provided during<br />

off-hours to prevent entry by off-si te personnel.<br />

4.4.1.5 Unstable Stackinq of Containers<br />

Drums were stacked inside <strong>the</strong> building. All employees were warned to<br />

approach <strong>the</strong>se areas with caution. No one was permitted to walk or climb<br />

on drums. Any obviously unstable drums were restacked or o<strong>the</strong>rwise moved<br />

to eliminate <strong>the</strong> potential of falling.<br />

4.4.1.6 Manual Material Handling<br />

Wherever possible, material handling was done mechanically. Fork1 ift<br />

trucks for drum handling were used on-site. Where manual handling was<br />

necessary, personnel were instructed in techniques of safe handling.<br />

4.4.1.7 Confined Soaces<br />

The drainage sump, sludge tank, dip tanks, and boiler tank were pumped<br />

and/or cleaned during site activities. Entry into sump, sludge tank, dip<br />

tanks, or boiler tank was required during cleaning. Confined space entry<br />

and monitoring procedures were implemented during <strong>the</strong>se activities, as<br />

described in Section 4.5.<br />

4.4.2 Chemical Hazards<br />

Chemical hazards were encountered during <strong>the</strong> excavation activities and in<br />

handling unknown materials found in containers on-site. The drum yard<br />

soils were considered to be contaminated to varying degrees. All personnel<br />

wore steel toed neoprene boots while working in <strong>the</strong> yard. Kneeling and/or<br />

sitting directly on <strong>the</strong> ground was prohibited. Special procedures,<br />

including air monitoring and upgrading of health and safety protection<br />

levels, were implemented during excavating, cleaning and drum hand1 ing<br />

activities.


4.5 Air Monitoring<br />

4.5.1 Air Monitorinq Durinq Liquid Removal Activities<br />

The air monitoring at Bay Area Drum consisted of organic vapor<br />

concentration determination using an organic vapor analyzer (OVA).<br />

Monitoring was done at <strong>the</strong> beginning of each work activity to evaluate<br />

potential exposure levels. The chemical constituents of <strong>the</strong> liquids to be<br />

removed had previously been identified as styrene, methylene chloride, and<br />

C3benzene.<br />

Styrene has a threshold limit value of 50 ppm for an eight-hour time<br />

weighted average. The threshold limit value for methylene chloride is<br />

being lowered to 50 ppm, and it is considered a suspect carcinogen.<br />

C3benzene has not had a threshold limit value established by <strong>the</strong> American<br />

Conference of Governmental Industrial Hygienists. None of <strong>the</strong>se compounds<br />

are readily absorbed through <strong>the</strong> skin.<br />

Work at <strong>the</strong> Bay Area Drum facility was initiated on August 20, 1987. The<br />

OVA was calibrated using zero hydrocarbon air and methane in air at 6.7<br />

ppm. The background readings obtained outside <strong>the</strong> fence and upwind of <strong>the</strong><br />

site indicated 3.6 ppm.<br />

The first activity, pumping <strong>the</strong> liquids from <strong>the</strong> open tank, was monitored.<br />

The personal protective equipment worn by <strong>the</strong> employees was Level C with<br />

full face Scott respirators, chemical-resistant gloves (inner and outer),<br />

polytyveks, and rubber boots. The OVA readings during this activity were<br />

as follows:<br />

Pum~inq Tank<br />

Outside plastic sheet 3.6<br />

Above drum 70<br />

Above tank 20


Later in <strong>the</strong> day <strong>the</strong> OVA was re-calibrated and background established at<br />

1.6 ppm. The next activity was <strong>the</strong> pumping of <strong>the</strong> sump. The same level of<br />

protection, previously noted, was utilized by <strong>the</strong> employees. The OVA<br />

readings during this activity were as follows:<br />

Pumoinq sum^<br />

Top of sump<br />

Above drum<br />

Concentration (om)<br />

The next activity to be monitored involved <strong>the</strong> shoveling of <strong>the</strong> sludge in<br />

<strong>the</strong> sump. Re-calibration of <strong>the</strong> OVA was not possible due to a low battery.<br />

All activity was stopped and postponed until <strong>the</strong> next day.<br />

On August 21, 1987, <strong>the</strong> work activity centered on <strong>the</strong> shoveling and steam<br />

cleaning of <strong>the</strong> sump. The level of protection utilized was Level C. The<br />

OVA was calibrated and <strong>the</strong> background level established at 2.5 ppm. All<br />

employees noted an odor through <strong>the</strong>ir respirator at <strong>the</strong> beginning of <strong>the</strong><br />

shoveling activity. Re-adjustment of <strong>the</strong> respirator face piece alleviated<br />

<strong>the</strong> problem. The OVA readings during <strong>the</strong> day were as follows:<br />

40<br />

3.0<br />

Shovelinq Sumo Concentration (porn1<br />

Top of sump 4.2<br />

Shovel ing to bucket 2 5<br />

Bucket transfer to drum 82<br />

Removing motor 11<br />

Sludge trap inside 70<br />

Steam Cleanins Sumo Concentration (oomr<br />

Inside trap 150<br />

Outside 40<br />

Due to <strong>the</strong> extremely high moisture content in <strong>the</strong> air during <strong>the</strong> steam<br />

cleaning operation, <strong>the</strong> OVA readings are not considered val id.


On August 24, 1987, <strong>the</strong> removal of <strong>the</strong> sludge from open tank was begun. A<br />

backhoe with a small bucket attachment was utilized to fill <strong>the</strong> drums. The<br />

OVA was calibrated and background was established at 2.0 ppm. The<br />

protection levels initially were set for <strong>the</strong> employee guiding <strong>the</strong> sludge<br />

from <strong>the</strong> backhoe bucket to <strong>the</strong> drums at Level B with an airline respirator,<br />

polytyveks, chemical-resistant gloves (inner and outer), and rubber boots.<br />

The o<strong>the</strong>r employees were at Level C with a full face respirator. The OVA<br />

readings during this activity were as follows:<br />

Cleaninq Tank Concentration (om)<br />

Above tank 4.2<br />

Above tank after breaking<br />

sludge crust 400<br />

Inside barrel berm-top of<br />

barrel 70-150<br />

Backhoe operator seat 4.2<br />

Outside barrel berm 5.0<br />

Following this evaluation, <strong>the</strong> protection levels for <strong>the</strong> backhoe operator,<br />

forklift operator, and <strong>the</strong> barrel steam cleaner were downgraded to a<br />

modified Level D with polytyveks, rubber boots, chemical -resi stant gloves<br />

(inner and outer), and a hardhat with faceshield. The employee guiding <strong>the</strong><br />

sludge from <strong>the</strong> backhoe bucket to <strong>the</strong> drums remained at Level B.<br />

Additional OVA readings were obtained throughout <strong>the</strong> day and <strong>the</strong> ranges<br />

obtained were as follows:<br />

Cleaninq Tank Concentration ( om1<br />

Above tank 400-500<br />

Inside barrel berm-top of<br />

barrel 50-150<br />

Outside berm 3-5<br />

On August 25, 1987, <strong>the</strong> work activity of cleaning <strong>the</strong> tank continued with<br />

<strong>the</strong> same protection levels as <strong>the</strong> previous day. The OVA readings were as<br />

follows:


Cleaninu Tank Concentration (om)<br />

Above tank<br />

Inside barrel berm - top<br />

of barrel<br />

Outside berm<br />

Backhoe<br />

Some final clean up in <strong>the</strong> sump area was also conducted. The employees<br />

wore Level C with a full face respirator for this activity. The OVA<br />

readings were as follows:<br />

Cl eanina Sumo Concentration (ooml<br />

Outside sump area<br />

Sump trap inside<br />

During <strong>the</strong> day, it became necessary for an employee to enter <strong>the</strong> open tank<br />

to shovel <strong>the</strong> residual sludge into <strong>the</strong> backhoe bucket. Confined Space<br />

Entry procedures were utilized for this activity. The employee entering<br />

<strong>the</strong> tank wore an airline respirator with an escape bottle, saranex suit,<br />

rubber boots, chemical-resistant gloves (inner and outer), and a safety<br />

harness with a safety line attached. A stand-by observer was equipped with<br />

a SCBA, saranex suit, rubber boots, and chemical-resistant gloves (inner<br />

and outer). The OVA was re-cal i brated and <strong>the</strong> background established at<br />

0.8 ppm. The OVA readings obtained were as follows:<br />

Tank Entry Concentration (o~rn)<br />

Above tank<br />

Outside berm<br />

Backhoe<br />

After lunch, cleaning inside <strong>the</strong> tank continued with <strong>the</strong> same level of<br />

protection as noted above. Upon completion of <strong>the</strong> sludge removal, <strong>the</strong><br />

inside of <strong>the</strong> tank was steam-cleaned. The OVA was re-calibrated and <strong>the</strong><br />

background established at 2.0 ppm. The OVA readings were as follows:


Tank Entry Concentration (oom)<br />

Above tank 200<br />

Outside perimeter of tank 5.0<br />

Backhoe 2.0<br />

Inside barrel berm - top of barrel 120<br />

Outside berm 2.0<br />

Above tank - after steam clean 5.0<br />

During <strong>the</strong> tank entry activities, two employees, Jeff Buhl and Scott<br />

Freiwald, experienced direct skin contact with <strong>the</strong> sludge material. A<br />

small area on <strong>the</strong>ir neck and jaw indicated contact. The sludge was washed<br />

off with water. Since <strong>the</strong> known constituents are not readily absorbed<br />

through <strong>the</strong> skin, this contact would not be considered a significant source<br />

of exposure.<br />

The final activities during <strong>the</strong> liquid removal phase of this project<br />

involved <strong>the</strong> pumping of <strong>the</strong> liquid from a trough inside <strong>the</strong> building and<br />

<strong>the</strong> draining of <strong>the</strong> water from <strong>the</strong> boiler tank. The OVA reading for both<br />

operations were at background 1 eve1 s.<br />

4.5.2 Air Monitorinq Durinq Soil Excavation Activities<br />

4.5.2.1 Summarv of Excavation Activities<br />

During <strong>the</strong> week of October 5, 1987, air monitoring was conducted at <strong>the</strong> Bay<br />

Area Drum site. The site activities during this time period included<br />

uncovering of buried drums, excavation of contaminated soi 1 s, and grading<br />

of site yard. Direct reading instrumentation, consisting of an Organic<br />

Vapor Analyzer (OVA) and Draeger tubes for vinyl chloride were utilized at<br />

various steps throughout <strong>the</strong> activities. In addition, integrated ambient<br />

air samples were obtained from <strong>the</strong> site perimeter. Personal exposure<br />

monitoring of employees was conducted based on <strong>the</strong>ir assigned job func-<br />

tions. The ambient and employee samples collected were full duration<br />

samples and <strong>the</strong> results are considered time weighted averages.


The integrated samples were analyzed by an independent laboratory which<br />

maintains certification by <strong>the</strong> American Industrial Hygiene Association, <strong>the</strong><br />

National Institute for Occupational Safety and Health, and <strong>the</strong> Environ-<br />

mental Protection Agency.<br />

The direct reading instrumentation indicated potential exposure to vinyl<br />

chloride monomer based on <strong>the</strong> Draeger tube length of stain. With this<br />

indication, personnel protective equipment was upgraded to minimize <strong>the</strong><br />

potential exposure. The Draeger tube method is subject to several<br />

interferences and is not considered as accurate as <strong>the</strong> integrated samples.<br />

The integrated samples were specific for determining airborne concentra-<br />

tions of vinyl chloride monomer, polychlorinated biphenyl, lead, and total<br />

dust. The analytical results indicated no detectable levels of vinyl<br />

chloride or polychlorinated biphenyl on any of <strong>the</strong> ambient or personal<br />

samples. One sample indicated a measurable concentration for lead. This<br />

sample was obtained along <strong>the</strong> sou<strong>the</strong>rn perimeter fence on <strong>the</strong> final day of<br />

3<br />

activity monitoring. The result reported was 0.004 mg/m . All <strong>the</strong> remain-<br />

ing samples submitted for lead analysis indicated no detectable levels.<br />

Several of <strong>the</strong> samples analyzed for total dust concentrations reported<br />

detectable concentrations. For those samples which did indicate total dust<br />

3 3<br />

concentration, <strong>the</strong> range was reported between 0.1 mg/m and 0.6 mg/m .<br />

The Occupational Safety and Health Administration (OSHA) has established<br />

Permissible Exposure Limits for occupational exposure to each of <strong>the</strong> in-<br />

tegrated sample analytes. In all instances <strong>the</strong> reported concentration<br />

levels were well below <strong>the</strong> permissi ble exposure 1 imits.<br />

4.5.2.2 Direct Readinq Instrumentation<br />

The direct reading instrumentation used during <strong>the</strong> excavation phase at Bay<br />

Area Drum consisted of an organic vapor analyzer (OVA) and Draeger tubes<br />

for vinyl chloride. The range for <strong>the</strong> vinyl chloride tubes was 0.5 parts<br />

per million (ppm) to 6 ppm with 10 pump strokes.


On Friday, October 2, 1987, old drums which were buried along <strong>the</strong> east side<br />

of <strong>the</strong> yard were uncovered. The OVA was calibrated using zero hydrocarbon<br />

air and methane at 6.7 ppm. Background level was established outside <strong>the</strong><br />

exclusion area and upwind of <strong>the</strong> site. Background level was 1.8 ppm. OVA<br />

reading and vinyl chloride tubes evaluated levels before and during <strong>the</strong><br />

removal of <strong>the</strong> buried drums.<br />

Above drums -<br />

prior to removal 1.8<br />

Above open drum 1.8<br />

East pit - after some drums<br />

removed and fresh soil<br />

uncovered 3.0<br />

Leaking drum 3.0<br />

East pit - after drums removed 3.0<br />

General yard 1.8<br />

Sump area 3.2<br />

OVA Vinyl Chloride<br />

Concentration (porn1 Concentration (oomr<br />

None detected<br />

None detected<br />

0.5<br />

None detected<br />

None detected<br />

N/A<br />

N/A<br />

During <strong>the</strong> drum removal activities <strong>the</strong> protection levels utilized were<br />

Level C, with full face Scott respiratory protection, chemical resistant<br />

gloves (inner and outer), rubber boots, hard hat, and polytyveks for <strong>the</strong><br />

employee in <strong>the</strong> pit hooking up <strong>the</strong> drums and <strong>the</strong> employee unhooking <strong>the</strong><br />

drums. The remaining personnel on site utilized Level D protection with<br />

boots, tyveks, gloves, and hard hats.<br />

On Monday, October 5, 1987, <strong>the</strong> activities centered around preparing for<br />

excavation and grading of <strong>the</strong> general yard area. No OVA or vinyl chloride<br />

Draeger tubes were used. All employees in <strong>the</strong> yard area wore Level D<br />

protection with boots, tyveks, gloves and hard hats. Dust suppression<br />

methods were employed during <strong>the</strong> grading activities.


On Tuesday, October 6, 1987, <strong>the</strong> excavation activities started. The OVA<br />

was calibrated using zero hydrocarbon air and methane at 6.7 ppm. Back-<br />

ground was established outside <strong>the</strong> exclusion area and upwind of <strong>the</strong> site.<br />

Background level was 1.0 ppm. During <strong>the</strong> majority of <strong>the</strong> day, <strong>the</strong> OVA did<br />

not register any significant levels above background in <strong>the</strong> area of excava-<br />

tion or <strong>the</strong> general yard. When <strong>the</strong> excavation started along <strong>the</strong> building<br />

foundation, <strong>the</strong> employee providing dust suppression to <strong>the</strong> excavation<br />

reported a strong odor. Excavation activities were stopped while OVA and<br />

Draeger tube readings could be obtained.<br />

OVA Vinyl Chloride<br />

Concentration Imml Concentration (~oml<br />

Foundation 2 5 6.0<br />

Top of excavation pit None detected None detected<br />

Based on <strong>the</strong> positive detector tube reading, it was determined that fur<strong>the</strong>r<br />

excavation would be continued with continuous reading being taken at <strong>the</strong><br />

top of <strong>the</strong> excavation pit near <strong>the</strong> backhoe operator. Due to <strong>the</strong> moist<br />

soil, it was determined that dust suppression during excavation would be<br />

discontinued. For <strong>the</strong> remainder of <strong>the</strong> day, <strong>the</strong> OVA reading at <strong>the</strong> top of<br />

<strong>the</strong> excavation pit did not indicate any sustained levels above <strong>the</strong><br />

background level of 1.0 ppm. Instantaneous levels up to 1.4 ppm were<br />

noted. The level of protection utilized was Level D with boots, tyveks,<br />

gloves, and hard hats.<br />

On Wednesday, October 7, 1987, <strong>the</strong> excavation activities continued. The<br />

OVA was calibrated using zero hydrocarbon air and methane at 6.7 ppm.<br />

Background was established outside <strong>the</strong> exclusion area and upwind of <strong>the</strong><br />

site. Background level was 1.5 ppm. Continuous OVA readings were taken at<br />

<strong>the</strong> top of <strong>the</strong> excavation pit. The initial protection level for <strong>the</strong> back-<br />

hoe operator was Level D with boots, tyveks, gloves, and hard hats. When<br />

<strong>the</strong> OVA registered sustained levels of 1 ppm above background, in this<br />

instance 2.5 ppm, a Draeger tube reading for vinyl chloride was taken. The


-<br />

.- -<br />

Draeger tube indicated a vinyl chloride level of 0.5 ppm at <strong>the</strong> top of <strong>the</strong><br />

excavation pit. The protection level for <strong>the</strong> backhoe operator was upgraded<br />

to Level B with boots, tyveks, gloves, hard hat and airline respirator.<br />

The remaining employees kept away from <strong>the</strong> excavation pit. The OVA was<br />

used to establish a line when <strong>the</strong> levels were reported at <strong>the</strong> background<br />

1 eve1 .<br />

A survey of <strong>the</strong> yard during grading indicated a sustained level of 4 ppm on<br />

<strong>the</strong> OVA. A Draeger tube for vinyl chloride indicated that no detectable<br />

vinyl chloride was in <strong>the</strong> grading area. The protection level for grading<br />

<strong>the</strong> yard remained at Level D with boots, tyveks, gloves, and hard hats.<br />

The truck loaded with excavated material was checked with <strong>the</strong> OVA. The<br />

level indicated 7.5 ppm. A vinyl chloride Draeger tube taken in <strong>the</strong> same<br />

area of <strong>the</strong> truck indicated 1 ppm.<br />

At <strong>the</strong> end of <strong>the</strong> day's activity, <strong>the</strong> OVA reading at <strong>the</strong> top of <strong>the</strong><br />

excavation was at background and a Draeger tube for vinyl chloride<br />

indicated no detectable level.<br />

On Thursday, October 8, 1987, <strong>the</strong> excavation activities continued. The OVA<br />

was calibrated using zero hydrocarbon air and methane at 6.7 ppm.<br />

Background was established outside <strong>the</strong> exclusion area and upwind of <strong>the</strong><br />

site. Background level was 2.3 ppm. Continuous OVA readings were taken at<br />

<strong>the</strong> top of <strong>the</strong> excavation pit. The initial protection level for <strong>the</strong><br />

backhoe operator was Level D with boots, tyveks, gloves, and hardhat. When<br />

<strong>the</strong> OVA registered sustained levels of 3.3 ppm, <strong>the</strong> protection level for<br />

<strong>the</strong> operator was upgraded to Level B with <strong>the</strong> addition of airline<br />

respiratory protection. The remaining employees were kept away from <strong>the</strong><br />

excavation pit by establishing a 1 ine where <strong>the</strong> OVA readings were at<br />

background level s.<br />

A survey of <strong>the</strong> yard identified one area where <strong>the</strong> OVA readings were at<br />

14.3 ppm. The vinyl chloride Draeger tube reported no detectable level.


The equipment operator and <strong>the</strong> employee providing dust suppression were<br />

required to upgrade <strong>the</strong>ir protection level to Level C with boots, gloves,<br />

tyveks, hard hat and a half-mask respirator with organic vapor cartridges<br />

and a dust pre-filter. The area was re-evaluated an hour later with <strong>the</strong><br />

OVA. The levels reported were 5.3 ppm. At this time, <strong>the</strong> employees<br />

working in this area were advised that <strong>the</strong> continued use of <strong>the</strong> respiratory<br />

protection was optional.<br />

At <strong>the</strong> end of <strong>the</strong> day's activity, <strong>the</strong> OVA reading at <strong>the</strong> top of <strong>the</strong><br />

excavation pit was at background levels.<br />

On Friday, October 9, 1987, <strong>the</strong> excavation activities were completed. The<br />

last part of <strong>the</strong> contaminated soil was stockpiled to await transportation.<br />

The stockpile was covered with plastic and backfill material. The OVA was<br />

calibrated using zero hydrocarbon air and methane at 6.7 ppm. Background<br />

was established outside <strong>the</strong> exclusion area and upwind of <strong>the</strong> site.<br />

Background level was 1.6 ppm. Readings taken surrounding <strong>the</strong> covered<br />

stockpile were reported at background levels. The level at <strong>the</strong> top of <strong>the</strong><br />

excavation pit was also at background.<br />

A series of soil samples were collected in <strong>the</strong> excavation pit. The<br />

protection level utilized during collection was Level B with boots, hard<br />

hat, chemical resistant gloves (inner and outer), tyveks, and airline<br />

respiratory protection.<br />

After <strong>the</strong> samples were collected, <strong>the</strong> excavation pit was backfilled with<br />

clean fill material.<br />

4.5.2.3 Intesrated Sam~le Collection and Analysis<br />

The sampling procedures utilized corresponded with specific National Insti -<br />

tute for Occupational Safety and Health (NIOSH) methods for collection.<br />

The pumps used to collect <strong>the</strong> samples were Gilian models. The pumps were<br />

calibrated prior to and after sample collection. Calibration methods were


ased on a primary standard of volumetric displacement using a buck<br />

calibrator with <strong>the</strong> appropriate sample media in <strong>the</strong> sample train. Each<br />

pump was fully charged prior to monitoring.<br />

The ambient sample stations were located along <strong>the</strong> temporary fence sur-<br />

rounding <strong>the</strong> site. The west fence station was approximately halfway be-<br />

tween <strong>the</strong> building and <strong>the</strong> end of <strong>the</strong> yard on Thomas Street. The sou<strong>the</strong>rn<br />

fence station was on <strong>the</strong> open gate panel on Hawes Street. The resident<br />

fence station was on <strong>the</strong> east side of <strong>the</strong> excavation area. All <strong>the</strong> fence<br />

stations had <strong>the</strong> pumps and sample media located approximately 4.5 feet off<br />

<strong>the</strong> ground. The predominant wind direction was from <strong>the</strong> northwest. The<br />

ambient temperatures ranged from 95'~ on Monday and Tuesday to 70' F during<br />

<strong>the</strong> latter part of <strong>the</strong> week.<br />

The employee samples were all collected from <strong>the</strong> breathing zone of <strong>the</strong><br />

individual wearing <strong>the</strong> monitoring equipment.<br />

The monitoring equipment was checked frequently throughout <strong>the</strong> sample<br />

period to ensure that an adequate flow rate was being maintained. The<br />

monitoring duration was for approximately seven hours or <strong>the</strong> duration of<br />

<strong>the</strong> activity. The sampling media was chilled prior to shipment to <strong>the</strong><br />

analytical laboratory. Field blanks for each sample media were submitted<br />

with <strong>the</strong> samples. Tables 3 and 4 indicate <strong>the</strong> sampling summaries for <strong>the</strong><br />

employee and ambient air monitoring.<br />

The analysis of <strong>the</strong> samples was conducted according to NIOSH methods speci-<br />

fic for constituent of interest. Tables 5 and 6 indicate <strong>the</strong> analytical<br />

results of <strong>the</strong> samples.<br />

4.6 Personal Protective Eaui~ment<br />

The minimum level of protection for exclusion area personnel included <strong>the</strong><br />

following:


1. Hardhat<br />

2. Calf length steel-toed neoprene boots<br />

3. Tyvek coveralls or PVC rainpants and safety glasses (for work<br />

where splash hazards and upper body skin contact were not expected<br />

to occur)<br />

During activities where upper body skin contact was a potential exposure<br />

mechanism, pol ycoated Tyvek coverall s were used, as appropriate, in place<br />

of <strong>the</strong> rainpants.<br />

Fur<strong>the</strong>r discussion of personal protective equipment during liquid removal<br />

and soil excavation activities is provided in Section 4.5.<br />

Eyewash bottles were maintained in <strong>the</strong> drum handling and support areas.<br />

The site first aid kit was located in <strong>the</strong> support area. Twenty pound ABC<br />

fire extinguishers were maintained in <strong>the</strong> drum handling area and in <strong>the</strong><br />

support area. Specific use of and changes in protection equipment were as<br />

required by <strong>the</strong> site Health and Safety Officer in consideration of site<br />

conditions and construction activities.<br />

4.7 Decontamination Procedures<br />

4.7.1 Personal Decontamination<br />

All disposable clothing was deposited in containers on-site for off-site<br />

disposal. Wash tubs with soap and water and rinse tubs were provided for<br />

decontamination of boots and outer gloves. Respirators were cleaned with<br />

sanitizing wipes unless gross contamination required submersion in a<br />

wash/rinse tub. All decontamination was performed in <strong>the</strong> area shown on<br />

Figure 3.<br />

Soap and water were provided for personnel to wash up with after work or if<br />

any skin contamination occurred during <strong>the</strong> work day.


4.7.2 Eauioment Decontamination<br />

All construction and drum handling equipment which had been in contact with<br />

contaminated materials was steam cleaned before leaving <strong>the</strong> site. Waste<br />

hauling trucks which became contaminated during loading were steam cleaned<br />

before leaving <strong>the</strong> site. Steam cleaning operations were performed by<br />

placing plastic in an area large enough to contain <strong>the</strong> equipment to be<br />

decontaminated. Steam cleaning water was allowed to flow onto contaminated<br />

areas to assist in dust suppression and to provide moisture for compaction.<br />

At no time was <strong>the</strong> steam cleaning water allowed to leave <strong>the</strong> site.<br />

Emergency berms were constructed, if required, to contain <strong>the</strong> water.<br />

4.8 General Site Health and Safetv and Work Rules<br />

No drinking, gambling, or illegal drugs were allowed on-site.<br />

Personal protective equipment was required in designated areas.<br />

Such equipment included, but was not limited to, respiratory<br />

protection, earplugs, hardhat, rainsuits, boots, gloves, and<br />

chemical goggles.<br />

Eating, drinking, smoking, and chewing gum or tobacco were allowed<br />

only in designated areas.<br />

Changes in work practice or work rules were implemented only after<br />

approval by <strong>the</strong> Project Manager and <strong>the</strong> site Health and Safety<br />

Officer.<br />

Construction equipment always had <strong>the</strong> right-of-way over regular<br />

vehicles.<br />

All employees entering <strong>the</strong> Exclusion Area completed <strong>the</strong> required<br />

decontamination procedure before leaving <strong>the</strong> Exclusion Area.<br />

41


7. All protective clothing worn inside <strong>the</strong> Exclusion Area was<br />

supplied. None of this equipment was permitted to leave <strong>the</strong> site<br />

until completion of <strong>the</strong> project.<br />

4.9 Traininq<br />

All on-site personnel had prior experience and training in compliance with<br />

29 CFR 1910.120.<br />

Project-specific training was provided before startup of on-site<br />

activities. This training included <strong>the</strong> following:<br />

site health and safety plan<br />

decontamination<br />

personnel protection levels<br />

chemical hazards<br />

medical monitoring<br />

air monitoring<br />

use and maintenance of personal protective equipment<br />

work zones<br />

site safety rules and conditions of employment<br />

10. emergency provisions<br />

11. buddy system<br />

On-site tailgate meetings on health and safety were held as appropriate.<br />

The site Health and Safety Officer conducted <strong>the</strong>se meetings.<br />

4.10 Medical Monitoring<br />

All on-site personnel participated in a medical monitoring program.<br />

Canonie staff or contractor personnel who are involved in <strong>the</strong> annual<br />

corporate medical program received a blood chemistry test and blood lead<br />

analysis before starting work at <strong>the</strong> site.


All on-site and trucking personnel hired specifically for <strong>the</strong> work at <strong>the</strong><br />

site received a pre-employment physical which included <strong>the</strong> following:<br />

medical history<br />

physical exam<br />

pulmonary function test<br />

EKG<br />

audiogram<br />

blood lead<br />

CBC with differential and platelets urinalysis with dipstick and<br />

microscopic morphology<br />

chest X-rays - P/A and lateral<br />

lumbar sacral X-rays - three views<br />

Post project exams were conducted at <strong>the</strong> discretion of <strong>the</strong> site Health and<br />

Safety Officer considering site conditions and exposures.<br />

4.11 Work Zone and Site Security<br />

4.11.1 Exclusion Area<br />

All of <strong>the</strong> drum yard and <strong>the</strong> excavation area were considered <strong>the</strong> exclusion<br />

area prior to cover placement. Access to this area was restricted to site<br />

personnel who had completed <strong>the</strong> training and medical exam requirements, and<br />

who were using appropriate protective equipment.<br />

Once <strong>the</strong> first layer of capping material had been applied to <strong>the</strong> drum yard,<br />

personal protective equipment was downgraded and exclusion areas revised,<br />

as appropriate.<br />

4.11.2 Decontamination Area<br />

The eastern area of <strong>the</strong> site as shown in Figure 3 was designated as <strong>the</strong><br />

decontamination or contamination reduction area. As personnel ei<strong>the</strong>r left


<strong>the</strong> drum yard or <strong>the</strong> site, <strong>the</strong>y passed through this area to <strong>the</strong> support<br />

area inside <strong>the</strong> building.<br />

4.11.3 Suo~ort Area<br />

The existing office and toilet facilities inside <strong>the</strong> building was used as a<br />

support area for <strong>the</strong> project.<br />

4.11.4 Site Security<br />

The perimeter of <strong>the</strong> site was surrounded by fencing with locked gates. The<br />

site was secured in this manner during <strong>the</strong> project. Security guards were<br />

used during implementation of <strong>the</strong> ERA until <strong>the</strong> HDPE liner and sand cover<br />

were placed.<br />

Daytime personnel access to <strong>the</strong> site was only through <strong>the</strong> personnel<br />

entrance shown on Figure 3. Equipment access was through <strong>the</strong> gate along<br />

Shafter Avenue. No personnel access was allowed through this gate except<br />

as required to deliver or operate equipment.<br />

4.12 Communitv Health and Safety<br />

The potential community hazards included <strong>the</strong> excavation of <strong>the</strong> residential<br />

backyards, airborne dust or organic vapors, <strong>the</strong> presence of construction<br />

equipment, and higher than normal truck traffic around <strong>the</strong> site.<br />

Temporary fencing was placed around <strong>the</strong> site during <strong>the</strong> ERA activities and<br />

will remain in place until final fencing has been installed. Any open<br />

excavation was fenced or barricaded to prevent entrance by off-site<br />

personnel. Warning tape or signs were posted to advise offsite personnel<br />

to stay out of <strong>the</strong> construction areas. Only authorized personnel were<br />

admitted onto <strong>the</strong> site.


Exposures to dust and/or organic vapors were minimized through wetting<br />

techniques, as appropriate. In addition, plastic sheeting was placed on<br />

temporary fencing in <strong>the</strong> residential yards to restrict migration of<br />

excavated materials. Residents were advised to keep windows and doors<br />

closed if <strong>the</strong>se openings face <strong>the</strong> excavation area.<br />

Air monitoring was conducted during several of <strong>the</strong> work activities as<br />

described in detail in Section 4.5.<br />

Truck traffic included del ivery and removal of construction materi a1 s,<br />

equipment and supplies, and trailers containing excavated materials and<br />

debris for off-site disposal. Vehicles were decontaminated before leaving<br />

ing <strong>the</strong> site, as necessary. Traffic control was not provided and was not<br />

considered necessary to prevent street congestion or traffic hazards to<br />

local residents or businesses. Site entrances were controlled to eliminate<br />

pedestrian traffic.<br />

45


TABLES


TXBLE I<br />

SUBCONTRACTOR LIST<br />

NAME REPRESENTATIVE PHONE<br />

West Coast Locators<br />

Nilex<br />

.AAA Fence<br />

Roscoe Moss<br />

American Soil Products<br />

Raisch Products<br />

Levine Metal<br />

Anchor Fence<br />

Wells Security Service<br />

Esquivel Grading<br />

and Paving<br />

Dolan Concrete<br />

Herzog & Associates<br />

Chemical Waste Management<br />

Frank Zamira<br />

James Cramer<br />

scott<br />

Dorothy<br />

Adam Dauls<br />

Bob Renna<br />

Gary<br />

Tony Chapman<br />

Donna Wells<br />

Jon Walsh<br />

Dan Blamer<br />

Wayne Oakley<br />

Keith Pushaw<br />

With Fencing Bob With<br />

NUMBER TASK RESPONSIBILITY<br />

Utility Location<br />

Geotextile & HDPE Lining<br />

Temporary Fence<br />

PUC Pipe<br />

Fine Soil., Fill, Sand, Topsoil<br />

Aggregate Base<br />

Boiler Tank Removal<br />

Chain Link Fence Installation<br />

Security Guard<br />

Asphalt Construction<br />

Concrete Construction<br />

Soil Testing<br />

Transportation and Disposal of<br />

Waste Materials<br />

Wood Fence Installation


OR4 INVOICE #445<br />

OISWSllL<br />

- - - - - - - - -- - - -<br />

MANIFEST No. DATE<br />

.--....----. .. . . -.-..---.<br />

87341403-51 :: 10/6/87<br />

87341404-51 :: 10/6/87<br />

87341405-51 :: 10/6/87<br />

87341406-51 : : 10/6/87<br />

87341407-51 :: 10/6/87<br />

87341408-51 :: 10/6/87<br />

TABLE 2<br />

SUMMRRY OF HAZRRWUS WASTE OISWSAL<br />

BAY ARE& DRUM<br />

10/87<br />

YRRDAGE : WEIGHT : PROFILE :DISPOSAL<br />

10/87 10/87 10/87 10/87<br />

TRANSPORT : DEMURRAGE: LINERS : TAX ::<br />

-<br />

BAY RREA DRUM 87-035.21<br />

EXTENTION<br />

CWM<br />

---------.<br />

3.133.43<br />

3,511.93<br />

3,490.90<br />

3,511.93<br />

3,448.84<br />

3,427.82<br />

3,469.87<br />

3,385.76<br />

3,133.43<br />

3.133.43


3W INVOICE Y446<br />

OISWSAL<br />

------.-----<br />

------------<br />

MANIETST No. :: DATE : YARDAGE<br />

. . .<br />

87080611-51 :: 9/29/87 : 20.00<br />

87080612-51 :: 9/29/87 : 20.00<br />

81080596-51 :: 1011187 : 20.00<br />

i3W4 INVOICE a473<br />

DISWSAL<br />

------------<br />

.<br />

TABLE 2 (CONTINUED)<br />

SUHMARY OF HAZAROOUS WASTE DISPOSAL<br />

BAY ARFA DRUM<br />

WEIGHT : PROFILE<br />

0 :ENR-G57146<br />

0 :m-G5714b<br />

13,080 :m-G51146<br />

19,300 :EMR-G57146<br />

8,760 :ERR-G5714b<br />

0 :W-G51146<br />

20,660 :FBI-G57146<br />

0 :Ern-G57146<br />

61800<br />

MANIFEST No. DATE : YARDAGE : WEIGHT : PROFILE<br />

.<br />

87341238-51 : : 10/27/87 : 15 : 0 :ENR-G98113<br />

87341239-51 :: 10/27/87 : 15 : 0 :ENR-G98713<br />

87440407-51 :: 10/27/87 : 15 : 0 :ENR-G98713<br />

87440408-51 :: 10/27/87 : 15 : 0 :ENR-G98713<br />

87341240-51 :: 10/29/87 : 15 : 0 :ENR-G98713<br />

87341241-51 :: l0/29/87 : 15 : 0 :ENR-G98713<br />

87341242-51 :: 10/29/87 : 15 : 0 :ENR-G98713<br />

87341243-51 :: 10129187 : 15 : 0 :Em-G98713<br />

10/87 10/87 10187<br />

:DISPOSAL : TRANSPORT : DEMURRAGE:<br />

:DISPOSAL : TRANSPORT : DEMURRAGE:<br />

.<br />

: 1,800.00 : 1.093.43 :<br />

: 1.800.00 : 1.093.43 :<br />

10/87<br />

LINERS :<br />

10/87<br />

TAX : :<br />

. . .<br />

240.00 ::<br />

240.00 ::<br />

240.00 ::<br />

192.00 ::<br />

240.00 ::<br />

240.00 ::<br />

240.00 ::<br />

240.00 ::<br />

. .<br />

. .<br />

.............<br />

1,872.00<br />

BAY RRWL DRUM 87-035.21<br />

EXTENTION<br />

LINERS : TAX : : CWM<br />

36,000.00 21,868.60 315.42 1,200.00 3,600.00 62,984.02<br />

Environmental


CWH INVOICE W515<br />

TABLE 2 (CONTINUED)<br />

SUMMARY OF HAZRRWUS WASTE DISPOSAL<br />

BAY AREA DRUH<br />

DISWSAL<br />

------------<br />

MANIFEST No. :: DATE : YARDAGE : WEIGHT : PROFILE<br />

.----------- . .<br />

10/87<br />

:DISPOSAL<br />

10187 10/87 10187<br />

: TRANSPORT : DEMURRAGE: LINERS :<br />

10/87<br />

TAX<br />

' EXTENTION<br />

:: cnn<br />

. .<br />

87341214-51 :: 11/24/87 : 15 : 0.00 :EN-G98713 : 1,800.00 : 1,093.43 : 84.11 : 60.00 : 180.00 :: 3,217.54<br />

.. ---------- . -----------<br />

. . . .<br />

. .<br />

. . 0.00<br />

. . 0.00<br />

---------~~~~~~~~~.....~~-~~~----------~--~~~<br />

1,800.00 1,093.43 84.11 60.00 180.00 3,217.54<br />

Environmental


Sample<br />

Number<br />

87035-25<br />

87035-26<br />

87035-27<br />

87035-28<br />

87035-41<br />

87035-42<br />

87035-43<br />

87035-56<br />

87035-57<br />

87035-58<br />

87035-59<br />

87035-60<br />

87035-61<br />

I I]<br />

Sample<br />

Enolovee Media<br />

TABLE 3<br />

EMPLOYEE A IR MONITORING COLLECTION SUMMARY<br />

Flow Rate Dvration<br />

Supervisor, Charcoal Tube 11934 47 cc/m 452 min.<br />

General Site Fluorsil Tube 200 cc/m<br />

Glass Fiber Filter 200 cc/m<br />

Laborer, Pre-Wei hted 17840 1.9l/m 443 min.<br />

Excavation Area MCEF ~iqter<br />

Equipment Charcoal Tube 5067-10 46 cc/m 429 min.<br />

Operator, Fluosil Tube 200 cc/m<br />

Grading Area Glass Fiber Filter 200 cc/m<br />

Equipment Charcoal Tube 5067-10 46 cc/m 434 min.<br />

Operator, Fluorsil Tube 200 cc/m<br />

Excavation Area Glass Fiber Filter 200 cc/m<br />

Equipment Charcoal Tube 5067-10 46 cc/m 434 min.<br />

Operator, Fluorsil Tube 200 cc/m<br />

Excavation Area Glass Fiber Filter 200 cc/m<br />

NIOSH<br />

Method Chemical<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

S262 Total Dust<br />

PlCAM173 Lead<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

I Environmental


TABLE 4<br />

AMBIENT AIR MONITORING COLLECTION SUMMARY<br />

NlOSH<br />

Flow Rate Duration Volume Method Chemical<br />

10/5 87035-01 West Fence Pre-Wei hted 17840 2.1 l/m 49 min. 1.0 M3 S262 Total Dust<br />

MCEF ~igter PLCAM173 Lead<br />

87035-02 Charcoal Tube 5 47 cc/m 480 min. 23 1 S25 Vinyl Chloride<br />

87035-03 Fluorsil Tube 200 cc/m 87 1 5503 PCB-vapor<br />

87034-04 Glass Fiber Filter 200 cc/m 87 1 5503 PCB-particulate<br />

10/5 87035-05 Resident Pre-Weighted 17839 2.1 1/m 479 min. 1.0 M~ 5262 Total Dust<br />

Fence MCEF filter PtCAM173 Lead<br />

87035-06 Charcoal Tube 11934 48 cc/m 480 min. 23 1 525 Vinyl Chloride<br />

87035-07 Fluorsil Tube 200 cc/m 94 1 5503 PCB-vapor<br />

87035-08 Glass Fiber Filter 200 cc/m 94 1 5503 PCB-particulate<br />

10/5 87035-09 Plating Shop Pre-Weighted 17841 2.2 1/m 480 min. 1.1 M3 5262 Total Dust<br />

MCEF filter PLCAM173 Lead<br />

87035-10 Charcoal Tube 11935 49 cc/m 440 min. 22 1 525 Vinyl Chloride<br />

87035-1 1 Fl uorsi 1 Tube 210 cc/m 92 1 5503 PCB-vapor<br />

87035-12 Glass Fiber Filter 210 cc/m 92 1 5503 PCB-particulate<br />

10/5 87035-13 Sou<strong>the</strong>rn Pre-Wei hted 17842 2.2 1/m 478 min. 1.0 M~ S262 Total Oust<br />

Fence MCEF fii'ter P&CAM173 Lead<br />

87035-14 Charcoal Tube 5067-10 49 cc/m 488 min. 24 1 S25 Vinyl Chloride<br />

87035-15 Fluorsil Tube 200 cc/m 98 1 5503 PCB-vapor<br />

87035-16 Glass Fiber Filter 200 cc/m 98 1 5503 PCB-particulate<br />

I Environmental


Sample<br />

e e f s E B r & & ?<br />

10/7 87035-33 Sou<strong>the</strong>rn<br />

Fence<br />

87035-34<br />

87035-35<br />

87035-36<br />

Sample<br />

TABLE 4<br />

AMBIENT AIR MONITORING COLLECTION SUMMARY<br />

(Continued)<br />

Pre-Uei hted 17841<br />

MCEF filter<br />

Charcoal Tube 11935<br />

Fluorsil Tube<br />

Glass Fiber Filter<br />

10/7 87035-37 West Fence Pre-Wei hted 17842<br />

MCEF fi7ter<br />

Charcoal Tube 11935<br />

Fluorsil Tube<br />

Glass Fiber Filter<br />

10/B 87035-14 West Fence Pre-Uei hted 17839<br />

MCEF filter<br />

Charcoal Tube 5<br />

Fluorsil Tube<br />

Glass Fiber Filter<br />

10/8 87035-48 Sou<strong>the</strong>rn<br />

Fence<br />

87035-49<br />

87035-50<br />

87035-51<br />

Pre-Wei hted 17839<br />

NCEF fiyter<br />

Charcoal Tube 11934<br />

Fluorsil Tube<br />

Glass Fiber Filter<br />

&p Flow Rate<br />

2.2 l/m<br />

Ouration<br />

393 min.<br />

392 min.<br />

438 min.<br />

442 min.<br />

425 min.<br />

428 min.<br />

418 min.<br />

421 min.<br />

NIOSH<br />

--<br />

Method Chemical<br />

S262 Total Dust<br />

PllCAM173 Lead<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

S262 Total Dust<br />

P&CAH173 Lead<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

5262 Total Dust<br />

PtCAM173 Lead<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

S262 Total Dust<br />

P&CAM173 Lead<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate


Sample<br />

t&!w<br />

87035-66<br />

87035-67<br />

87035-68<br />

87035-69<br />

87035-70<br />

87035-71<br />

87035-72<br />

87035-73<br />

87035-52<br />

87035-53<br />

87035-54<br />

87035-55<br />

87035-62<br />

87035-63<br />

87035-64<br />

87035-65<br />

fmIQw2<br />

Sou<strong>the</strong>rn<br />

Fence<br />

Sou<strong>the</strong>rn<br />

Fence<br />

Resident<br />

Fence<br />

Resident<br />

Fence<br />

Sample<br />

TABLE 4<br />

AMBIENT AIR MONlTORlNG COLLECTION SUMMARY<br />

(Continued)<br />

m<br />

Pre-Weighted 17840<br />

MCEF filter<br />

Charcoal Tube 11935<br />

Fluorsil Tube<br />

Glass Fiber Filter<br />

Pre-Wei hted 17842<br />

MCEF fi'i'ter<br />

Charcoal Tube 11934<br />

Fl uorsi 1 Tube<br />

Glass Fiber Filter<br />

Pre-Weighted 17841<br />

REF filter<br />

Charcoal Tube 11935<br />

Fluorsil Tube<br />

Glass Fiber Filter<br />

Pre-Weighted 17839<br />

MCEF filter<br />

Charcoal Tube 5<br />

Fluorsil Tube<br />

Glass Fiber Filter<br />

Flow Rate<br />

1.9 l/m<br />

46 cc/m<br />

200 cc/m<br />

200 cc/m<br />

2.1 l/m<br />

46 cc/m<br />

200 cc/m<br />

200 cc/m<br />

2.0 l/m<br />

46 cc/m<br />

200 cc/m<br />

200 cc/m<br />

2.1 l/m<br />

38 cc/m<br />

200 cc/m<br />

200 cc/m<br />

Duration<br />

429 min.<br />

428 min.<br />

425 min.<br />

429 min.<br />

416 min.<br />

417 min.<br />

455 min.<br />

460 min.<br />

SZ62 Total Dust<br />

PKAM173 Lead<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

S262 Total Dust<br />

PaCAM173 Lead<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

5262 Total Dust<br />

PKAM173 Lead<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

S262 Total Dust<br />

PaCAM173 Lead<br />

S25 Vinyl Chloride<br />

5503 PCB-vapor<br />

5503 PCB-particulate<br />

I Environmental


Sample Sample<br />

~~~~<br />

TABLE 4<br />

AMBIENT AIR MONlTORING COLLECTION SUMMARY<br />

(Continued)<br />

NIOSH<br />

Flow Rate Duration Volume Method Chemical<br />

10/6 87035-21 Resident Pre-Wei hted 17842 2.1 1/m 615 min. 1.3 M3 S262 Total Dust<br />

Fence MCEF filter P&CAH173 Lead<br />

87035-22 Charcoal Tube 5 39 cc/m 617 min. 24 1 S25 Vinyl Chloride<br />

87035-23 Fluorsil Tube 200 cc/m 125 1 5503 PCB-vapor<br />

87035-24 Glass Fiber filter 200 cc/m 125 1 5503 PCB-particulate<br />

10/7 87035-29 Resident Pre-Wei hted 17839 2.1 1/rn 394 min. 830 1 S262 Total Dust<br />

Fence HCEF fii'ter P&CAM173 Lead<br />

87035-30 Charcoal Tube 5 40 cc/m 397 rnin. 16 1 S25 Vinyl Chloride<br />

87035-31 Fluorsil Tube 200 cc/m 79 1 5503 PCB-vapor<br />

87035-32 Glass Fiber Filter 200 cc/m 79 1 5503 PCB-particulate


TABLE 6<br />

AMBIENT AIR MONlTORlNG ANALYTICAL RESULTS<br />

Date- K - PCB Lead fMs/m31<br />

10/5 Sou<strong>the</strong>rn Fence BDL BDL<br />

West Fence BDL BDL<br />

Resident Fence BDL BDL<br />

Plating Shop BDL BDL<br />

BDL<br />

BDL<br />

BDL<br />

BDL<br />

10/6 Resident Fence BDL BDL BDL<br />

10/7 Sou<strong>the</strong>rn Fence BDL BDL<br />

West Fence BDL BDL<br />

Resident Fence BDL BDL<br />

10/8 Sou<strong>the</strong>rn Fence BDL BDL<br />

West Fence BDL BDL<br />

Resident Fence BDL BDL<br />

10/9 Sou<strong>the</strong>rn Fence<br />

West Fence<br />

Resident Fence<br />

BDL BDL<br />

BDL BDL<br />

BDL BDL<br />

BDL<br />

BDL<br />

BDL<br />

BDL<br />

BDL<br />

BDL<br />

BDL<br />

BDL<br />

BDL<br />

Limit of Detection: 0.001 nq 0.05 ug tubes 0.002 mg<br />

0.3 ug-filters<br />

NIOSH Method: S25 5503 PllCAM173<br />

BDL: Below Detection Limit<br />

Total ~ust (ns/m3)<br />

0.2<br />

BDL<br />

0.3<br />

0.4<br />

BDL<br />

BDL<br />

BDL<br />

0.2<br />

BDL<br />

0.1<br />

0.2<br />

BDL<br />

BDL<br />

I<br />

I Environmental<br />

, ,~ .. .....m?.......... ~~.., ~~~ , ~~ ~.<br />

~. ... ,.... ..-~.


FIGURES


APPENDIX A<br />

Environmental


APPENDIX B<br />

Environmental


100 50 10 5<br />

GRAIN SlZE IN MILLIMETERS<br />

:OBBLES<br />

GRAVEL<br />

coARs, 1 FINE<br />

I SAND<br />

ICOARSE~ MEDIUM I FINE I SILT OR CLAY 1<br />

Symbol Sample Source I Classiflcatlon<br />

0<br />

%<br />

Felton Sand<br />

Sand 95.8 Light Brown Silty<br />

American Soils Products, Inc. % Silt 1.2 Clayey Sand (SP)<br />

% Clay 3.0<br />

Job No:<br />

DONALD 5674.3-0-8 PARTICLE SIZE ANALYSIS PLATE<br />

HERZGG Appr:<br />

& ASSEIATES. INC. 0G-o Canonie Engineers<br />

CEOTECH\IC+L C0'.51( T.\'.rS<br />

Aug. 1987<br />

1


(Common F ill) % Clay 24.5<br />

and 38.2 Light Brown Clayey<br />

% silt 37.3 Sandy S ilt (ML)<br />

Canonie Engineers


TEST MET OD: ASTM 0 1 57-70 (C)<br />

I 50 60<br />

MOISTURE CONTENT<br />

' ShMPLE DEPTH I CLASSIFICATION I SOURCE<br />

/ BULK A 0.00 '<br />

OONALO<br />

'iERZO[j<br />

ASSCCIFITES<br />

GEOTECHNICfiL CONSULTANTS<br />

LIGHT BROWN GRAVELLY SANO


' SAMPLE DEPTH I<br />

CLASSIFICATION<br />

20 38 48 50<br />

MOISTURE CONTENT (%I<br />

BULK B 0.88 LIGHT BROWN CLAYEY SILT(ML> COMMON FILL 118<br />

DONALD<br />

YERZCG<br />

ASSOCIATES<br />

GEOTECHNICAL CONSULTANTS<br />

Job No:<br />

5674.03.ee.8<br />

Date:<br />

w<br />

Septembar 1987<br />

COMPACTION TEST DATA<br />

BAY AREA DRUM<br />

Bay firma, California<br />

OPTIMIUM<br />

'IOISTURE (%)<br />

PLATE<br />

5


20 30 40 50<br />

MOISTURE CONTENT (%)<br />

MAXIMUM DRY OPTIMUM<br />

SAMPLE CLASSIFICATION SOURCE DENSITY f~cfl MOISTURE I%)<br />

DONALD<br />

HERZOG<br />

& ASSmIATES<br />

GEOTECHNICAL AND<br />

ENVIRONMENTAL CONSULTANTS<br />

Job No:<br />

Date:<br />

56'74.03.00.8<br />

November 1987<br />

COMPACTION TEST DATA<br />

CANONIE ENVIRONMENTAL<br />

Mountain View, California<br />

PLATE<br />

1


NUCLEw<br />

t<br />

RELATIVE<br />

COMPACTION<br />

PRoJECT NAME A RL-A DRUM TESTED BY G ~ t e h ) ~ ~<br />

PROJECT No A7 -03-r CALCULATED BY -J.&<br />

DATE CHECKED BY w ~uo(/i TEST DATA<br />

WET DENSITY<br />

(PCF) )24. 5 123.L 123 /<br />

YOIGTWIE<br />

COUNT<br />

STANMRD COUNT REMARKS :<br />

DOI$ITY I MOISTURE<br />

-.<br />

I<br />

-<br />

,~


PROJECT NAME 3.b 1'<br />

PROJECT No. 87 - n 7.7<br />

PGk, PW TESTED 8. Y A 'dl -<br />

DATE 1 I//() 1 Q J ~<br />

WBER OF<br />

PASSES<br />

-.<br />

LIFT<br />

THICKNESS<br />

DENSITY<br />

CWNT<br />

,. 7. .<br />

DRY DENSITY<br />

(PCF)<br />

CALCULATED BY ii /c l<br />

CHECKED BY A4 AX; 5,~ ct<br />

Y,P<br />

I IS: 0-<br />

sh<br />

/ 1-1<br />

/ci%<br />

90.2%<br />

I1 :<br />

. NUCLEkcc<br />

RELATIVE<br />

TEST DATA<br />

-<br />

"7


E-W COORD. /+s: 1<br />

ELEVATION 1 I I I<br />

.<br />

LIFT<br />

THICKNESS<br />

ENSITY<br />

MUNT 2 853- -, , .<br />

SrANDARD COUNT REMARKS :<br />

DDI8ITY I MOISTURE<br />

x-<br />

I<br />

I I<br />

- -<br />

. .<br />

I C<br />

NUCLEA,~<br />

RELATIVE<br />

COMPACTION<br />

TEST DATA<br />

J/' 4


PROJECT NAME TESTED BY ___.----<br />

PROJECT No. CALCULATED BY<br />

DATE CHECKED BY<br />

N-8 COORD.<br />

I<br />

i E-W COOAD.<br />

ELNATION<br />

YOOE DEPTH<br />

WET DENSITY<br />

IPCF)<br />

MOISTURE<br />

C U T<br />

I C (-1 9<br />

NUCLEkn<br />

I<br />

RELATIVE<br />

COMPACTION<br />

TEST DATA


APPENDIX C


I DATE<br />

PROJ. NO. PROJECr NAME<br />

L.P. NO. I SAMPLERS: Lipnafura)<br />

NO.<br />

-- UP<br />

I SAMPLE ID.<br />

CON<br />

TAINERS<br />

Relinquishad by: lsignatvrsl DatelTlme Recdned by: l~@nalural<br />

I<br />

12:~Flf<br />

Relinquished by: lslgnalure)<br />

I<br />

DatelTlms<br />

I<br />

Re~dved by: (Slg~lurs)<br />

I<br />

Relinquishsd by: ISipnslurd Daleilime Re~slved lor Laboratory by:<br />

(Sipnalure)<br />

Remarks<br />

Stockton, Ca. 95207<br />

Canary Aetu r TO snipper v~nk Lab Copy<br />

s !'


TO: R. Greenwood<br />

FROM: J. Buerger<br />

MEMO<br />

Bay Area Orum Compositinq<br />

e 4 3 O<br />

July 20, 1987<br />

The following table defines which of <strong>the</strong> 12 individual samples taken from Bay<br />

Area Orum were composited toge<strong>the</strong>r (according to compatibility). The table<br />

also includes a sample ID assigned to <strong>the</strong> composites as per <strong>the</strong> request of<br />

Keith Pushaw of Chem Waste Management. The composited samples were Federal<br />

Expressed out Friday July 17, 1987, to be delivered to Chem Waste Management<br />

on Saturday July 18. 1987.<br />

Associated charges for compositing and shipping w i l l be billed to Laboratory<br />

Project Number 87-0/5-2430. If <strong>the</strong>re are any questions please give me a call.<br />

JB/RR<br />

cc : J. Bartell<br />

K. Chirbas<br />

7


Bay Area Drum Compositing Scheme<br />

Assigned Individual<br />

Composite No. Sample ID Sample ID'S on<br />

Original Chain<br />

Custody<br />

1 ENRG 98713 Appletree<br />

Lead<br />

Sump Pit<br />

ENRG 98714 Cylinder Cut-off<br />

Trough<br />

Cement<br />

ENRG 98715 Barrel 1<br />

Barrel 2<br />

Barrel 3<br />

Union O i l<br />

ENRG 98716 Sump<br />

Boi 1 er


Laboratory Report for<br />

Mr. Rich Greenwood<br />

Canonie Environmental<br />

1825 S. Grant Street. Suite 260<br />

San Mateo. CA 94402<br />

August 4. 1987<br />

Canonie Environmental<br />

212 Frank West Circle. Suite A<br />

Stockton. CA 95206<br />

(209) 983-1340


Bay Area Drum<br />

87-035-2430<br />

Lab ID No Observations Sample ID<br />

Color: white<br />

Odor: strong paint<br />

Layers: single phased<br />

pH: 7.<br />

Semi-Sol i d<br />

Color: black<br />

Odor: strong hydrocarbons<br />

Layers: single phased<br />

pH: 10.<br />

Semi-Solid<br />

Color: whitelblack stripes<br />

Odor: strong paint<br />

Layers: black & white swirled<br />

pH: 7.<br />

Semi-Solid<br />

-<br />

(bi lavered)<br />

Color: honey<br />

Odor: strong motor oil<br />

Layers: single phased<br />

pH: 7.<br />

Liquid<br />

Color: beige<br />

Odor: strong rotten motor oil<br />

Layers: single phased<br />

pH:


Bay Area Drum<br />

87-035-2430<br />

Lab ID No Observations Sample ID<br />

Color: brown (fine,dry)<br />

Odor: none<br />

Layers: single phased<br />

pH: 6.<br />

Semi-Solid<br />

Appletree<br />

Brass Tube<br />

Color: dark brown/black (moist) Lead<br />

Odor: mild petroleum Brass Tube<br />

Layers: single phased<br />

pH: 6.<br />

Sol id<br />

Color: brown (fine, dry)<br />

Odor: none<br />

Layers: single phased<br />

pH: 6.<br />

Sol id<br />

Sump Pit<br />

Brass Tube<br />

Color: dark gray/white specks (paint) Cylinder Cut-off<br />

Odor: strong paint Mason Jar<br />

Layers: mostly solid. small amount<br />

liquid (bilayered)<br />

pH: 5.<br />

Moist Rubbery<br />

10% free liquid<br />

Color: rusty with purple & gray Trough<br />

pockets Mason Jar<br />

Odor: none<br />

Layers: single phased<br />

pH: 9.<br />

Solid (dry)<br />

Color: brown with green tint<br />

Odor: none<br />

Layers: single phased<br />

pH: 8.<br />

Solid. Moist<br />

Cement<br />

Mason Jar


. .<br />

Bay Area Drum<br />

87-035-2430<br />

Lab ID No Observations Sample I0<br />

Corposite of<br />

71 1382<br />

71 1383<br />

71 1384<br />

Corposite of<br />

71 1379<br />

71 1381<br />

Color: black<br />

Odor: strong petroleum<br />

Layers: single phased<br />

pH: 10.<br />

Semi-Sol i d<br />

Immiscible in water<br />

ENRG98715<br />

Mason Jar<br />

Color: dirty gray/orange ENRG98716<br />

Odor: we respect <strong>the</strong> potential Idason Jar<br />

hazards associated with <strong>the</strong><br />

inhalation of this composite<br />

Layers: single phased<br />

pH: 3.<br />

Liquid<br />

Miscible in water<br />

Produced off-gas upon compositing<br />

No noticeable heat generation


Client ID: BAY ARE?? DRUM Data Fi la:>1940V<br />

Sample ID: 87-035-2478 SAMPLE TOPSOIL 711940<br />

Matrix : SOIL<br />

COMPOUND NAME<br />

--_11-.--11----1---__II<br />

DICHLORODIFLUOROMETHANE<br />

CHLOROMETHANE<br />

BROMOMETHANE<br />

VINYL CHLORIDE<br />

CHLOROETHGNE<br />

METHYLENE CHLORIDE<br />

TRICHLOROFLUOROMETHANE<br />

1,l-DICHLOROETHENE<br />

Ill-DICHLOROETHANE<br />

TOTAL 1,2-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHRNE<br />

1,1,1-TRICHLOROETHANE<br />

CRRBON TETRACHLORIDE<br />

BROMODICHLOROMETHANE<br />

1,2-DICHLOROPROPANE<br />

TRANS-1,3-DICHLOROPROPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

DIBROflOCHLOROMETH~NE<br />

1,1,2-TRICHLOROETHANE<br />

CIS-1,3-OICHLOROPROPANE<br />

2-CHLOROETHYL VINYL ETHER<br />

BROMOFORM<br />

1,1,2,2-TETRKHLOROETHANE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,3-DICHLOROBENZENE<br />

1,2-DICHLOROBENZENE<br />

1,4-DICHLOROBEMZENE<br />

I;C/MS<br />

VOLATILE ANALYSIS<br />

AMOUNT<br />

P19111-I-l-<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

NO<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

KRECOUERY<br />

1.1111=----<br />

84.9<br />

93.8<br />

87.4<br />

DET, LIMIT<br />

.1.--====-<br />

629 ug/'kg<br />

1250 ug/kg<br />

1290 ug/kg<br />

1250 ug,'kg<br />

1250 ug/kg<br />

625 uglkq<br />

625 ugAg<br />

625 ugf'kg<br />

62hg/kg<br />

625 ug.'kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

62% ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/'kg<br />

625 ug/k.g<br />

625 ug/kg<br />

625 ug/lrg<br />

625 ug/kg<br />

625 ug/kg<br />

1250 ug/kg<br />

625 ugj'kg<br />

625 ugx'kg<br />

625 ugfkg<br />

625 ug/kg<br />

625 ,ug/kg<br />

,625 ug/kq<br />

625 ug/kg<br />

ii25 ug/kg<br />

625 ug/kg<br />

------------ ---me-----....<br />

Analyst Checked By<br />

03-lo-** THU 19:13:42 G 3 ** **** NO. 03<br />

~ -~<br />

~- ~<br />

\


C!ient ID: RAY AREA DRUM Data File:>194lU<br />

Sem~ la ID: 07-035-2478 SAMPLE COMMERFILL 711941<br />

Matrix : SOIL<br />

COMPOUND NAME<br />

1--1---1I----111---1111<br />

DICHLORODIFLUOROMETHANE<br />

CHLOROMETHANE<br />

BROMOMETHANE<br />

UINYL CHLORIDE<br />

CHLOROETHANE<br />

ETHYLENE CHLORIDE<br />

TRICHLOROFLUOROMETHANE<br />

1,l-DICHLOROETHENE<br />

Ill-DICHLOROETHANE<br />

TOTGL 1,2-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHAME<br />

1,1,1-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICHLOROMETHANE<br />

1,P-DICHLOROPROPANE<br />

TRANS-1,3-DICHLOROPROPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

DIBRONOCHLOROMETHANE<br />

1,1,2-TRICHLOROETHANE<br />

CIS-1,3-DICHLOROPROPANE<br />

2-CHLOROETHYL UIMYL ETHER<br />

BROMOFORM<br />

1,1,2,2-TETRACHLOROETHeNE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,3-DICHLOROBENZENE<br />

1,Z-DICHLOROBENZENE<br />

1,4-DICHLOROBENZENE<br />

GC/MS<br />

UOLAT I LE ANALYS 19<br />

AMOUNT<br />

IP-II-1I.D-<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

NW<br />

ND<br />

rm<br />

ND<br />

NO<br />

ND<br />

ND<br />

. ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

NO<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

1.10<br />

ND<br />

t.ID<br />

NP<br />

ND<br />

ND<br />

------------<br />

Analyst<br />

03-lo-** THU 19:12:48 G 3 ** ****<br />

DET. LIMIT<br />

I-I-=-3===<br />

625 ua/kg<br />

1250 ug/kg<br />

1250 ug/kg<br />

1250 ugj'kg<br />

1250 ug/kg<br />

625 ug./kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ugfkg<br />

625 ,ug/kg<br />

625 ug*kg<br />

625 ug/kg<br />

625 ug4.g<br />

625 ug/kg<br />

625 ug/'kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

1250 ug/kg<br />

625 ugfkg<br />

625 irgikg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

629 ug/kg<br />

------------<br />

Checked By


August 11. 1987<br />

Mr. Rich Greenwood<br />

Canonie Environmental<br />

1825 S. Grant Street, Suite 260<br />

San Mateo. CA 94402<br />

Dear Mr. Greenwood:<br />

Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />

Canonie Environmental Analytical Laboratory.<br />

Canonie Environmental SeMces Corp.<br />

212 Frank West Circle<br />

Suite A<br />

Stockton. Califomla 95206<br />

Unless o<strong>the</strong>rwise instructed by you samples will be returned or disposed of<br />

two weeks from <strong>the</strong> date of this letter.<br />

If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />

Very puly yours,<br />

Kenneth C. Wahl<br />

Manager of Laboratory Services<br />

Enclosure


Laboratory Report for<br />

Mr. Rich Greenwood<br />

Canonie Environmental<br />

1825 S. Grant Street. Suite 260<br />

San Mateo, CA 94402<br />

August 11, 1987<br />

Canonie Environmental<br />

212 Frank West Circle. Suite A<br />

Stockton, CA 95206<br />

(209) 983-1340


Sampler ID<br />

Analysis: Toxic Metals<br />

Table 1<br />

Codes of Samples Received<br />

From Bay Area Drum<br />

Project: 87-035<br />

Date Date<br />

Sampled Received Lab ID# Sample T ~ E<br />

Commerfi 11 bag 07-17-87 07-21-87 711943 Soi 1<br />

Topsoi 1 bag 07-17-87 07-21-87 711942 Soi 1<br />

08-10-1987<br />

87-035-2478<br />

Page 1<br />

Container<br />

Plastic bag<br />

Plastic bag


Sampler ID:<br />

Lab ID#:<br />

Analyte(s)<br />

Arsenic<br />

Antimony<br />

Bari um<br />

Beryllium<br />

Cadmi um<br />

Chromium<br />

Cobalt<br />

Copper<br />

Lead<br />

Mercury<br />

Molydbenum<br />

Nickel<br />

Selenium<br />

Silver<br />

Thal 1 i um<br />

Vanadium<br />

Zinc<br />

Table 2<br />

Results of Toxic Metals Analysis on Soil<br />

Samples Received From Bay Area Drum<br />

Results in mg/kg<br />

[Checked by<br />

Topsoi 1<br />

bag<br />

71 1942<br />

08-10-1987<br />

87-035-2478<br />

Page 2<br />

Note:<br />

ND X denotes none detected to a level of X.<br />

'VD X denotes none detected to a level of X due t In interfering peak. CarrorrieEnvironmental


Client ID: BAY AREA DRUM Data F~le:>1940U<br />

Sample ID: 87-035-2478 SAMPLE TOPSOIL 711940<br />

Matrlx : SOIL<br />

COMPOUND NAME<br />

.......................<br />

DICHLORODIFLUOROMETHANE<br />

CHLOROMETHANE<br />

BROMOMETHANE<br />

UINYL CHLORIDE<br />

CHLOROETHANE<br />

METHYLENE CHLORIDE<br />

TRICHLOROFLUOROMETHANE<br />

1,l-DICHLOROETHENE<br />

1,l-DICHLOROETHANE<br />

TOTAL 1,2-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHANE<br />

1,1,1-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICHLOROMETHANE<br />

1,2-DICHLOROPPOPANE<br />

TRANS-1,3-DICHLOROPROPENE<br />

TPICHLOPOETHENE<br />

BENZENE<br />

DIBRONOCHLORO~ETHANE<br />

1 ,1,2- TR I CHLOROETHANE<br />

CIS-1,3-DICHLOROPROPANE<br />

2-CHLOROETHYL VINYL ETHER<br />

BROMOFORM<br />

1,1,2,2-TETRACHLOROETHANE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,3-DICHLOROBENZENE<br />

1,2 -D I CHLOROBENZENE<br />

1,0-DI CHLOROBENZENE<br />

GC.'MS<br />

VOLATILE ANALYSIS<br />

AMOUNT<br />

-----------<br />

N D<br />

ND<br />

ND<br />

ND<br />

NCI<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

NU<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

NC<br />

ND<br />

ND<br />

ND<br />

ND<br />

DET. LIMIT<br />

----------<br />

----------<br />

625 ~ ~ / k g<br />

1250 ugjkg<br />

1250 ugx'kg<br />

1250 ugfkg<br />

1250 ug/kg<br />

625 ug4.g<br />

625 ug/kg<br />

625 ug.'ka<br />

625 ugfkg<br />

625 uq/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/kg<br />

625 ug/k.g<br />

625 ug/kg<br />

625 ug/kg<br />

625 ugikg<br />

625 ug4g<br />

625 ug/kg<br />

625 ug/kg<br />

625 uq/! g<br />

625 ug/kg<br />

1250 ug.,'kg<br />

625 ug.'kg<br />

625 ug/kg<br />

625 ug.'kg<br />

625 ug/kg<br />

625 ug&g<br />

625 ug/kg<br />

625 ug4q<br />

625 ug.'kg<br />

625 ug/kg<br />

Checked B<br />

" &honie~rwironrne&


Tlient ID: BAY AREA DRUM Data Flle:,1?41U<br />

Sarno le ID: 87-035-2478 SAMPLE COMMERFILL 711941<br />

Matrix : SOIL<br />

COMPOUND NAME<br />

.......................<br />

DICHLORODIFLUOROMETHANE<br />

CHLOROMETHANE<br />

BROROMETHANE<br />

VINYL CHLORIDE<br />

CHLOROETHANE<br />

METHYLENE CHLORIDE<br />

TRICHLOROFLUOROMETHANE<br />

. 1 ,1-D ICHLOROETHENE<br />

1,1-DICHLOROETHANE<br />

TOTAL 1,2-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLORUETHANE<br />

1,1,1-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMOOICHLOROMETHANE<br />

1,2-DICHLOROPROPANE<br />

TRANS-1,3-DICHLOROPPOPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

DIBROMOCHLOPOMETHANE<br />

1,1,2-TRICHLOROETHANE<br />

CIS-1,3-DICHLOROPROPANE<br />

2-CHLOROETHYL VINYL ETHER<br />

BROMOFORM<br />

1,1,2,2-TETRACHLOROETHQNE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,s-DICHLOROBENZENE<br />

1,2-DICHLOROBENZENE<br />

1,4-DICHLOROBENZENE<br />

D4-1,2-DICHLOROETHANE (SURF!)<br />

D8 - TOLUENE<br />

4-BROMOFLUOROBENZEl4E<br />

GUMS<br />

VOLATILE ANALYSIS<br />

AMOUNT<br />

-----------<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

tJC1<br />

DET.<br />

=====<br />

625<br />

1250<br />

125 0<br />

1250<br />

1250<br />

625<br />

625<br />

625<br />

625<br />

625<br />

625<br />

625<br />

625<br />

625<br />

625<br />

625<br />

625<br />

625<br />

025<br />

625<br />

625<br />

625<br />

1250<br />

625<br />

625<br />

625<br />

625<br />

625<br />

Ana 1 st Checked By<br />

bnonie~nvironrnental


Client ID: BAY RREA DRUM<br />

Sample ID: 87-035-2478 COMMERF I LL TUBE<br />

Matrix : SOIL<br />

COMPOUND NAME<br />

.......................<br />

N-Nitrosodimethylamine<br />

Pheno 1<br />

his(-2-Chloroethyl )E<strong>the</strong>r<br />

2-Ch loropheno 1<br />

1,3-Dichlorobenzene<br />

1,4-Dichlorobenzene<br />

1,2-Dichlorobenzene<br />

bis(2-chloroisopropy1)E<strong>the</strong>r<br />

N-Nitroso-Di-Propylamine<br />

Hexachloroethane<br />

Nitrobenzene<br />

fsophorone<br />

2-Ni t ropheno 1<br />

2,4-Dimethylphenol<br />

his(-2-Ch1oroethoxy)Methane<br />

2;4-Dichlorophenol<br />

1,2,4-Tr ich lorobenzene<br />

Naphthalene<br />

Hexachlorobutadiene<br />

4-Chloro-3-Methylphenol<br />

Hexachlorocyclopentadiene<br />

2,4,6-Trlch lorophenol<br />

2-Chloronaphthalene<br />

Dimethyl Phthalate<br />

Acenaphthylene<br />

2,6-Dlnitrotoluene<br />

Acenaph<strong>the</strong>ne<br />

2,4-Dinitrophenol<br />

4-Nitrophenol<br />

2,4-Dinitrotoluene<br />

Diethylphthalate<br />

4-Chlorophenyl-phenyle<strong>the</strong>r<br />

Fluorene<br />

Benzidine<br />

4,6-Dlnit ro-2-Methylphenol<br />

N-Nitrosodiphenylarn~ne<br />

4-Brornophenyl-phenyle<strong>the</strong>r<br />

Hexachlorobenzene<br />

Pentach lorophenol<br />

Phenanthrene<br />

Ant hracene<br />

Di-N-Butylphthalate<br />

Fluoran<strong>the</strong>ne<br />

GC/MS<br />

SEMI-UDLATILE ANALYSIS<br />

Data File:>B1941<br />

71 1941


BAY AREA DRUM<br />

711941 LP-2478<br />

PAGE 2<br />

Pyrene<br />

Butylbenzylphthalate<br />

3,3'-Dichlorobenzidine<br />

Benzo(a)Anthracene<br />

bis-(2-Ethylhexy1)Phthalate<br />

Chrysene<br />

Di-N-Octyl Phthalate<br />

Benzo(b)Fluoran<strong>the</strong>ne<br />

Benzo(k)Fluoran<strong>the</strong>ne<br />

Benzo(a )Pyrene<br />

Indeno(l,2,3-cd)Pyrene<br />

DibenzoCa ,h )Anthracene<br />

Benzo(g,h,i)Perylene<br />

Analyst Checked By


Tllent ID: BAY AREA DRUM<br />

Sarno le ID: 87-035-2478 TOPSOIL TUBE<br />

natr~x : SOIL<br />

L<br />

- COMPOQND NAME<br />

.......................<br />

N-Nitrosodirnethylarnine<br />

Pheno 1<br />

his(-2-Chloroethy1)E<strong>the</strong>r<br />

2-Chlorophenol<br />

1,3-Dichlorobenzene<br />

l,4-Dichlorobenzene<br />

1,2-Dichlorobenzene<br />

bis(2-chloroisopropy1)E<strong>the</strong>r<br />

N-Nitroso-Di-Propylarnlne<br />

Hexach lo roethane<br />

Nitrobenzene<br />

Isophorone<br />

2-Nitrophenol<br />

2,4-Dlrnethylphenol<br />

b is(-2-Ch1oroethoxy)Methane<br />

2,4-Dichlorophenol<br />

1,2,4-Tr ichlorobenzene<br />

Naphthalene<br />

Hexachlorobutadiene<br />

4-Ch loro-3-Methylphenol<br />

Hexachlorocyclopentadiene<br />

2,4,6-Tr~chlorophenol<br />

2-Chloronaphthalene<br />

Dirnethyl Phthalate<br />

Acenaphthylene<br />

2,6-Dinitrotoluene<br />

Acenaph<strong>the</strong>ne<br />

2,4-Dinitrophenol<br />

4-Ni t ropheno 1<br />

2,4-Dinitrotoluene<br />

D~ethylphthalate<br />

4-Chlorophenyl-phenyle<strong>the</strong>r<br />

Fluorene<br />

Benz id ine<br />

4,6-Dinitro-2-Methylphenol<br />

N-Nitrosodiphenylamine<br />

4-Brornophenyl-phenyle<strong>the</strong>r<br />

Hexach lorobenzene<br />

Pentachlorophenol<br />

Phenanthrene<br />

Anthracene<br />

Di-N-Butylphthalate<br />

Fluoran<strong>the</strong>ne<br />

GC/MS<br />

SEMI-VOLATILE ANALYSIS<br />

Data File:>B1940<br />

711840


ND<br />

~thalate -<br />

- ND<br />

obenz~dlne<br />

ND<br />

racene<br />

ND<br />

'xyl )Phthalate ND<br />

hthalate<br />

tn t hene<br />

lnt hene<br />

ie<br />

d)Pyrene<br />

thracene<br />

'erylene<br />

& &&+ /<br />

---- -_--__ --- ------<br />

Analyst Checked By


-<br />

Water<br />

Soi 1<br />

Reference Methods<br />

Volatile Organic Analysis<br />

Preparation Analysis<br />

x - EPA 5030<br />

ANALYST RGP<br />

1) Eisenberg. Don M. et al. "Guidelines for<br />

Addressing Fuel Leaks". California Regional<br />

Water Quality Control Board.<br />

Bay Region. Sept. 1985.<br />

San Francisco<br />

EPA 601<br />

-EPA - 602<br />

- EPA 624<br />

- EPA 8010<br />

- EPA 8020<br />

AEPA 8240<br />

Project # 87-035-2478<br />

Date fompieted 08-1 0-1 987<br />

- Guidelines for<br />

Addressing<br />

Fuel Leaks 1


Preparation<br />

Water - EPA 3510<br />

- EPA 3520<br />

- EPA 3540<br />

&PA 3150<br />

Reference Methods<br />

Semi-volatile Organics<br />

(BNA's)<br />

Analysis<br />

- EPA 625<br />

Project # 87-035-2478<br />

Date Completed m-in-1982<br />

ANALYST b


-<br />

Preparation:<br />

Reference Methods<br />

Metals<br />

Project # 87-035-2478<br />

Acid Digestion - EPA 3010<br />

- EPA 3020<br />

- EPA 3030<br />

Date Completed 08-10-1 987<br />

- EPA 3040<br />

J EPA 3050<br />

-<br />

Mercury Digestion - EPA 7470 Water<br />

-<br />

$/ EPA 7471 Soil<br />

Alkaline Digestion - EPA 3060<br />

EP Toxicity - EPA 1310<br />

CAM STLC - T itle 22 CAC<br />

ANALYST a??-


Reference Methods<br />

Metals<br />

Soi 1<br />

Atomic Absorption Metals Analysis<br />

Project # 87-035-2478<br />

Date Completed 08-10-1- ~.<br />

Graph~te Hydride Cold<br />

Element Flame Furnace Generation Vapor ICP<br />

- -<br />

A1 umi num<br />

Antimony<br />

Arsenic<br />

Barium<br />

Bery 11 ium<br />

Cadmi um<br />

Calcium<br />

Chromi urn (Total)<br />

Cobalt<br />

Copper<br />

Iron<br />

Lead<br />

Magnesium<br />

Manganese<br />

Mercury<br />

Molybdenum<br />

Nickel<br />

Potassiuii;<br />

Selenium<br />

Silver<br />

Sodium<br />

Strontium<br />

Thal 1 i urn<br />

Vanadi urn<br />

Zinc<br />

- EPA 7040<br />

- EPA 7080<br />

- EPA 7090<br />

- EPA 7130<br />

- EPA 7190<br />

- EPA 7210<br />

- EPA 7380<br />

- EPA 7420<br />

- EPA 7460<br />

- EPA 7520<br />

- EPA 7760<br />

EPA 7770<br />

- EPA 7840<br />

- EPA 7910<br />

- EPA 7950<br />

VEPA 7041<br />

>PA - 7060<br />

- EPA 7081<br />

- EPA 7091<br />

EPA 7131<br />

- EPA 7191<br />

- EPA 7211<br />

- EPA 7381<br />

- EPA 7421<br />

- EPA 7461<br />

- EPA 7521<br />

- iEPA 7740<br />

- EPA 7761<br />

,&PA 7841<br />

-EPA - 7911<br />

- EPA 7951<br />

- EPA 7061<br />

- EPA 7741<br />

- L


. . .~ tianary. netmrcmy-r~snipp~r<br />

SL(3NIVl<br />

vv<br />

'11'1 3ldWVS 31VO<br />

NO3<br />

30 IW"ls"BtS1 :SU3ldWVS 'ON 'd'l<br />

ON<br />

'-'. . - -?<br />

i 1<br />

Pl"k Lab copy<br />

.<br />

---


ILUTIDN -<br />

YORKER


I DATE ANAL: I t a m , - I


CLIENT: I. j v FIt-ee Drd!:<br />

PROJECT r: L-!-


LLIENT: hty R ~ E C P:.ur'.<br />

PROJECT *: E;7-G35-ATE .<br />

>ILUTION<br />

NORKER<br />

.A8 I.D.<br />

:lNAL<br />

-


Water<br />

Soi 1<br />

Reference Methods<br />

Grganochlorine Pesticides<br />

And PCB's<br />

Pre~aration Analysis<br />

- EPA 3510 - ~ E P A 608<br />

- *?A 3520 - EPA 625<br />

Date Completed 08-27-1987


.- -<br />

Water<br />

Soi 1<br />

Reference Methods<br />

Volatile Organic Analysis<br />

Preparation Analysis<br />

- EPA 601<br />

EPA 602<br />

~ E P 624 A<br />

- EPA 5030 - EPA 8010<br />

- EPA 8020<br />

- EPA 8240<br />

- Guidelines for<br />

Addressing<br />

Fuel Leaks 1<br />

ANALYST fi 6-4'<br />

.-<br />

1) Eisenberg. Don M. et al, "Guidelines for<br />

Addressing Fuel Leaks", California Regional<br />

Water Quality Control Board, San Francisco<br />

Bay Region, Sept. 1985.<br />

-


Water<br />

Soi 1<br />

Preparation<br />

- EPA 3510<br />

>PA 3520<br />

- EPA 3540<br />

EPA 3550<br />

Reference Methods<br />

Semi-volatile Organics<br />

(BNA's)<br />

Analysis<br />

- EPA 8270<br />

project # 87-035-03-2652<br />

Date Completed 08-37-1 9~<br />

ANALYST hq


Element<br />

A1 umi num<br />

Antimony<br />

Arsenic<br />

Barium<br />

Beryllium<br />

Cadmi um<br />

Cal ci um<br />

Chromium ( Total)<br />

Cobalt<br />

Copper<br />

Iron<br />

Lead<br />

Magnesi um<br />

Manganese<br />

Mercury<br />

Molybdenum<br />

Nickel<br />

Potassi um<br />

Selenium<br />

Silver<br />

Sod i urn<br />

Strontium<br />

Thal 1 ium<br />

Vanadi um<br />

Zinc<br />

Reference Methods<br />

Metals<br />

Water<br />

Atomic Absorption Metals Analysis<br />

Graphite Hydride<br />

- Flame Furnace Generation<br />

- EPA 202.1 EPA 202.2<br />

- EPA 204.1 TEPA - 204.2<br />

Cold<br />

Vapor<br />

&PA 206.2 EPA 206.3<br />

- -<br />

EPA 208.1 - EPA 208.2<br />

EPA 210.1 EPA 210.2<br />

-. A<br />

- EPA 213.1 - EPA 213.2<br />

- EPA 215.1<br />

- EPA 218.1 - EPA 218.2<br />

- EPA219.1 EPA219.2<br />

A EPA 220.1 - EPA 220.2<br />

- EPA 236.1 - EPA 236.2<br />

- EPA 239.1 - EPA 239.2<br />

- EPA 242.1<br />

- EPA 243.1 - EPA 243.2<br />

- EPA 246.1 - EPA 246.2<br />

EPA 249.1 EPA 249.2<br />

-EPA A 258.1 -<br />

JEPA 270.2 EPA 270.3<br />

- EPA 272.1 - -EPA 272.2 -<br />

- EPA 273.1<br />

- EPA 279.1 - JEPA 279.2<br />

- EPA 286.1 - EPA 286.2<br />

- EPA 289.1 - EPA 289.2<br />

ANALYST 98<br />

Project # 87-035-03-2652<br />

Date Completed 08-27-1987<br />

- JEPA 245.1<br />

- ICP<br />

- EPA 200.7<br />

- EPA 200.7<br />

- EPA 200.7<br />

- JEPA 200.7<br />

- /EPA 200.7<br />

- &PA 200.7<br />

- EPA 200.7<br />

- YEPA 200.7<br />

- /€PA 200.7<br />

- JEPA 200.7<br />

- EPA 200.7<br />

- r/EPA 200.7<br />

- EPA 200.7<br />

- EPA 200.7<br />

- JEPA 200.7<br />

- &PA 200.7<br />

- EPA 200.7<br />

- EPA 200.7<br />

- /EPA 200.7<br />

- EPA 200.7<br />

EPA 200.7<br />

~ E P A 200.7<br />

&PA 200.7


Sampler ID:<br />

Lab ID#:<br />

Anal yte(s)<br />

Arsenic<br />

Antimony<br />

Barium<br />

Beryllium<br />

Cadmium<br />

Chromium<br />

Cobalt<br />

Copper<br />

Lead<br />

Mercury<br />

Molybdenum<br />

Nickel<br />

Selenium<br />

Silver<br />

Thallium<br />

Vanadium<br />

Zinc<br />

Table 2<br />

Results of CAM Metals TTLC Analysis on Water<br />

Samples Received From Bay Area Drum<br />

Results in mg/l<br />

Boiler<br />

Tank<br />

71 4054<br />

08-27-1987<br />

87-035-03-2652<br />

Page 2<br />

Note:<br />

ND X denotes none detected to a level of X.<br />

ND X denotes none detected to a level of X due an interfering peak. @an~ouieEnvironrnental


Sampler ID:<br />

Lab ID#:<br />

I I<br />

Table 3<br />

Results of Organochlorine Pesticides Analysis on Water<br />

Samples Received From Bay Area Drum<br />

Results in ug/l<br />

Analyte(s)<br />

Aldrin<br />

Alpha BHC<br />

Beta-BHC<br />

Del ta-BHC<br />

Gamma-BHC<br />

Chlordane<br />

4.4'-DDD<br />

4,4'-DDE<br />

4,4'-DDT<br />

Dieldrin<br />

Endosulfan I<br />

Endosulfan I1<br />

Endosulfan Sulfate<br />

Endrin<br />

Endrin Aldehyde<br />

Heptachlor<br />

Heptachlor Epoxide<br />

Toxaphene<br />

PCB quantified as 1242<br />

PCB quantified as 1254<br />

PCB quantified as 1260<br />

T plr<br />

Analyst C ecked by<br />

Boi 1 er<br />

Tank<br />

714054<br />

08-27-1 987<br />

87-035-03-2652<br />

Page 3<br />

Note:<br />

ND X denotes none detected to a level of X.<br />

YD X denotes none detected to a level of X due t in interfering peak. Call~~~ieEnvironmental


Ciient ID: BAY WEA DRUM Data File:>4053U<br />

Samole ID: 87-035-03-2652 SAMPLE ST-1 714053<br />

Matrix : LIQUID<br />

COMPOUND NAME<br />

GC/MS<br />

VOLATILE ANALYSIS<br />

-I-*---------------____<br />

--I-------=<br />

DICHLORODIFLUOROMETHANE<br />

CHLOROMETHANE<br />

BROMOMETHANE<br />

VINYL CHLORIDE<br />

CHLOROETHANE<br />

METHYLENE CHLORIDE<br />

TRICHLOROFLUORONETHANE<br />

1,l-DICHLOROETHENE<br />

1 -1-D I CHLOROETHANE<br />

TOTAL 1, 2-D I CHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHANE<br />

1,1,1-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICHLDROMETHANE<br />

1,2-DICHLOROPROPANE<br />

TRANS-1,3-DICHLOROPROPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

DIBROMOCHLOROMETHANE<br />

1,1,2-TRICHLOROETHANE<br />

CIS-1,3-DICHLOROPROPANE<br />

2-CHLOROETHYL VINYL ETHER<br />

BROMOFORM<br />

1,1,2,2-TETRACHLORDETHANE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,3-DICHLOROBENZENE<br />

1 ,2-Dl CHLOROBENZENE<br />

1,4-DICHLOROBENZENE<br />

SURROGATE STANDARD<br />

-====-========m=======m-===<br />

D4-1,2-DICHLOROETHANE (SURR)<br />

DB-TOLUENE (SURR<br />

4-BROMOFLUOROBENZENE (SURR)<br />

AMOUNT<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

470.<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

2500.<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

DETECTION LIMIT RAISED DUE TO MATRIX INTERFERENCE<br />

DET. LIMIT<br />

----=----P<br />

250 ug/L<br />

500 ug/L<br />

500 ug/L<br />

500 ug/L<br />

500 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

500 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

Analyst Checked By<br />

CanonieErwironmenta1


Client ID: BAY AREA DRUM Data File:>4054U<br />

Sample ID: 87-035-03-2652 SAMPLE BOILER TANK 714054<br />

Matrix : LIQUID<br />

COMPOUND NAME<br />

DICHLORODIFLUOROHETHANE<br />

CHLOROMETHANE<br />

BROMOMETHANE<br />

VINYL CHLORIDE<br />

CHLOROETHANE<br />

METHYLENE CHLORIDE<br />

TRICHLOROFLUOROMETHANE<br />

1,l-DICHLOROETHENE<br />

1 ,1-D I CHLOROETHANE<br />

TOTAL 1,2-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHANE<br />

1,1,1-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICHLOROHETHANE<br />

1,2-DICHLOROPROPANE<br />

TRANS-1,3-DICHLOROPROPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

DIBROMOCHLOROMETHANE<br />

1,1,2-TRICHLOROETHANE<br />

CIS-1,3-DICHLOROPROPANE<br />

2-CHLOROETHYL VINYL ETHER<br />

BROMOFORN<br />

1,1,2,2-TETRACHLOROETHANE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,3-DICHLOROBENZENE<br />

1,2-DICHLOROBENZENE<br />

1,4-DICHLOROBENZENE<br />

SURROGATE STANDARD<br />

D4-1,2-DICHLOROETHANE (SURR)<br />

D8-TOLUENE ( SURR<br />

4- BROMOFLUOROBENZENE ( SUR~ )<br />

GC/MS<br />

VOLATILE ANALYSIS<br />

AMOUNT<br />

__-=m-__L--<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

1100.<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

DETECTION LIMIT RAISED DUE TO MATRIX INTERFERENCE<br />

DET. LIMIT<br />

----==----<br />

250 ug/L<br />

500 ug/L<br />

500 ug/L<br />

500 ug/L<br />

500 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

500 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 . ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

250 ug/L<br />

Analyst Checked By


Client ID: RAY AREA DPUU<br />

Sample ID: 87-035-2652 ST1<br />

Matrix : WATER<br />

COMPOUND NAME<br />

.......................<br />

Y-Nitrosodimethylamine<br />

Pheno 1<br />

his(-2-Chloroethyl )E<strong>the</strong>r<br />

2-Ch loropheno 1<br />

1,3-Dich lorobenzene<br />

1,4-Dich lorobenzene<br />

l,2-Dichlorobenzene<br />

bis(2-chloroisopropyl>E<strong>the</strong>r<br />

N-Nitroso-Di-Propylamine<br />

Hexachloroethane<br />

Nitrobenzene<br />

Isophorone<br />

2-Ni t ropheno 1<br />

2;4-Dimethylphenol<br />

his(-2-Ch1oroethoxy)Methane<br />

2:d-Dichlorophenol<br />

1,2,4-Trichlorobenzene<br />

Naphthalene<br />

Hexachlorobutadiene<br />

4-Chloro-3-Methylphenol<br />

Henachlorocyclopentadiene<br />

2:4;6-Trichloropheno1<br />

2-Chloronaphthalene<br />

Dimethyl Phthalate<br />

Acsnaphthylene<br />

2;6&Dinitrotoluene<br />

Acenaph<strong>the</strong>ne<br />

2,4-Dinitrophenol<br />

4-Nitrophenol<br />

2.4-Dinitrotoluene<br />

~ieth~lphthalate<br />

4-Chlorophenyl-phenyle<strong>the</strong>r<br />

Fluorene<br />

Benzidine<br />

4,6-Dinitro-2-Methylphenol<br />

N-Nitrosodiphenylamine<br />

4-Bromoohenyl-phenyle<strong>the</strong>r<br />

Hexachlorobenzene<br />

Pentachlorophenol<br />

Phenanthrene<br />

Anthracene<br />

Di-N-Butylphthalate<br />

Fluoran<strong>the</strong>ne<br />

GC/MS<br />

SEMI-VOLATILE ANALYSIS


BAY QREQ DRUM<br />

714053 LP-2652<br />

PAGE 2<br />

,Irene<br />

p ,-<br />

Butylbenzylphthalate<br />

3:3'-Dichlorobenzidine<br />

Benzo(a1Anthracene<br />

bis-(2-Ethylhexy1)Phthalate<br />

Chrysene<br />

Di-N-Octyl Phthalate<br />

Benzo(b1Fluoran<strong>the</strong>ne<br />

Benzo(k IFluoran<strong>the</strong>ne<br />

Benzo (a )Pyrene<br />

Indeno(l,2,3-cd)Pyrene<br />

Dibenzo(a,h)Anthracene<br />

Benzo(q:h:i)Perylene<br />

Analyst Checked Bu


Cl~ent ID: EQY APEA DRUM<br />

Sam@ le ID: 57-035-2652 BOILER TQYW<br />

Matr~x : UATEP<br />

COMPOUND NPYE<br />

.......................<br />

N-Ni t rosodimethylamine<br />

Pheno 1<br />

bisl-2-Chloroethy1)E<strong>the</strong>r<br />

2-Chlorophenol<br />

1 :3-Dich lorobenzene<br />

1,4-Dich lorobenzene<br />

1 ,2-Dichlorobenzene<br />

bis(2-chloroisopropyl>E<strong>the</strong>r<br />

N-Ni t roso-Di-Propylarnine<br />

Hexachloroethane<br />

Nitrobenzene<br />

Isophorone<br />

2-Nitrophenol<br />

2,4-Dimethylphenol<br />

his(-2-Ch1oroethoxy)Methane<br />

2,4-Dichlorophenol<br />

1,2,4-Trichlorobenzene<br />

Naphthalene<br />

Herachlorobutadiene<br />

4-Ch loro-3-Methylphenol<br />

Hexach lorocyc lopentadiene<br />

2,4,6-Trichlorophenol<br />

2-Chloronaphthalene<br />

Pirnethyl Phthalate<br />

Acenaphthulene<br />

2:6-Dinitrotoluene<br />

Acenaph<strong>the</strong>ne<br />

2,4-Dinitrophenol<br />

4-Ni t ropheno 1<br />

2,4-Dinitrotoluene<br />

Diethylphthalate<br />

4-Chlorophenyl-phenyle<strong>the</strong>r<br />

Fluorene<br />

Benzidine<br />

4,6-Dinitro-2-Methylphenol<br />

N-Ni t rosod ipheny larnine<br />

4-Bromopheny 1-phenyle<strong>the</strong>r<br />

Hexachlorobenzene<br />

Pentachlorophenol<br />

Phenant hrene<br />

Anthracene<br />

Di-N-Butylphthalate<br />

Fluoran<strong>the</strong>ne<br />

r;C/US<br />

SEMI-VOLATILE ANALYSIS<br />

Data File:>R4054<br />

714054


BAY AREA DRUM<br />

714054 LP-2652<br />

PAGE 2<br />

Py~rene<br />

Butylbenzylphthalate<br />

3:3'-Dichlorobenzidine<br />

Benzo(a!Anthracene<br />

bis-(2-Ethy1hexyl)Phthalate<br />

Chrysene<br />

Di-N-Octyl Phthalate<br />

Benzo(b )Fluoran<strong>the</strong>ne<br />

Renzo(k!Fluoran<strong>the</strong>ne<br />

Benzo (a )Pyrene<br />

Indeno


BAY ARER DRUM<br />

714054 LP-2652<br />

PAGE 2<br />

Pyrene<br />

Butylbenzylphthslate<br />

3,3'-Diehlorobenzld~ne<br />

Benzo(a)Anthrscene<br />

bis-(2-Ethylhexy1)Phthalate<br />

Chryaene<br />

bi-N-Octyl Phthalate<br />

Benzotb)Fluoran<strong>the</strong>ne<br />

Benzo(k)Fluoran<strong>the</strong>ne<br />

Benzo(s)Pyrene<br />

Indeno(l,2,3-cd)Pyrcnc<br />

Dibanzo(a,h)Anthrecens<br />

Benzo(g,h,i)Perylene


October 21, 1987<br />

- Environmental<br />

Ms. Irene Fanelli<br />

Canonie Environmental<br />

1825 S. Grant Street. Suite 260<br />

San Mateo. CA 94402<br />

Dear Ms. Fanelli:<br />

Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />

Canonie Environmental Analytical Laboratory.<br />

Canonw Enwronmental Se~ces Corp<br />

212 Frank West Clrcie<br />

Suite A<br />

Stockton. Caiifomia 95206<br />

Phone: 209-983-1340<br />

Unless o<strong>the</strong>rwise instructed by you samples will be returned or disposed of<br />

two weeks from <strong>the</strong> date of this letter.<br />

If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />

Very truly yours,<br />

Kenneth C. Wahl<br />

Manager of Laboratory Services<br />

Enclosure


Laboratory Report for<br />

Ms. Irene Fanelli<br />

Canonie Environmental<br />

1825 S. Grant Street, Suite 260<br />

San Mateo. CA 94402<br />

October 21, 1987<br />

Canonie Environmental<br />

212 Frank West Circle. Suite A<br />

Stockton, CA 95206<br />

(209) 983-1 340


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Sampler ID:<br />

Lab ID#:<br />

Analyte(s)<br />

Bromodichloromethane<br />

Bromof orm<br />

Bromomethane<br />

Carbon tetrachloride<br />

Chlorobenzene<br />

Chloroethane<br />

2-Chloroethylvinyl e<strong>the</strong>r<br />

Chloroform<br />

Chloromethane<br />

Dibromochloromethane<br />

1.2-Dichlorobenzene<br />

1.3-Dichlorobenzene<br />

1,4-Dichlorobenzene<br />

Dichlorodifluoromethane<br />

1.1-Dichloroethane<br />

1.2-Dichloroethane<br />

1,l-Dichloroe<strong>the</strong>ne<br />

trans-1.2-Dichloroe<strong>the</strong>ne<br />

1,2-Dichloropropane<br />

cis-1.3-Dichloropropene<br />

trans-1,3-Dichloropropene<br />

1.1.2.2-Tetrachloroethane<br />

Tetrachloroe<strong>the</strong>ne<br />

l.l,l-Trichloroethane<br />

1,1.2-Trichloroethane<br />

Trichloroe<strong>the</strong>ne<br />

Trichlorofluoromethane<br />

Vinyl chloride<br />

Methylene chloride<br />

51 mp<br />

AnBlyst Chec ed by<br />

Table 2<br />

Results of Purgeable Halocarbons Analysis on Soil<br />

Samples Received From Bay Area Drum<br />

Results in mg/kg<br />

10-20-1987<br />

87-035-2872<br />

Page 2


u<br />

-<br />

Water<br />

Soi 1<br />

Reference -Methods<br />

Volatile Organic Analysis<br />

Preparation Analysis<br />

ANALYST<br />

- 1) Eisenberg. Don M.. et al, "Guidelines for<br />

Addressing Fuel Leaks", California Regional<br />

Water Qua1 ity Control Board. San Francisco<br />

Bay Region, Sept. 1985.<br />

EPA 601<br />

-EPA - 602<br />

EPA 624<br />

- Guidelines for<br />

Addressing<br />

Fuel Leaks 1


ili3NlVl 0'1 3ldWVS 3110<br />

NO3<br />

do x 4117/ii/)2/<br />

I*ml."81Sl :Sli3ldWIS 'ON 'dl<br />

'ON


October 19, 1987<br />

Mr. Rich Greenwood<br />

Canonie Environmental<br />

1825 S. Grant Street, Suite 260<br />

San Mateo, CA 94402<br />

Dear Mr. Greenwood:<br />

Environmental<br />

Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />

Canonie Environmental Analytical Laboratory.<br />

Canonie Enviionmenta Sewices Cop.<br />

212 Frank West Circle<br />

Suite A<br />

Stockton, Caiiiomia 95206<br />

Unless o<strong>the</strong>rwise instructed by you samples w i l l be returned or disposed of<br />

two weeks from <strong>the</strong> date of this letter.<br />

If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />

Very truly yours,<br />

Kenneth C. Wahl<br />

Manager of Laboratory Services<br />

Enclosure


Laboratory Report for<br />

Mr. Rich Greenwood<br />

Canonie Environmental<br />

1825 S. Grant Street, Suite 260<br />

San Mateo, CA 94402<br />

October 19, 1987<br />

Canonie Environmental<br />

212 Frank West Circle, Suite A<br />

Stockton, CA 95206<br />

(209) 983-1340


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Sampler ID:<br />

- Andlyte(s)<br />

Bron~od ichloroniethane<br />

bromof or111<br />

Bru~~~ol~~ul.t~urle<br />

Curbun tetruchloride<br />

Chlorobenzene<br />

Chloroethane<br />

2-Chloroethylvinyl e<strong>the</strong>r<br />

Chlorof'orm<br />

Chlorosiethane<br />

Oi bron~ochlorornethane<br />

1,2-Dichlorobenzene<br />

1,3-Dichlorobenzene<br />

1.4-Oichlorobenzene<br />

Dichlorodif luoroo~ethane<br />

1,l-Oichloroethane<br />

1.2-Oichloroethane<br />

1.1-Oicliloroe<strong>the</strong>ne<br />

trans-'I. 2-Dichloroe<strong>the</strong>ne<br />

1,Z-Dichloropropane<br />

cis-1.3-Dichloropropene<br />

trans-1,3-Dichloropropene<br />

1.1.2.2-Tetrachloroethane<br />

Tetrachloroe<strong>the</strong>ne<br />

l.l,l-Trichloroethane<br />

1,1.2-Trichloroethane<br />

Trichloroe<strong>the</strong>ne<br />

Trichlurof luoron~ethane<br />

Vinyl chloride<br />

Methylene chloride<br />

Sj ma-<br />

AndI)-st Checked by<br />

Table 2<br />

Results of Purgeable Halocarbons Analysis on Soil<br />

Samples Received From Bay Area Drum<br />

Results in nlg/kg<br />

10-16-1987<br />

87-035-2865<br />

Page 2


u<br />

-<br />

Water<br />

Soi 1<br />

Reference Methods<br />

Volatile Organic Analysis<br />

Preparation Analysis<br />

EPA 601<br />

-EPA - 602<br />

- EPA 624<br />

- EPA 5030 $PA 8010<br />

- EPA 8020<br />

- EPA 8240<br />

ANALYST<br />

1) Eisenberg, Don M.. et al, "Guidelines for<br />

Addressing Fuel Leaks". California Regional<br />

- Water Quality Control Board. San Francisco<br />

Bay Region. Sept. 1985.<br />

5.p<br />

project # 87-035-2865<br />

Date Completeqo-16-1 q87<br />

- Guidelines for<br />

Addressing<br />

Fuel Leaks 1


Sampler ID:<br />

Lab ID#:<br />

Analyte(s)<br />

Antimony<br />

~rsenic-<br />

Bari urn<br />

Beryllium<br />

Cadmium<br />

Chromium<br />

Cobalt<br />

Copper<br />

Lead<br />

Mercury<br />

Molybdenum<br />

Nickel<br />

Selenium<br />

Silver<br />

Thallium<br />

Vanadium<br />

Zinc<br />

Table 2<br />

Results of Toxic Metals Analysis on Soil<br />

Samples Received From Bay Area Drum<br />

Results in mg/kg<br />

AG BASE PERM. SAND<br />

11-13-1987<br />

87-035-3020<br />

Page 2<br />

Note:<br />

ND X denotes none detected to a level of X.<br />

IN0 X denotes none detected to a level of X due to an interfering peak. Canonielh I!II.~ fl ilrxrlt


NOV 13 '87 15:40 CRNONIE, STOCKTON<br />

Client ID: BAY AREA DRUM<br />

Sample ID: 87-035-3020<br />

Matrix : SOIL<br />

Phenol<br />

bis(-2-Chloroethy1)E<strong>the</strong>r<br />

2-Chlorophenol<br />

1,3-Dicniorobenzene<br />

;,4-Dichiorobenzene<br />

1,2-Dichlorobenzene<br />

bis(2-chioroisopropy1)E<strong>the</strong>r<br />

N-Nitroso-Di-Propylamine<br />

Hexachloroethane<br />

Nitrobenzene<br />

Isophorone<br />

2-Nitrophenol<br />

2,4-Dimethylphenol<br />

bis(-2-Ch1oroethoxy)Methane<br />

2,4-Dichiorophenol<br />

1,2,4-Trichlorobenzene<br />

Naphthalene<br />

Hexachlorobutadiene<br />

4-Chioro-3-Methylphenol<br />

Hexachlorocyclopentadiene<br />

2,4,6-Trichlorophenol<br />

2-Chloronaphthalene<br />

Dimethyl Phthalate<br />

Acenaphthylene<br />

2,6-Dinitrotoluene<br />

Acenaph<strong>the</strong>ne<br />

2,4-Dinitrophenol<br />

4-Nitrophenol<br />

2,4-Dinitrotoluene<br />

Diethylphthalate<br />

4-Chlorophenyl-phenyle<strong>the</strong>r<br />

Fluorene<br />

Benzidine<br />

4.6-~initro-2-Methylphenol<br />

N-Nitrosodiphenylamine<br />

4-Bromophenyl-phenyle<strong>the</strong>r<br />

Hexachlorobenzene<br />

Pentachlorophenol<br />

Phenanthrene<br />

Anthracene<br />

Di-N-Butylphthalate<br />

Fluoran<strong>the</strong>ne<br />

AMOUNT<br />

===========<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

XD<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

Data ~ile:>B9153<br />

719153


BAY AREA DRUM<br />

719153 X87-035-3020<br />

PAGE 2<br />

Pyrexe<br />

Butylbenzylphthalate<br />

3,3'-Dichlorobenzidine<br />

L.<br />

- Benzo(a)Anthracene<br />

bis-(2-Ethy1hexyl)Phthalate<br />

Chrysene<br />

Di-N-Occyl Phthalaze<br />

bis-(2-Ethyihexy?)Phtkahte<br />

Chrysene<br />

Di-N-Octyl Phthalate<br />

Benzo(b)F:uorac<strong>the</strong>ce<br />

Benzo(k)Fluoran<strong>the</strong>ne<br />

Benzo(a)Pyrece<br />

Indeno(:,2,3-cd)Pyrene<br />

Dibenzo(a,h)Anthracene<br />

Benzo(g,h,i)Perylene<br />

Analyst Checked By


Client ID: BAY AREA DRUM<br />

Sample ID: 87-035-3020<br />

Matrix : SOIL<br />

COMPOUND NAME<br />

GC/MS<br />

SEMI-VOLATILE AANLYSIS<br />

.......................<br />

N-Nitrosodimethylamine<br />

Phenol -<br />

bis(-2-Chloroethy1)E<strong>the</strong>r<br />

2-Chlorophenol<br />

1,3-Dichiorobenzene<br />

1,4-Dichlorobenzene<br />

1,2-Dichlorobenzene<br />

bis(2-chloroisopropy1)E<strong>the</strong>r<br />

N-Nitroso-Di-Propylamine<br />

Hexachloroethane<br />

Nitrobenzene<br />

Isophorone<br />

2-Nitrophenol<br />

2,4-Dimethylphenol<br />

his(-2-Ch1oroethoxy)Methane<br />

2,4-Dichlorophenol<br />

1,2,4-Trichlorobenzene<br />

Naphthalene<br />

Hexachlorobctadiene<br />

4-Chloro-3-Methylphenol<br />

Hexachlorocyclopentadiene<br />

2,4,6-Trichlorophenol<br />

2-Chloronaphthaiene<br />

Dimethyl Phthalate<br />

- Acensphthylene<br />

2,6-Dinitrotoluene<br />

Acenaph<strong>the</strong>ne<br />

2,4-Dinitrophenol<br />

4-Nitrophenol<br />

2,4-Dinitrotoluene<br />

Diethylphthalate<br />

4-Chlorophenyl-phenyle<strong>the</strong>r<br />

Fluorene<br />

Benzidine<br />

4,6-Dinitro-2-Methylphenol<br />

N-Nitrosodiphenylamine<br />

4-Bromophenyl-phenyle<strong>the</strong>r<br />

Hexachlorobenzene<br />

Pentachlorophenol<br />

Phenanthrene<br />

Anthracene<br />

Di-N-Butylphthalate<br />

Fluoran<strong>the</strong>ne<br />

AMOUNT<br />

-----------<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

Data Filt:>R9152<br />

719152<br />

DET. LIMIT<br />

----------<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 uc/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 uq/kg<br />

660 ug/kg<br />

660 ug/kg<br />

3300 ug/kg<br />

3300 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

3300 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

3300 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg<br />

660 ug/kg


BAY AREA DRUM<br />

719152 W87-035-3020<br />

PAGE 2<br />

Pyrene<br />

Butylbenzylphthalate<br />

u 3,3'-Dichlorobenzidine<br />

- Benzo(a)Anthracene<br />

bis-(2-Ethylhexy1)Phthalate<br />

Chrysene<br />

Di-N-Octyl Phthalate<br />

bis-(2-Ezky1hexyi)Phthalate<br />

Chryse~e<br />

Di-N-Octyl Phthalate<br />

Benzo(b)Fluoran<strong>the</strong>ne<br />

Benzo(k)Fiuoran<strong>the</strong>ne<br />

Benzo(a)Pyrene<br />

Indeno(l,2,3-cd)Pyrene<br />

Dibenzo(a,h)Anthracene<br />

Benzo(g,h,i)Perylene<br />

Analyst Checked By


Client ID: BAY AREA DRUM<br />

Sample ID: 87-035-3020<br />

Matrix : SOIL SAMPLE: AG BASE<br />

COMPOUND NAME<br />

.......................<br />

DICHLORODIFLUOROMETHANE<br />

L<br />

- CHLOROMETHANE<br />

BROMOMETHANE<br />

VINYL CHLORIDE<br />

CHLOROETHANE<br />

METHYLENE CHLORIDE<br />

TRICHSOROFLUOROMETHANE<br />

1,i-DICHLOROETHENE<br />

1,l-DICHLOROETHANE<br />

TOTAL 112-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICHLOROMFTHANE<br />

TRANS- 1,3-DICHLOROPROPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

DIBROMOCHLOROKETHANE<br />

1,1,2-TRICHLOROEISANE<br />

CIS-1,3-DICHLORO?ROPAXE<br />

2-CHLOROE'THYL VINYL ETHER<br />

- BROMOFOFX<br />

l,i,2,2-TETFSCHLO3OET:iANE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,3-DICHLOROBENZENE<br />

1,2-DICHLOROBENZENE<br />

114-DICHLOROBENZENE<br />

TOTAL XYLENE<br />

2-PROPANONE (ACETONE)<br />

GC/MS<br />

VOLATILE ANALYSIS<br />

Data File:>9152V<br />

719152<br />

Checked By


Client ID: BAY AREA DRUM<br />

Sample ID: 87-035-3020<br />

Matrix : SOIL SAMPLE-: PER. SAND<br />

COMPOUND N WE<br />

.......................<br />

DICHLORODIFL,OROMETHANE<br />

.- - CHLOROMETHANS<br />

BROMOMETHWE<br />

VINYL CHLORIIE<br />

CHLOilOETHAtiF<br />

METHYLENE CELORIDE<br />

TRICELOROFKOXOMETHANE<br />

1,l-DICHLOROETHENE<br />

1,l-DICHLOROETHANE<br />

TOTAL 1,2-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHANE<br />

1,1,1-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICfiLOROMETHANE<br />

1,2-DICHLOR07ROPAKE<br />

TRAhS-1,3-DICHLOROPROPENE<br />

TRICELOROETEENE<br />

BENZENE<br />

DIBROMOCHLOROMETHANE<br />

1,1,2-TRICHLOXOETHANE<br />

CIS-Ij3-DICEIOROPROPANE<br />

2-CHLOROETEYL VINYL ETHER<br />

- BROXOFORM<br />

1,1,2,2-TEl.7-.CHLOROETEANE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

TOTAL XYLENE<br />

2-PROPANONE (ACETONE)<br />

GC/MS<br />

VOLATILE ANALYSTS<br />

AMOUNT<br />

-----------<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

N3<br />

ND<br />

ND<br />

ND<br />

ND<br />

Nrl<br />

N3<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

Data File:>9153V<br />

719153<br />

DE?. LIMIT<br />

----------<br />

125 ug/kg<br />

250 ug/kg<br />

250 ug/kg<br />

250 ug/kg<br />

258 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

250 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

i25 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

Checked By


November 14. 1987<br />

Mr. Kurt Ah1 ich<br />

Canonie Environmental<br />

1825 S. Grant Street, Suite 260<br />

San Mateo, CA 94402<br />

Dear Mr. Ahlich:<br />

Environmental<br />

Canonie Environmental Services COP<br />

212 Frank West Circle<br />

Suite A<br />

Stockton. California 95206<br />

Phone: 209.983-1340<br />

87-035-3020<br />

Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />

Canonie Environmental Analytical Laboratory.<br />

Unless o<strong>the</strong>rwise instructed by you samples will be returned or disposed of<br />

two weeks from <strong>the</strong> date of this letter.<br />

If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />

Very truly yours,<br />

Kenneth C. Wahl<br />

Manager of Laboratory Services<br />

Enclosure


Laboratory Report for<br />

Mr. Kurt Ahlich<br />

Canonie Environmental<br />

1825 S. Grant Street, Suite 260<br />

San Mateo, CA 94402<br />

November 14. 1987<br />

Canonie Environmental<br />

212 Frank West Circle, Suite A<br />

Stockton, CA 95206<br />

(209) 983-1 340


Sampler - ID<br />

Analysis: Toxic Metals<br />

Table 1<br />

Codes of Samples Received<br />

From Bay Area Drum<br />

Project: 87-035<br />

Date Date<br />

Sampled Received Lab ID# Sample Type<br />

AG BASE 11-04-87 11-06-87 7191 52 Soi 1<br />

PERM. SAND 11-04-87 11-06-87 719153 Soi 1<br />

11-13-1~87<br />

87-035-3020<br />

Page 1<br />

Container<br />

Mason Jar<br />

Mason Jar


PROJ. NO. I PROJECI NAME<br />

p-0~~3 -)jA)' A-pGn<br />

L.P. NO. SAMPLERS: ISlgnalur4<br />

DATE I SAMPLE 1.0<br />

j3P d w<br />

Recslvsd lor Laboratoq by:<br />

ISIgn.tur.)<br />

NO.<br />

CON^<br />

TAINERS<br />

Zanonle Environmental, 212 Frank West Circle, Sulte A, Stockton, CA 95206


Sampler ID:<br />

Lab ID#:<br />

Analyte(s)<br />

Antimony<br />

Arsenic<br />

Bari um<br />

Beryllium<br />

Cadmi um<br />

Chromium<br />

Cobalt<br />

Copper<br />

Lead<br />

Mercury<br />

Molybdenum<br />

Nickel<br />

Selenium<br />

Silver<br />

Thal 1 i urn<br />

Vanadium<br />

Zinc<br />

able 2<br />

Results of Toxic Metals Analysis on Soil<br />

Samples Received From Bay Area Drum<br />

Results in mg/kg<br />

AG BASE PERM. SAND<br />

11-13-1~d7<br />

87-035-3020<br />

Page 2<br />

Note:<br />

ND X denotes none detected to a level of X.<br />

#ND X denotes none detected to a level of X due to an interfering peak. CanonieEnvi ronmenbl


Client ID: BAY AREA DRUM<br />

Sample ID: 87-035-3020<br />

Matrix : SOIL<br />

COMPOUND NAME<br />

.......................<br />

N-Nitrosodimethylamine<br />

Phenol<br />

bis(-2-Chloroethy1)E<strong>the</strong>r<br />

2-Chlorophenol<br />

1,3-Dichlorobenzene<br />

1,4-Dichlorobenzene<br />

1,2-Dichlorobenzene<br />

bis(2-chloroisopropy1)E<strong>the</strong>r<br />

N-Nitroso-Di-Propylamine<br />

Hexachloroethane<br />

Nitrobenzene<br />

Isophorone<br />

2-Nitrophenol<br />

2,4-Dimethylphenol<br />

bis(-2-Ch1oroethoxy)Methane<br />

2,4-Dichlorophenol<br />

1,2,4-Trichlorobenzene<br />

Naphthalene<br />

Hexachlorobutadiene<br />

4-Chloro-3-Methylphenol<br />

Hexachlorocyclopentadiene<br />

2,4,6-Trichlorophenol<br />

2-Chloronaphthalene<br />

Dimethyl Phthalate<br />

Acenaphthylene<br />

2,6-Dinitrotoluene<br />

Acenaph<strong>the</strong>ne<br />

2,4-Dinitrophenol<br />

4-Nitrophenol<br />

2,4-Dinitrotoluene<br />

Diethylphthalate<br />

4-Chlorophenyl-phenyle<strong>the</strong>r<br />

Fluorene<br />

Benzidine<br />

4,6-Dinitro-2-Methylphenol<br />

N-Nitrosodiphenylamine<br />

4-Bromophenyl-phenyle<strong>the</strong>r<br />

Hexachlorobenzene<br />

Pentachlorophenol<br />

Phenanthrene<br />

Anthracene<br />

Di-N-Butylphthalate<br />

Fluoran<strong>the</strong>ne<br />

GC/MS<br />

SEMI-VOLATILE ANALYSIS<br />

AMOUNT<br />

-----------<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

Data File:>B9153<br />

719153<br />

DET. LIMIT<br />

----------<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

1650 ug/kg<br />

1650 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

1650 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

1650 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg<br />

330 ug/kg


BAY AREA DRUM<br />

719153 #87-035-3020<br />

PAGE 2<br />

Pyrene<br />

Butylbenzylphthalate<br />

3,3'-Dichlorobenzidine<br />

Benzo(a)Anthracene<br />

bis-(2-Ethylhexy1)Phth<br />

Chrysene<br />

Di-N-Octyl Phthalate<br />

ate<br />

bis-(~-~th~lhex~l)~hthalate<br />

Chrysene<br />

Di-N-Octyl Phthalate<br />

Benzo(b)Fluoran<strong>the</strong>ne<br />

Benzo(k)Fluoran<strong>the</strong>ne<br />

Benzo(a)Pyrene<br />

Indeno(l,2,3-cd)Pyrene<br />

Dibenzo(a,h)Anthracene<br />

Benzo(g,h,i)Perylene<br />

Checked By


Client ID: BAY AREA DRUM<br />

Sample ID: 87-035-3020<br />

Matrix : SOIL<br />

COMPOUND NAME<br />

.......................<br />

N-Nitrosodimethylamine<br />

Phenol<br />

bis(-2-Chloroethy1)E<strong>the</strong>r<br />

2-Chlorophenol<br />

1,3-Dichlorobenzene<br />

1,4-Dichlorobenzene<br />

1,2-Dichlorobenzene<br />

bis(2-chloroisopropy1)E<strong>the</strong>r<br />

N-Nitroso-Di-Propylamine<br />

Hexachloroethane<br />

Nitrobenzene<br />

Isophorone<br />

2-Nitrophenol<br />

2,4-Dimethylphenol<br />

bis(-2-Ch1oroethoxy)Methane<br />

2,4-Dichlorophenol<br />

1,2,4-Trichlorobenzene<br />

Naphthalene<br />

Hexachlorobutadiene<br />

4-Chloro-3-Methylphenol<br />

Hexachlorocyclopentadiene<br />

2,4,6-Trichlorophenol<br />

2-Chloronaphthalene<br />

Dimethyl Phthalate<br />

Acenaphthylene<br />

2,6-Dinitrotoluene<br />

Acenaph<strong>the</strong>ne<br />

2,4-Dinitrophenol<br />

4-Nitrophenol<br />

2,4-Dinitrotoluene<br />

Diethylphthalate<br />

4-Chlorophenyl-phenyle<strong>the</strong>r<br />

Fluorene<br />

Benzidine<br />

4,6-Dinitro-2-Methylphenol<br />

N-Nitrosodiphenylamine<br />

4-Bromophenyl-phenyle<strong>the</strong>r<br />

Hexachlorobenzene<br />

Pentachlorophenol<br />

Phenanthrene<br />

Anthracene<br />

Di-N-Butylphthalate<br />

Fluoran<strong>the</strong>ne<br />

GC/MS<br />

SEMI-VOLATILE ANALYSIS<br />

Data File:>R9152<br />

719152<br />

DET. LIMIT<br />

----------


BAY AREA DRUM<br />

719152 #87-035-3020<br />

PAGE 2<br />

Pyrene<br />

Butylbenzylphthalate<br />

3,3'-Dichlorobenzidine<br />

Benzo(a)Anthracene<br />

bis-(2-Ethylhexy1)Phthalate<br />

Chrysene<br />

Di-N-Octyl Phthalate<br />

bis-(2-Ethylhexy1)Phthalate<br />

Chrysene<br />

Di-N-Octyl Phthalate<br />

Benzo(b)Fluoran<strong>the</strong>ne<br />

Benzo(k)Fluoran<strong>the</strong>ne<br />

Benzo(a)Pyrene<br />

Indeno(l,2,3-cd)Pyrene<br />

Dibenzo(a,h)Anthracene<br />

Benzo(g,h,i)Perylene<br />

Checked By


Client ID: BAY AREA DRUM<br />

Sample ID: 87-035-3020<br />

Matrix : SOIL SAMPLE: PER. SAND<br />

COMPOUND NAME<br />

.......................<br />

DICHLORODIFLUOROMETHANE<br />

CHLOROMETHANE<br />

u<br />

- BROMOMETHANE<br />

VINYL CHLORIDE<br />

CHLOROETHANE<br />

METHYLENE CHLORIDE<br />

TRICHLOROFLUOROMETHANE<br />

TOTAL 1,2-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHANE<br />

1,1,1-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICHLOROMETHANE<br />

1,2-DICHLOROPROPANE<br />

TRANS-1,3-DICHLOROPROPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

DIBROMOCHLOROMETHANE<br />

1,1,2-TRICHLOROETHANE<br />

CIS-1,3-DICHLOROPROPANE<br />

2-CHLOROETHYL VINYL ETHER<br />

BROMOFORM<br />

1,1,2,2-TETRACHLOROETHANE<br />

- TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,3-DICHLOROBENZENE<br />

1,2-DICHLOROBENZENE<br />

1,4-DICHLOROBENZENE<br />

TOTAL XYLENE<br />

2-PROPANONE (ACETONE)<br />

GC/MS<br />

VOLATILE ANALYSIS<br />

AMOUNT<br />

-----------<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

Data File:>9153V<br />

719153<br />

DET. LIMIT<br />

----------<br />

125 ug/kg<br />

250 ug/kg<br />

250 ug/kg<br />

250 ug/kg<br />

250 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

250 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 .ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

125 ug/kg<br />

Checked By


Element<br />

Aluminum<br />

Antimony<br />

Arsenic<br />

Barium<br />

Beryllium<br />

Cadmi um<br />

Calcium<br />

Chromium (Total)<br />

Cobalt<br />

Copper<br />

Iron<br />

Lead<br />

Magnesium<br />

Manganese<br />

Mercury<br />

Molybdenum<br />

Nickel<br />

Potassium<br />

Selenium<br />

Si lver<br />

Sodi um<br />

Stronti um<br />

Thall ium<br />

Vanadium<br />

Zinc<br />

Reference Methods<br />

Metals<br />

Soi 1<br />

Atomic Absorption Metals Analysis<br />

Graphite Hydride<br />

F 1 ame Furnace Generation<br />

- I<br />

- EPA 7040 AA 7041<br />

ZA P A 7060 - EPA 7061<br />

- EPA 7080 - EPA 7081<br />

- EPA 7090 -EPA 7091<br />

- EPA 7130 - EPA 7131<br />

- EPA 7190 - EPA 7191<br />

-<br />

EPA 7210 EPA 7211<br />

A<br />

- EPA 7380 EPA 7381 -<br />

- EPA 7420 EPA 7421 -<br />

- EPA 7460 EPA 7461 -<br />

- EPA 7520 EPA 7521 -<br />

- .&PA 7740<br />

-<br />

- EPA 7760 EPA 7761<br />

- EPA 7770<br />

-<br />

- EPA 7840 YEPA 7841<br />

EPA 7910 - EPA 7911<br />

-EPA 7950 EPA 7951<br />

- -<br />

- EPA 7741<br />

ANALYST IL LS<br />

proJect # 87-035-3020<br />

Date Compf eted 1 1 -1j-19~<br />

Cold<br />

Vapor ICP<br />

-<br />

- EPA 6010<br />

- EPA 6010<br />

- EPA 6010<br />

- ,+PA 6010<br />

- EPA 6010<br />

- EPA 6010<br />

- YEPA 6010<br />

- EPA 6010<br />

- EPA 6010<br />

- 4 A 6010<br />

&PA 6010<br />

-


u<br />

Preparation:<br />

Reference Methods<br />

I"tetc1s<br />

Acid Digestion EPA 3010<br />

- EPA 3020<br />

- EPA 3030<br />

- EPA 3040<br />

/ EPA 3050<br />

-<br />

Mercury Digestion - EPA 7470 Water<br />

-<br />

EPA 7471 Soi 1<br />

Alkaline Digestion - EPA 3060<br />

EP Toxicity EPk 1310<br />

CAM STLC -<br />

OTHER<br />

Title 22 CAC


Preparation<br />

Water - EPA 3510<br />

- EPA 3520<br />

Soi 1 - EPA 3540<br />

Reference Methods<br />

Semi-volatile Organics<br />

(BNA's)<br />

Analysis<br />

- EPA 625<br />

Project # 87-035-3020<br />

Date Completed 11-13-1 987<br />

ANALYST DL-/


Water<br />

Soi 1<br />

Reference Methods<br />

Volatile Organic Analysis<br />

Preparation Analysis<br />

ANALYST ".c-v<br />

1) Eisenberg, Don M.. et al, "Guidelines for<br />

Addressing Fuel Leaks", California Regional<br />

Water Quality Control Board. San Francisco<br />

Bay Region, Sept. 1985.<br />

- EPA 601<br />

- EVA 602<br />

- EPA 624<br />

- EPA 8010<br />

- EPA 8015<br />

- EPA 8020<br />

EPA 8240<br />

i<br />

- Guidelines for<br />

Addressing<br />

Fuel Leaks 1


Client ID: BAY AREA DRUM Data ~ile:>9822V<br />

Sample ID: 87-035-03-3086 719822<br />

Matrix : SOIL SAMPLE: VCS2<br />

COMPOUND NAME<br />

P==P======PP======I=E==<br />

DICHLORODIFLUOROMETHANE<br />

CHLOROMETHANE<br />

BROMOMETHANE<br />

VINYL CHLORIDE<br />

CHLOROETHANE<br />

METHYLENE CHLORIDE<br />

TRICHLOROFLUOROMETHANE<br />

1, 1-DICHLOROETHENE<br />

1,l-DICHMROETHANE<br />

TOTAL 1,2-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHANE<br />

lIltl-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICIILOROMETHANE<br />

1,2-DICHLOROPROPANE<br />

TRANS-1,3-DICHLOROPROPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

CIS- 1,3-DICHLOROPROPANE<br />

2-CHLOROETHYL VINYL ETHER<br />

BROMOFORM<br />

1,1,2,2-TETRACHLOROETHANE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,4-DICHMROEENZENE<br />

TOTAL XYLENE<br />

2-PROPANONE (ACETONE)<br />

GC/MS<br />

VOLATILE ANALYSIS<br />

AMOUNT<br />

========PI=<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

730.<br />

ND<br />

ND<br />

150.<br />

ND<br />

ND<br />

ND<br />

ND<br />

1300.<br />

160.<br />

ND<br />

ND<br />

ND<br />

DET. LIMIT<br />

==E..i======<br />

25 ug/kg<br />

50 ug/kg<br />

50 ug/kg<br />

50 ug/kg<br />

50 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

50 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

Checked By


u<br />

-<br />

Client ID: BAY AREA DRUM Data File: >9822V<br />

Sample ID: 87-035-03-3086 719822<br />

Matrix : SOIL SAMPLE: VCS2<br />

COMPOUND NAME<br />

I I ~ I I I P I I I I I I P e P = m E p I L I<br />

DICHLORODIFLUOROMETHANE<br />

CHLOROMETHANE<br />

BROMOMETHANE<br />

VINYL CHLORIDE<br />

CHLOROETHANE<br />

METHYLENE CHLORIDE<br />

TRICHLOROFLUOROMETHANE<br />

Ill-DICHLOROETHENE<br />

lll-DICHMROETHANE<br />

TOTAL 112-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHANE<br />

1,1,1-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICHLOROMETHANE<br />

112-DICHLOROPROPANE<br />

TRANS-113-DICHLOROPROPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

DIBROMOCHLOROMETHANE<br />

1,1,2-TRICHLOROETHANE<br />

CIS-1,3-DICHLOROPROPANE<br />

2-CHLOROETHYL VINYL ETHER<br />

- BROMOFORM<br />

~I~,~,~-TETRACHLOROETHANE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,3-DICHLOROBENZENE<br />

1,2-DICHLOROBENZENE<br />

- - - - - - - -<br />

1 ; 4-DICHLOROBENZENE<br />

TOTAL XYLENE<br />

2-PROPANONE (ACETONE)<br />

GC/MS<br />

VOLATILE ANALYSIS<br />

AMOUNT<br />

P==EPII=ILI<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

730.<br />

ND<br />

ND<br />

150.<br />

ND<br />

ND<br />

ND<br />

ND<br />

1300.<br />

160.<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

26.<br />

490.<br />

ND<br />

370.<br />

ND<br />

DET. LIMIT<br />

IIPPIIPIII<br />

25 ug/kg<br />

50 ug/kg<br />

50 ug/kg<br />

50 ug/kg<br />

50 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

50 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

25 ug/kg<br />

Checked By


November 19, 1987<br />

Mr. Rich Greenwood<br />

Canonie Environmental<br />

1825 S. Grant Street, Suite 260<br />

San Mateo, CA 94402<br />

Dear Mr. Greenwood:<br />

Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />

Canonie Environmental Analytical Laboratory.<br />

Canonie Environmental Services Cop. -<br />

212 Frank Wen Circle<br />

Suite A<br />

Stockion. California 95206<br />

Phone: 209-983-1340<br />

Unless o<strong>the</strong>rwise instructed by you samples will be returned or disposed of<br />

two weeks from <strong>the</strong> date of this letter.<br />

If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />

Very truly yours.<br />

~anhydr of- Laboratory Services<br />

Enclosure<br />

I


Laboratory Report for<br />

Mr. Rich Greenwood<br />

Canonie Environmental<br />

1825 S. Grant Street. Suite 260<br />

San Mateo, CA 94402<br />

November 19, 1987<br />

Canonie Environmental<br />

212 Frank West Circle, Suite A<br />

Stockton, CA 95206<br />

(209) 983-1 340


Client ID: BAY AREA DRUM<br />

Sample ID: 87-035-03-3086<br />

Matrix : SOIL SAMPLE: VCS2<br />

COMPOUND NAME<br />

.......................<br />

DICHLORODIFLUOROMETHANE<br />

L CHLOROMETHANE<br />

-<br />

BROMOMETHANE<br />

VINYL CHLORIDE<br />

CHLOROETHANE<br />

METHYLENE CHLORIDE<br />

TRICHLOROFLUOROMETHANE<br />

1,l-DICHLOROETHENE<br />

1,l-DICHLOROETHANE<br />

TOTAL 1,2-DICHLOROETHENE<br />

CHLOROFORM<br />

1,2-DICHLOROETHANE<br />

1,1,1-TRICHLOROETHANE<br />

CARBON TETRACHLORIDE<br />

BROMODICHLOROMETHANE<br />

1,2-DICHLOROPROPANE<br />

TRANS-1,3-DICHLOROPROPENE<br />

TRICHLOROETHENE<br />

BENZENE<br />

DIBROMOCHLOROMETHANE<br />

1,1,2-TRICHLOROETHANE<br />

CIS-1.3-DICHLOROPROPANE<br />

2-CHLOROETHYL VINYL ETHER<br />

BROMOFORM<br />

- 1,1,2,2-TETRACHLOROETHANE<br />

TETRACHLOROETHENE<br />

TOLUENE<br />

CHLOROBENZENE<br />

ETHYL BENZENE<br />

1,3-DICHLOROBENZENE<br />

1,2-DICHLOROBENZENE<br />

1,4-DICHLOROBENZENE<br />

TOTAL XYLENE<br />

2-PROPANONE (ACETONE)<br />

GC/MS<br />

VOLATILE ANALYSIS<br />

AMOUNT<br />

-----------<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

ND<br />

730.<br />

ND<br />

ND<br />

150.<br />

ND<br />

ND<br />

ND<br />

Data File:>9822V<br />

719822<br />

Checked By


L. Water<br />

-<br />

-<br />

So1 1<br />

Reference Methods<br />

Volatile Organic Analysis<br />

1) Eisenberg. Don M.. et al, "Guidel~nes for<br />

Preparation Analysis<br />

Addressing Fuel Leaks", California Regional<br />

Water Qua1 i ty Control Board. San Francisco<br />

Bay Reg~on. Sept. 1985.<br />

- EPA 601<br />

-. EVA 602<br />

- EPA 624<br />

- EPA 5030 - EPA 8010<br />

- EPA 8015<br />

EPA 8020<br />

.* EPA 8240<br />

Project # 87-035-03-3086<br />

Date Completed 11-19-1987<br />

- Guidelines for<br />

Addressing<br />

Fuel Leaks 1


-<br />

:tiv~ty.,. ... . b Enf 0 SUIV SiIeMit o ~ermltting _a A I Tech ~<br />

O!hrr<br />

10. SAMPLING LOCATION<br />

11. SAMPLES<br />

- -<br />

12. ANALYSIS REQUESTED I. PC8<br />

Container I<br />

k. q Ext. Orp<br />

(Scroeng)<br />

e. 0 pH g. c VOA I. ~Cnlorinrtrd<br />

Pect~c~drr<br />

JM~tal<br />

Scan h. 0 PAH<br />

m. ~Organo-P<br />

PestIclde8<br />

d. a W.E.T.<br />

4<br />

I. 0 Phenols n, Cl<br />

I. ucarba-<br />

- ~ L ~ O S 0.0<br />

13. CHAIN OF CUSTODY I<br />

4. SPECIAL REMARKS j<br />

7 ANALYSIS REQUESTED<br />

.<br />

-<br />

L I<br />

A I<br />

B I<br />

, ,


ww QCliEPT<br />

. .- 02-19-** . - - -<br />

FRI 05:33:36 G 3 ** ****<br />

. .<br />

NO. 85


L<br />

-<br />

LABORATORY REPORT FOR TOTAL METAL ANALYSIS<br />

COLLECTOR'S NAHE: C DAVENPORT COLLECTOR'S SAMPLE NO. : RY-1R<br />

WlPLE LOCATION : BRY AREA DRUM H Y BITER ACTIVITY :<br />

8FO DATE RECEIVED :<br />

ANALYTICAL SAMPLES ARE DIOESTED WITH CONCENfRdTED NITRIC ACID OVER A HOT<br />

PROCEDURE : PCdTE. THE DIGEBTED BAHPLEB ARE FILTERED AND MADE TO 100 ML<br />

WITH 5% NITRIC ACID IN DISTILLED DEIONIZED WATER. RETAL ANALYSIS<br />

OF THE DIOEBT IS BY ICPREB. RESULTS ARE REPORTED R8 UOIGRRH,<br />

HUL NUUBER : Dl047 Dl048<br />

COLLECT SAHP #: RW-LA RY-10<br />

SAMPLE TYPE : LIQUID LIPUlD<br />

AG-S ILVE R<br />

WRSENIC<br />

BA-BARIUFI<br />

BE-BERYLLIUH<br />

CD-CADMIUH<br />

CO-COBALT<br />

CR-CHROUIUFl<br />

CU-COPPER<br />

flO-MOLYBDENUH<br />

N1-NICKEL<br />

Pa-LEAD<br />

SO-ANTfUONY<br />

BE-SELENIUM<br />

V -VANADIUM<br />

ZN-ZINC<br />

TL-THflLLIUH<br />

-<br />

NOTE: < BELOW DETECTION LIMIT OF INBTRUMENT (***).NOT DETERMINED BY ICP<br />

- :<br />

.. 02-19-** FRI 05:31:14 G3<br />

: hx .<br />

3%:<br />

Y* **** N0.03


STAT5 OF CAiiiD2i::i-iiEiilK ASC VIE::AEE AGENCY GEORGE DE~l~EjiiN, Gor?.nar<br />

--<br />

DEPARTMENT OF HEALTH SERVICES<br />

2151 GEiKE:F\ r' : i<br />

JAN74 198F /--a?!<br />

'CKELEY. CA PI704<br />

Tommy Lee<br />

SF Dept. of Public Works<br />

750 Phelps Street<br />

SF, CA 94124<br />

Dear Tommy,<br />

January 13, 1987<br />

As per our phone conversation yesterday, I am forwarding to you<br />

our laboratory analysis of <strong>the</strong> rainwater that has pnded inside<br />

<strong>the</strong> Bay Area Drum building. The cyanide analysis is enclosed, and<br />

<strong>the</strong> metals analyses have already been sent to you. The cyanide<br />

analysis was delayed dua to internal prioritization at <strong>the</strong><br />

laboratory.<br />

As we agreed, I have informed Kurt Ahlich of Canonie<br />

Environmental that he can take <strong>the</strong> necessary steps to transfer<br />

this water to <strong>the</strong> sewer. He will contact you to arrange a<br />

convenient time for both you and him to initiate <strong>the</strong> discharge.<br />

-<br />

Thanks again for your cooperation in assisting DHS in <strong>the</strong>ir<br />

cleanup efforts at <strong>the</strong> Site. If you have any questions, please<br />

contact me at (415) 540-3401.<br />

4<br />

cc: u ~ Ahlich, t Canonie<br />

Herome ~arcotte, DHS<br />

Cordially<br />

~lif#on W. ~avendort<br />

Associate Engineering Geologist<br />

Site Mitigation Unit


. site BOLL A\- -? c fipk? 1'.2<br />

. . c'<br />

- c. .As'dress 13 \I<br />

a. EPk ID W3.<br />

6. INDEX<br />

>\c&z . S.F (.&<br />

ii.73~: Sirecl Cily Zip . .<br />

-<br />

i... 3 Ex:. 0:g<br />

72. A~\'.~LYs:s EC:.ISTED 1. n PCB (sc;;t"g)


Cate Received<br />

lector's ::me c/;/'hm II&UP~,D"~P by Laboratory /2//// 87<br />

San?plin,- Location R&, q.-c, A!. fd =?;re<br />

J Collector's Sarcple !,Qwl(d to<br />

Reference: MNL Hg - /A oob<br />

ANALYSIS RiSULTS: . . . .<br />

. .. . . .<br />

. .. . . . .<br />

Analyst ' s Sienatures: ..<br />

7 . /I cL 22<br />

I , ..Ll!zU' date<br />

2.<br />

M CRLY.)<br />

'date<br />

California Department of Health Services - Hazardous Materials Laborntory<br />

-<br />

.


APPENDIX D<br />

Environmental


James M. Cramer<br />

VICE PRESIDENT<br />

/<br />

IILEX USA INC.<br />

:alltornla Branch PO 80x 24397 Venlura CA 93002<br />

ax 1805) 642.0777<br />

NlLEX<br />

February 13, 1958<br />

Canonie Environmental<br />

1E25 S. Grant Ave. Suite 2LO<br />

San Mateo, CA.<br />

944ii2<br />

Attention: Mike Klein<br />

RE: BAY AREA DRUM, 60 MIL HDPE CAPlGEDTETFILE<br />

NlLEX USA INC;<br />

Csllfornla Branch<br />

PO Box 24397<br />

Ventura. CA 93002<br />

Phone (805) 654-0610<br />

Fax (8051 642-0777<br />

As per your request we are providing you with <strong>the</strong> required<br />

submittals far <strong>the</strong> above project.<br />

It is our recommendation that <strong>the</strong> gectextiie not be<br />

connected to <strong>the</strong> structure as it will interfere with <strong>the</strong><br />

sealing of <strong>the</strong> membrane at <strong>the</strong> concrete interface. ; n e<br />

geotextile shall be terminated within six inches 16'! frcm<br />

<strong>the</strong> edge of <strong>the</strong> liner.<br />

All seams fc~r <strong>the</strong> geotextile shall be overlapped 2' ta<br />

ensure proper continuity a+ <strong>the</strong> fabric.<br />

4 miii certificate or certifiration that ths geotextile<br />

meets ail of <strong>the</strong> enclosed specifications shall be forwarded<br />

tn <strong>the</strong> owner as soon as possible.<br />

Tie fabric shall be shi~ped in black poiyethylene wrapping<br />

te ensure protection frnm U.V. The material shall be<br />

unloaded and handled with rare to ensure <strong>the</strong> original state<br />

of <strong>the</strong> fabric.<br />

I trust <strong>the</strong> above submittal will meet with your approval<br />

should you have any comments or questions please cali me at<br />

your convenience.<br />

Sincerely,<br />

NILEX USA INC.<br />

James M Cramer<br />

Vice President<br />

I" canada: NILEX GEOTECHNICAL PRODUCTS INC. ~dmonton, AB ana ~urnaby. BC<br />

-.


Canonie Environmental<br />

1825 S. Grant fivr. Suite P60<br />

San Wateo, CQ.<br />

94 40;'<br />

RE: HUNTERS POINT 60 MIL HDPE CAP--SUBMITT0LS<br />

NlLEX USA INC.<br />

calnmla Bmnch<br />

PO Box 24397<br />

Ventura. CA 93002<br />

Phone (805) 654-0610<br />

Fax (805) 642-0777<br />

As per your recluest we are providing you with <strong>the</strong> required<br />

submittals for thp above project.<br />

1.5 HDPE Lininq<br />

1.5.1 Item C.<br />

Schleqel Lining Technology ~ 1.11 warrant <strong>the</strong> material for a<br />

period of two (2) year5 from date of installation. Nilex<br />

US0 Inr. will warrant <strong>the</strong> installation of <strong>the</strong> material for a<br />

period of two (2) years from <strong>the</strong> date of installation.<br />

1.6. Item 0.<br />

The HDPE sheet shall be laid out as per <strong>the</strong> Nilex field<br />

representative's direction. Prior to any fipld welding<br />

commencing a test weld of 3 feet shall be performed to<br />

ensure <strong>the</strong> welder- is set to <strong>the</strong> present ambient outdoor<br />

c~nditions. These welds will be tested for tensile and peel<br />

values by <strong>the</strong> Nilex technician. Pending <strong>the</strong> Nil€*x<br />

technicians approval <strong>the</strong> welding will start. Sheet that can<br />

not be seamed will not be la~d out that day. Rs <strong>the</strong> sheet<br />

is laid out at <strong>the</strong> penetrations for <strong>the</strong> fer~ce a<br />

prefabricated boot shall be installed over <strong>the</strong> fence post<br />

and welded to <strong>the</strong> parent sheet material. A compression<br />

fitted band will be installed as per enclosed detail. Upon<br />

completion of <strong>the</strong> installation of <strong>the</strong> membrane <strong>the</strong> Nilex<br />

technician shall visually inspect <strong>the</strong> entire site and all<br />

seams for any holes or defects. Upon <strong>the</strong> approval of <strong>the</strong><br />

Nilex technician backfilling of <strong>the</strong> membrane w ~ll commence.<br />

Nilex certifies that all field seams performed in <strong>the</strong> above<br />

contract will meet <strong>the</strong> enclosed General Specifications For<br />

HDPE Lining. Any samples requiring verification by an<br />

independent laboratory will be at <strong>the</strong> owners expense.<br />

In CM.d.: HIW QEOTECHNICALPROWCTS INC. E m ,<br />

*B am BuW, sC


1.5.1 Item R<br />

It is o:Jr 1-rv:oamendat~on that <strong>the</strong> r:t.otext;le not be<br />

corinected to <strong>the</strong> structirre as it will ~nterfere WI th t.hc!<br />

seal lnq OF tl;e menhi-ane at <strong>the</strong> co~lcretr. interf-?ace. The<br />

qrwt~xtile shall be tcrmlnated within six inches (6") fr-on:<br />

<strong>the</strong> ~dqe of <strong>the</strong> 1 ~ ner<br />

.<br />

All se.tms for <strong>the</strong> geolextile %hall be overlapped 2' to<br />

ensure proprr cant~nu: ty of <strong>the</strong> fabi-IC.<br />

R m i l l certificate or certlflcatlon that <strong>the</strong> geotextlle<br />

meets all of <strong>the</strong> enclosed specif~cations shall be forwarded<br />

to <strong>the</strong> owner as soon as possibl~.<br />

Ihe fabr~c shall he shlpped in ti lack polyethylene wrappinq<br />

to ensure protection from L1.V. The material shall be<br />

unloaded and handled with care to ensure <strong>the</strong> criginal state<br />

of <strong>the</strong> fabric.<br />

I trust <strong>the</strong> above submittal will meet with your approval<br />

should you have any comments or questions please call me at<br />

your convenlencc.<br />

Sincerely,<br />

James M Cramer<br />

Vice President


a NlLEX<br />

USA INC.<br />

P 0 BOX 24397<br />

VENTURA. CA 93002<br />

PHONE (805) 654-0610<br />

N'iEX FAX. ,805) 642.0777


~ - ,-<br />

. . . ... I . ~Z3ELsALLREnSJ~E?4EXTS<br />

A. Ssgae<br />

GENERAL S1ECIIICYUONS FOR HDPE LINING<br />

The work covers <strong>the</strong> manufacture and installation of a<br />

high den'sity polyet-hylene (SCELEGEL~ sheet) liner for<br />

<strong>the</strong> lining of ear<strong>the</strong>n basins for <strong>the</strong> protection of<br />

groundwater.<br />

i<br />

The work includes furnishing all equipment and<br />

materials, providing all labor, supervision,<br />

administration and managenest; and supplying ail<br />

construction equipment, materials and services<br />

necessary to perfora <strong>the</strong> work as detailed in this<br />

specification.<br />

The lining contractor's asproved drawings for<br />

construction will specify all components and details<br />

require? to meat specifications. The responsibility<br />

of <strong>the</strong> owner or <strong>the</strong> lining contractor will be clearly<br />

indicated.


-<br />

9 d ~<br />

.~~<br />

~~ ~.<br />

.The manufacturer/installer must have at least five ( 5)<br />

years continuous ex2erience in <strong>the</strong> manufactnre and<br />

installation of SCSLEGZL~ sheet, and must have<br />

- . . . . . . -. -. manufactured and installed at least 20,000,000 square<br />

feet of <strong>the</strong> material specified for this project.<br />

The manufacturer/installer shall submit a list of ten<br />

(10) similar installations which have besn in service<br />

at least two (2) yebrs. .The list shall include <strong>the</strong><br />

owner's name, location of project, square feet of<br />

product installed, ahd <strong>the</strong> completion date.<br />

.Submittals not including this.required information<br />

will not be acce?ted.<br />

Submit for approval samples of SCELEGZL~ sheet<br />

for customer reviev 2nd testing. Testing shall<br />

include compatibility analysis by material<br />

supplier or owner.<br />

Submit for approval as soon as practical after<br />

award of <strong>the</strong> contract, six (6) sets of full and


complete shop and installation drawings showinq a<br />

minimum of:<br />

a. Layout of <strong>the</strong> liner systen.<br />

.b. .Details of jointing, liner system, liner<br />

anchorages to concrete structures, details<br />

of sealing <strong>the</strong> SCHLZGZLO sheet to concrete<br />

structures, and any o<strong>the</strong>r openings into <strong>the</strong><br />

structure.<br />

Certificates of compliance with <strong>the</strong> requirezests<br />

of standards and testing methods specified herein<br />

shall be submitred prior to delivery. .The liner<br />

material manufacturer must satisfy by affidavit<br />

to <strong>the</strong> owner and contractor, jointly, that <strong>the</strong><br />

material he offers to furnish and install will<br />

meet in every aspect <strong>the</strong> requirenents set forth<br />

in <strong>the</strong> specifications. .The contractoc shall<br />

transmit to <strong>the</strong> owner <strong>the</strong> affidavit given him by<br />

<strong>the</strong> manufacturer or supplier prior to apgroval<br />

for <strong>the</strong> furnishing and installing of any such<br />

material.


The contractor shall submit a schedule detailing<br />

<strong>the</strong> liner fabrication and installation,<br />

1. .&1i-vo=,v<br />

.Materials shall be delivered to <strong>the</strong> site after<br />

<strong>the</strong> required submittals have been ap~roved.<br />

Storage and handling of <strong>the</strong> materials shall<br />

conform to <strong>the</strong> manufacturerls recarmendations and<br />

shall be done in such a manner as to prevent<br />

dainage to any part of <strong>the</strong> work.<br />

Reference Standards shall comply with <strong>the</strong> apglicable<br />

. . . - . . .<br />

- - - - ---provisions and recommendations of <strong>the</strong> American Society<br />

for Testing Materials (AST:4), exce~t as o<strong>the</strong>rvise<br />

shown or specified.


F. Job Conddfl~ns<br />

Prior to installation of <strong>the</strong> liner, contractor shall<br />

verify conditions of existing facilities and<br />

structures to ensure an adequate subgrade for <strong>the</strong><br />

liner, as specified in Section 1II.B of this docmeat.<br />

Destructive and non-destructive testing are carried<br />

.out by trained personnel of <strong>the</strong> lining contractor.<br />

.Quality cantrol procedures are specified in Section IV<br />

of this document.<br />

Terns and conditions of <strong>the</strong> wtrranty to be agreed uFcn<br />

between <strong>the</strong> owner and <strong>the</strong> lining cont:ackor.<br />

The lining shall be a high density polyethylene<br />

(SCSLEGZL9 sheet] containing no additives, fillers or<br />

extenders. Carbon black 23 2 .51 shall be added to


___--_ ..-._L__..._.-.._.-~I_.- -- -- -- ---tke<br />

resin for ultraviolet resisk~nce. The lining sy~==~ sh211<br />

be manuftctured, furnished and installed by a single<br />

contractor. Typical physical progerties of <strong>the</strong> DPE: liner<br />

(SC~LEGZL~ sheet) are described in Table 1.<br />

Resin use? for extrusion joining shests and shest to<br />

pipe shall be WPS produced from <strong>the</strong> same resin es <strong>the</strong><br />

sheet. .Physical properties shall be <strong>the</strong> same as tkose<br />

of <strong>the</strong> resin &ed in <strong>the</strong> manufacture of <strong>the</strong> HDPE<br />

liner. The resin shall be sucolied in black.<br />

Sponge rubber sheeting shall be type SCS-41,<br />

Neoprene/EPT/SaR, Closed Cell Medium, 114 inch thick,<br />

one side adhesive.<br />

PYTHON, neoprene adhesive shall be use? for gluing<br />

sponge rubber shesting to concrete and EDPE surfac=s.<br />

Batten strips shall be No. 12 gauge steel type A-36.<br />

Width of strips shall be two inches (2") minimum.


- 7<br />

.. ~<br />

- -<br />

- -<br />

Product and manufacturez: provide alloy steel<br />

fasteners as manufactured by <strong>the</strong> following:<br />

1. -2 -Molly .Parabolts by US?{ Corporation<br />

2. Kwik-Bolt Eilti Corporation<br />

3 .Ramset, Inc.<br />

.4. Or Ap~roved Equal<br />

.Wet or dry elastic roof sealer as manufactured by<br />

Bonsey Products, Inc.<br />

The lining contractor shall be res~onsible for<br />

inspection of <strong>the</strong> sheet rolls at <strong>the</strong> job site. Should<br />

rolls show damage from transit, <strong>the</strong>y will be so<br />

identified by <strong>the</strong> lining contractor and set aside.<br />

During unrolling of <strong>the</strong> lining material, <strong>the</strong> lining<br />

contractor will carry out visual inspection of tbe


sheet surface. Any faulty areas shall be marked and rezaire; - ir.<br />

an approved mznner by <strong>the</strong> lining contractor.<br />

. B . B1f:2-S~bazzd5-E~_e2az3f i-01)<br />

The Purchaser shall be responsible for presaring <strong>the</strong><br />

earthwork as required. .No broken stones or hard<br />

objects shall be present on <strong>the</strong> surface to be lined.<br />

Stones larger than t-do inches (2") in diameter, shaq<br />

.edged stones of any size, and hard objects shall not<br />

be persitted within four inches (4") of <strong>the</strong> surface to<br />

be line?. The surface shall be compacted to a density<br />

to allow tbe movenest of vehicles and weldina<br />

equipment on it without causing rutting or o<strong>the</strong>r<br />

deleterious effects. .Typically, this is a density of<br />

.85-90 Standard Proctor.<br />

The surface of all concrete bonding surfaces shall be<br />

cleaned and smoo<strong>the</strong>d prior to anchoring <strong>the</strong> liner.<br />

The SCSLEG2L9 sheet shall be laid out and<br />

installed by manufact=reras trained technicians<br />

in ac=ordance with <strong>the</strong> applicable approved shop<br />

drawings.


-<br />

6 ~ ~ .<br />

- ' - - . - . The sheets shall be placed in <strong>the</strong> basin to persit<br />

termination at <strong>the</strong> top of <strong>the</strong> side slopes and<br />

adjacent to concrete structures and pipe conduits<br />

as shown on <strong>the</strong> drawings. The layout shall be<br />

'<br />

- - - -- - - .<br />

. - . . . . .<br />

. . . - - -<br />

.<br />

designed to minimize <strong>the</strong> number and length of <strong>the</strong><br />

field joints, consistent with proper methods of<br />

liner installation.<br />

.Field joints shall be made by overlapping<br />

adjacent sheets a minimum of eight inches<br />

- (8") and extruding a ribbon of extrusion<br />

joining resin no less than 1.5 inches (1.5")<br />

in width between <strong>the</strong> overlapped sheets or<br />

over <strong>the</strong> seam beheen <strong>the</strong> sheets where hand<br />

welds are required,<br />

Prior to extrusion welding of <strong>the</strong> seams, all<br />

.areas whicb are to become seam intezfaces<br />

shall be cleaned of dust and dirt. The<br />

slick surfaces of <strong>the</strong> HDPE sheet which are<br />

to become Sean interfaces shall be rougherbed<br />

with a wire brush or o<strong>the</strong>r acceptable means<br />

before extrudate is placed between <strong>the</strong><br />

overlapping sheets or over a lapped sean.


Exkrusion joining shall not take place<br />

unless <strong>the</strong> sheet is dry and shall not take<br />

place unless <strong>the</strong> ambient tenperature is<br />

above 20 " F and below 90" F.<br />

Joints betveen <strong>the</strong> lining sheets shall be<br />

field welded using <strong>the</strong> manufacturer's<br />

extrusion joining equipment and techniques.<br />

The joining procedure shall consist of<br />

softening <strong>the</strong> liner material by heated air.<br />

.The teqerature of <strong>the</strong> air impinging on <strong>the</strong><br />

sheet for this purpose shall range from<br />

420 .F to 680' .F. The exact tenperature<br />

used shall be determined by <strong>the</strong> installation<br />

supervisor. Directly following <strong>the</strong><br />

application of heat, a one inch (1") minims<br />

width strip of <strong>the</strong> same high density<br />

polyethylene resin from which <strong>the</strong> sheet is<br />

made shall be extruded betxeen <strong>the</strong><br />

overlapped sheets. The temperature of <strong>the</strong><br />

resin as it emerges from <strong>the</strong> extrusion die<br />

shall range from 428" F to 536' F. The<br />

overlapped sheets are <strong>the</strong>n pressed toge<strong>the</strong>r<br />

to form <strong>the</strong> extrusion joint.


Penetrations through <strong>the</strong> liner for pige<br />

flashings, patches, etc., shall be field<br />

welded using an extrusion hand welder. The<br />

joining procedure shall consist of softening<br />

...- - - - . <strong>the</strong> liner material by heated air as<br />

*<br />

described above. Directly following <strong>the</strong><br />

agplication of heat, a hot strip of <strong>the</strong> saze<br />

material from which <strong>the</strong> sheet is made will<br />

be extruded over <strong>the</strong> joint to produce <strong>the</strong><br />

extruded joint.<br />

Any required repair of mall holes in <strong>the</strong><br />

liner surface shall be made with <strong>the</strong><br />

extrusion hand welder. Liner material shall<br />

be cleaned of all dirt, dust, and o<strong>the</strong>z<br />

. foreign material, all smooth SCBLEGZLO sheet<br />

surfaces roughened, air heated to <strong>the</strong><br />

prescribed temperature, and a strip of BDPE<br />

resin extruded over <strong>the</strong> hole to produce an<br />

extrusion weld repair.<br />

- - . . . - - . - - . . - - . - . Seals around penetrations shall be made as<br />

described below.


All pipe pesetrations shall be sleeve? with<br />

DPE pipe. Each EDPE pipe sleeve shall be<br />

sealed to <strong>the</strong> liquid carrying pipe to<br />

prevent leakage. The basin liner shall be<br />

. . .- -.-anchored to a concrete collar surrounding<br />

<strong>the</strong> pefietration. A SCSLEGEL~ sheet apron<br />

shall be extrusion welded to <strong>the</strong> pipe sleeve<br />

and shall be extrusion welded to <strong>the</strong> base<br />

sheet outside of <strong>the</strong> area where <strong>the</strong> base<br />

sheet is anchored to <strong>the</strong> concrete collar.<br />

The manufacturer of <strong>the</strong> HDPE resin used in sheet<br />

production tests eacfi batch before delivery to ensure<br />

a maximum consistency of raw material quality.<br />

The following tests shall be carried out by <strong>the</strong><br />

.. . - pcoducer of <strong>the</strong> raw material on each batch and <strong>the</strong><br />

results forwarded to <strong>the</strong> sheet fabricator:<br />

The density of <strong>the</strong> material reflects <strong>the</strong> degree<br />

of czystallinity, and thus serves as an indirect


check on mechanical qualities such as hardness,<br />

stiffness and tensile strength.<br />

- .Carbon black polyethylene serves primarily as<br />

protection against <strong>the</strong>rnal aging and harmful<br />

ultraviolet radiation present in outdoor<br />

wea<strong>the</strong>zing. Thus, quality control of <strong>the</strong> carbon<br />

black content ensures t5e good wes<strong>the</strong>ring<br />

properties of polyethylene.<br />

A material's melt index is a measure of its mezn<br />

molecglar weight and rheological properties.<br />

Thus, holding <strong>the</strong> melt index of <strong>the</strong> base material<br />

within a narrow ranse is a criterion for uniforz<br />

and optimum HDPZ liner production.<br />

Bell testing is a relatively fast method of<br />

testing a material's performance under mechanical<br />

stressing in aggressive media.


Maintaining a constant moisture content in <strong>the</strong><br />

base material is necessary for processing,<br />

resulting in a pore-free, bubble-free product.<br />

.Employing only material with a moisture content<br />

in a narrow tolerance range is ano<strong>the</strong>r<br />

requirenent for consistent product quality.<br />

The data determined is evaluated by <strong>the</strong> manufacturer<br />

and, if deviating from <strong>the</strong> agreed tolerance ranges,<br />

<strong>the</strong> tested batch is not delivered. As a 'result of<br />

this testing, <strong>the</strong> manufacturer is guaranteed<br />

consistent base material quality, essential in <strong>the</strong><br />

light of <strong>the</strong> denanding conditions prevailing in <strong>the</strong><br />

various apolications of WPE liners.<br />

The incoming raw material shall be sampled and tested<br />

in <strong>the</strong> lab facilities of <strong>the</strong> sheet manufacture;.<br />

Properties relative to processing shall be deternined,<br />

specifically:<br />

- Melt Index per ASTX Designation D-1238-73<br />

- Density per ASTM Designation D-792<br />

- Moisture Content per AST:I Designation D-570-63


This testing provides fur<strong>the</strong>r verification of<br />

consistent product quality, supplementary to <strong>the</strong><br />

manufacturer's certificate.<br />

If <strong>the</strong> test results are positive, a sample of <strong>the</strong><br />

. -. - --.-.---batch is processed in manufacturing and evaluated as<br />

- - to melting behavior, forming behavior, and <strong>the</strong> product<br />

sheet's visual appearance.<br />

No batch is sent into production before positive<br />

results are obtained for <strong>the</strong> incoming base material<br />

and <strong>the</strong> tesk processing. If negative results are<br />

obtained, <strong>the</strong> batch is excluded from processing and<br />

return& to <strong>the</strong> manufacturer.<br />

All properties determined in <strong>the</strong>se tests shall be<br />

compiled in <strong>the</strong> final shest certificate.<br />

Automatic control must be included in <strong>the</strong> extrusion<br />

process and <strong>the</strong> successive processing stages.<br />

Important parameters in all stages of processing shall<br />

be controlled by automatic control systems.<br />

Three different qualities of <strong>the</strong> sheet shall be<br />

inspected continuously during production:


.- -<br />

- Forming Process<br />

- Surface Apcearanco<br />

- Sheet Thickness<br />

-- - Processing parameters such as tezperature, pressure<br />

-- - and speed shall be continuously monitored for each<br />

liner produced. A measuring device, such as a strip<br />

chart recorder, shall be furnished, if requested.<br />

.Sheet thickness shall fall within <strong>the</strong> following<br />

parameters: Ninety percent (90%) of <strong>the</strong> gross sheet<br />

area shall be ,+ ten percent (2103) of nominal<br />

specified thickness. .Ten percent (103) of <strong>the</strong> gross<br />

sheet area shall be ,+ fifteen percent (215%) of<br />

nominal specified thickness.<br />

At least three random samples shall be taken from each<br />

sheet roll and forwarded to <strong>the</strong> laboratory for<br />

.- . .extensive testing. The sample sites shall be e~enly<br />

distributed to ensure a regresentative evaluation of<br />

<strong>the</strong> overall . quality.<br />

The following tests shall be carried out for each<br />

sheet:


-<br />

-<br />

. . - . - - . . - . .. "<br />

- Tensile Testing per ASTX Designation D-638<br />

-- Impact Tensile Testing per ASTX Designation D-1822<br />

- Thickness<br />

- Stress Cracking Resistance (Bell Test) per<br />

ASTX<br />

Designation D-1693-70.<br />

The following supglenentary tests shall be carried out<br />

for sheet samples from each raw material batch:<br />

- Melt Index per ASTX Designation D-1238-72<br />

- Thermal Shrinkage per ASTM Designation D-1204<br />

- Density per ASm Designation 0-792<br />

Records of this testing shall be a permanent<br />

surveillance of <strong>the</strong> production process and constant<br />

product quality, and shall be maintained by <strong>the</strong><br />

manufacturer.<br />

... . . -- Narrow tolerance ranges ensure high quality in<br />

production. Products deviating from <strong>the</strong>se ranges<br />

shall be renoved and <strong>the</strong> cause determined.<br />

Sheet installation work shall be carried out under<br />

painstaking supervision up to, and including, project<br />

completion.


The quality control shall be carried out by <strong>the</strong><br />

on-site personnel as well as outside testing<br />

institutions.<br />

Quality control of installation shall be divided into<br />

three areas:<br />

Checking <strong>the</strong> sheets delivered to <strong>the</strong> site for<br />

transport damages; checking of sheet<br />

identification number with number on certificzte.<br />

Inspection and continuous control of all welding<br />

process parameters.<br />

Testing of <strong>the</strong> completed weld seams.<br />

.on-site welding of <strong>the</strong> SCHLEGEL' sheet shall be<br />

carried out by an e:rtrusion welding process. This<br />

.-....p rocess shall guarantee consistent weld seam quality<br />

within a wide range of ambient conditions. The<br />

.control systea of <strong>the</strong> welding machines shall be<br />

- .- e:ctensively automated .to enable monitoring of <strong>the</strong><br />

welding process by <strong>the</strong> operating personnel.<br />

The welds shall be performed in one procedure by means<br />

of an automatic welding machine, which preheats <strong>the</strong><br />

welding surfaces to <strong>the</strong> desired temperature, injects a<br />

ribbon of molten HDPE material and <strong>the</strong>n applies<br />

contact pressure to <strong>the</strong> Sean.<br />

1


The procedure for fillet welds shall be similar in<br />

.that <strong>the</strong> welding area shall be preheated and <strong>the</strong><br />

welded material shall be molten WPE. The necessary<br />

contact pressure shall come from <strong>the</strong> weight of <strong>the</strong><br />

hand welding unit itself. Fillet welds shall be used<br />

only for resair .work and special designs.<br />

.Test welds shall be run preceding all extensive<br />

welding to assure good weld quality under <strong>the</strong><br />

prevailing site conditions; <strong>the</strong>se weld samples shall<br />

be subsequently subjected to mechanical testing.<br />

The main prereqiisite for good bonding shall be<br />

continuous monitoring of <strong>the</strong> welding process<br />

parameters, such as hot air tenperature, welding<br />

speed and contact pressure. This is best carried<br />

out by specially trained personnel. Visual<br />

inspection of <strong>the</strong> welding surfaces, <strong>the</strong> welding<br />

process and <strong>the</strong> completed weld by experienced<br />

- -. . . plastic welc?ezs, allows a reliable evaluation of<br />

seam quality.


Production of a quality welding sezm starts with<br />

G - - -.- - a preliminary test weld. The machine settings,<br />

-<br />

---. - pretreatment of <strong>the</strong> weld surfaces and adjustaent<br />

to environmental effects shall be tested on a<br />

sample welding sesm. A hand operable tensile<br />

testing macbine shall be on site for confirmation<br />

of <strong>the</strong> joint's tensile strength using strip<br />

samples.<br />

.After installation, two major types of quality<br />

,control shall be available for testing <strong>the</strong> seas:<br />

- Destructive material tests of weld samples<br />

(spot cbeck)<br />

- Non-Destructive material tests of all welding<br />

seams.<br />

Txo samples shall be taken daily for<br />

Destructive tests on all weld seams;

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