1 - the Envirostor
1 - the Envirostor
1 - the Envirostor
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March 22, 1988<br />
I . Ciifton W. Davenport<br />
California Department of Health Services<br />
5850 Sheilmound, Suite 100<br />
Emeryville, CA 94608<br />
Dear Mr. Davenport:<br />
Draft Final Report<br />
Bay Area Drum<br />
Expedited Response Action<br />
Canonie Envlronmentai Sewices Corp.<br />
1825 South Grant Sheet<br />
Suite 260<br />
San Matea, California 94402<br />
Mione: 415-573 8012<br />
Enclosed is one copy of <strong>the</strong> Draft Final Report, Bay Area Drum Expedited<br />
Response Action, for your review.<br />
If you have any questions, please contact us at (415) 573-8012.<br />
Very truly yours,<br />
Claude Carlos White, Jr.<br />
Assistant Project Engineer<br />
Richard J. Ereenwood, P.E.<br />
Project Manager<br />
Enc.
LIST OF TABLES<br />
LIST OF FIGURES<br />
LIST OF APPENDICES<br />
1.0 EXECUTIVE SUMMARY<br />
1.1 Introduction<br />
1.2 Site Background<br />
1.3 Implementation<br />
2.0 IMPLEMENTATION<br />
2.1 Mobilization and Site Setup<br />
2.1.1 Mobilization<br />
2.1.2 Site Setup<br />
2.1.3 Daily Records<br />
TABLE OF CONTENTS<br />
2.2 Phase I Demolition and Drum Yard Preparation<br />
2.2.1 Demolition<br />
2.2.2 Additional Excavation and Drum Removal<br />
2.2.3 Utility Protection<br />
2 .2.4 Site Grading and Surface Preparation<br />
2.2.4.1 Soil Excavation<br />
2.2.4.2 Drainage Ditch Excavation<br />
2.2.4.3 Equipment Decontamination<br />
2.2.4.4 Placement of Cover<br />
2.2.4.5 Orphan Drums<br />
2.2.4.6 Preparation of Roll-Off Boxes<br />
PAGE<br />
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TABLE OF CONTENTS<br />
(Cont i nued)<br />
2.3 Removal of Liquids and Sludges<br />
2.3.1 Sludge Tank<br />
2.3.2 Boiler Tank<br />
2.3.3 Sump and Dip Tanks<br />
2.3.4 Worker Protection<br />
2.4 Phase I1 Demo1 ition and Residential Yard Preparation<br />
2.4.1 Demolition<br />
2.4.2 Surface Preparation<br />
2.5 Soil Excavation and Backfill Placement<br />
2.5.1 Site Clearing and Grading<br />
2.5.2 Excavation<br />
2.5.3 Loading, Transportation and Disposal<br />
2.5.4 Backfill Placement<br />
2.6 Cap Construction<br />
Liner Placement<br />
Concrete Placement<br />
Drainage Pipe<br />
Permeable Sand<br />
Geotextile Pi acement<br />
Gravel Placement<br />
Paving of <strong>the</strong> Driveway and Surface Chip Seal<br />
2.7 Fence Reconstruction<br />
2.8 Drum Hand1 ing and Disposal<br />
2.9 Compatibility Testing<br />
2.10 Winterization and Demobilization<br />
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TABLE OF CONTENTS<br />
(Continued)<br />
- PAGE<br />
3.0 TRANSPORTATION PLAN 23<br />
3.1 Introduction 23<br />
3.2 Implementation 23<br />
4.0 SITE AND COMMUNITY HEALTH AND SAFETY 24<br />
4.1 Introduction 24<br />
4.2 Revisions to <strong>the</strong> Health and Safety Plan 24<br />
4.3 Key Personnel and Their Responsibilities 24<br />
4.4 Job Hazard Analysis 26<br />
4.4.1 Physical Hazards 26<br />
4.4.1.1 Noise 27<br />
4.4.1.2 Heat Stress 27<br />
4.4.1.3 Construction Equipment 2 7<br />
4.4.1.4 Uneven Terrain 2 7<br />
4.4.1.5 Unstable Stacking of Containers 28<br />
4.4.1.6 Manual Material Handling 28<br />
4.4.1.7 Confined Spaces 28<br />
4.4.2 Chemical Hazards 28<br />
4.5 Air Monitoring 29<br />
4.5.1 Air Monitoring During Liquid Removal Activities 29<br />
4.5.2 Air Monitoring During Soil Excavation Activities 33<br />
4.5.2.1 Summary of Excavation Activities 33<br />
4.5.2.2 Direct Reading Instrumentation 34<br />
4.5.2.3 Integrated Sample Collection and Analysis 38<br />
4.6 Personal Protective Equipment 39
REFERENCES<br />
TABLES<br />
FIGURES<br />
APPENDIX A<br />
APPENDIX B<br />
APPENDIX C<br />
APPENDIX D<br />
4.7 Decontamination Procedures<br />
TABLE OF CONTENTS<br />
(Continued)<br />
4.7.1 Personal Decontamination<br />
4.7.2 Equipment Decontamination<br />
4.8 General Site Health and Safety and Work Rules<br />
4.9 Training<br />
4.10 Medical Monitoring<br />
4.11 Work Zone and Site Security<br />
4.11.1 Exclusion Area<br />
4.11.2 Decontamination Area<br />
4.11.3 Support Area<br />
4.11.4 Site Security<br />
4.12 Community Health and Safety<br />
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TABLE<br />
NUMBER<br />
LIST OF TABLES<br />
Subcontractor List<br />
Summary of Hazardous Waste Disposal<br />
Employee Air Monitoring Coll ection Summary<br />
Ambient Air Monitoring Collection Summary<br />
Employee Air Monitoring Analytical Results<br />
Ambient Air Monitoring Analytical Results
-<br />
-<br />
LIST OF FIGURES<br />
FIGURE DRAWING<br />
NUMBER NUMBER TITLE<br />
1 87-035-E8 Project Schedule<br />
2 87-035-E5 Phase I Staging and Site Working Area<br />
3 87-035-E6 Phase I1 Staging and Site Working Area<br />
4 87-035-B10 Drum Hand1 i ng Site Plan
APPENDIX A<br />
APPENDIX B<br />
APPENDIX C<br />
APPENDIX D<br />
LIST OF APPENDICES<br />
As-Built Construction Drawings<br />
Test Results for Compliance with<br />
Technical Specifications<br />
Laboratory Test Results<br />
HDPE and Geotextile Fabric Instal 1 ation<br />
Procedures
The goal of <strong>the</strong> ERA was to rapidly reduce and mitigate public and<br />
environmental exposure to potentially harmful contaminants. The California<br />
Department of Health Services (DHS) had determined, based on <strong>the</strong> Public<br />
Health and Environmental Risk Assessment (PHERA), that <strong>the</strong> ERA was<br />
necessary to protect <strong>the</strong> public health and to limit risks of continued<br />
exposure due to potential time delays from <strong>the</strong> Remedial Investigation/<br />
Feasibility Study (RI/FS) and Remedial Planning Process. The objectives of<br />
<strong>the</strong> ERA were <strong>the</strong> following:<br />
1. Reduce potential direct contact of people with contaminated soil<br />
in residential and vacant lots on <strong>the</strong> south and east sides of <strong>the</strong><br />
site and within <strong>the</strong> drum yard;<br />
2. Reduce potential future environmental degradation from<br />
contaminated surface water runoff;<br />
3. Remove contaminated materials, tanks, and drums that might have<br />
presented <strong>the</strong> potential for future off-site contamination or<br />
fur<strong>the</strong>r degradation of <strong>the</strong> environment;<br />
4. Reduce <strong>the</strong> hazard of potentially contaminated airborne dust;<br />
5. Reduce <strong>the</strong> potential for fur<strong>the</strong>r degradation of <strong>the</strong> groundwater<br />
beneath <strong>the</strong> site from infiltration of precipitation or runoff.<br />
1.3 Imolementation<br />
The work required to implement <strong>the</strong> ERAS was performed by Canonie's contract<br />
team or <strong>the</strong>ir subcontractors. A list of subcontractors is provided in<br />
Table 1. The actual progression of activities and <strong>the</strong> schedule for any<br />
remaining activities are provided as Figure 1.
The work performed included nine major components:<br />
1. Mobilization and site setup;<br />
2. Demol i tion and disposal of drums, tanks, miscellaneous scrap<br />
metal, fencing, and debris from <strong>the</strong> drum yard;<br />
3. Excavation, grading, and placement of soil cover within <strong>the</strong> drum<br />
yard;<br />
4. Demol ition and disposal of fencing, sheds, concrete, and o<strong>the</strong>r<br />
miscellaneous debris from <strong>the</strong> residential lots;<br />
5. Excavation and disposal of soil from residential lots;<br />
6. Backfill and compaction of excavated areas;<br />
7. Construction of site cap and construction of surface drain system<br />
and retaining structures;<br />
8. Reconstruction of wood fencing;<br />
9. Winterization of site.<br />
The work was performed under <strong>the</strong> direction and supervision of DHS. During<br />
<strong>the</strong> course of <strong>the</strong> site activities, numerous additional activities were<br />
required to enhance <strong>the</strong> construction work and to fur<strong>the</strong>r protect <strong>the</strong> public<br />
from health risks due to exposure. These additional activities included:<br />
1. Increased levels of personal protective equipment by workers;<br />
2. Removal of buried drums and debris;<br />
3. Excavation of additional contaminated soil ;
4. Additional testing of drums and contaminated soil;<br />
5. Working overtime hours to complete critical work tasks;<br />
6. Mobilization of additional equipment and supplies necessary to<br />
meet <strong>the</strong> additional project requirements;<br />
7. Air monitoring and air sample testing;<br />
8. Construction of additional surface water control and drainage<br />
features.<br />
Although <strong>the</strong> time required to complete <strong>the</strong> work increased due to wea<strong>the</strong>r<br />
conditions and increased work activities, <strong>the</strong> project was completed in a<br />
timely fashion and fulfilled <strong>the</strong> goal and purpose of <strong>the</strong> ERA.
2.0 IMPLEMENTATION<br />
As presented in Section 1.0 of this report, <strong>the</strong> work covered under <strong>the</strong><br />
scope of activities included nine major components. The work required by<br />
<strong>the</strong>se components was carried out in accordance with <strong>the</strong> technical<br />
specifications, <strong>the</strong> procedures outlined in Section 2.0, <strong>the</strong> Transportation<br />
Requirements of Section 3.0, and <strong>the</strong> Health and Safety Requirements of<br />
Section 4.0.<br />
Some of <strong>the</strong> specifications and procedures presented in <strong>the</strong> technical<br />
specifications and work plan were modified as required by field conditions.<br />
These modifications were made after <strong>the</strong> necessity for change was determined<br />
by <strong>the</strong> Construction Superintendent and after approval was given by <strong>the</strong><br />
Project Manager. All modifications were authorized by <strong>the</strong> DHS Project<br />
Officer.<br />
2.1 Mobilization and Site Setuo<br />
2.1.1 Mobilization<br />
Mobilization of personnel, equipment, materials, and supplies was carried<br />
out as was necessary to meet <strong>the</strong> requirements of <strong>the</strong> technical<br />
specifications and included <strong>the</strong> specific items and personnel identified and<br />
presented in <strong>the</strong> work plan and reported in <strong>the</strong> financial reports of <strong>the</strong><br />
project. Mobilization of <strong>the</strong>se items was performed just before use.<br />
Transportation of equipment, materials, and supplies to <strong>the</strong> site was along<br />
<strong>the</strong> local routes specified in Section 3.0 of <strong>the</strong> Work Plan.<br />
Delivery dates and arrivals for equipment, materials, supplies, and<br />
personnel were based upon work progress. Materials and supplies were<br />
stored prior to use within <strong>the</strong> site building in <strong>the</strong> areas indicated on<br />
Figure 2. Equipment was stored within <strong>the</strong> fenced area near <strong>the</strong> work being<br />
performed by that equipment.
2.1.2 Site Setuo<br />
During site setup procedures, portions of <strong>the</strong> fencing within <strong>the</strong><br />
residential lots were removed and temporary fencing was placed at <strong>the</strong><br />
approximate locations shown in Figure 3. In addition, temporary fencing<br />
was placed around <strong>the</strong> perimeter of <strong>the</strong> site and a pedestrian walkway was<br />
constructed outside of <strong>the</strong> primary site security fencing. The excavation<br />
was sealed off from <strong>the</strong> residential lots by using temporary fencing lined<br />
with visquene.<br />
Because of <strong>the</strong> temporary nature of <strong>the</strong> site fencing and <strong>the</strong> risk of public<br />
exposure, full time security was maintained at <strong>the</strong> site. These security<br />
measures were necessary to prevent access to <strong>the</strong> site by non-authorized<br />
personnel and <strong>the</strong>reby reduce public exposure and protect onsite supplies<br />
and equipment.<br />
During setup procedures, <strong>the</strong> office areas within <strong>the</strong> building, areas used<br />
by construction personnel, and areas used for material/supply storage were<br />
cleaned. Cleaning of <strong>the</strong> office consisted of boxing all materials, papers,<br />
and debris for future DHS review. All debris, equipment parts, and tanks<br />
outside <strong>the</strong> office and within <strong>the</strong> area required for storage were moved to<br />
o<strong>the</strong>r portions of <strong>the</strong> building outside <strong>the</strong> storage area. These materials<br />
were handled under <strong>the</strong> same level of protection as presented in Section 4.0<br />
of this report.<br />
During preparation of <strong>the</strong> work plan and during site setup activities, <strong>the</strong><br />
City of San Francisco was contacted for <strong>the</strong> purpose of determining permit<br />
procedures and requirements. Due to <strong>the</strong> nature of <strong>the</strong> work (hazardous<br />
waste removal) normal permit procedures did not apply, and confusion<br />
developed concerning <strong>the</strong> type of permitting that would be required.<br />
Because of <strong>the</strong> permit conditions and requirements, delays to <strong>the</strong> project<br />
and increased work requirements resulted. The changes to <strong>the</strong> schedule are
shown in <strong>the</strong> project schedule (Figure 1). Costs associated with <strong>the</strong>se<br />
activities and remobil ization costs are reflected in <strong>the</strong> project financial<br />
reports.<br />
2.1.3 Dailv Records<br />
A daily record of activities of <strong>the</strong> work performed was prepared and<br />
submitted periodically to <strong>the</strong> DHS Project Officer. The reports gave <strong>the</strong><br />
number and type of personnel, <strong>the</strong> equipment used, and a description of <strong>the</strong><br />
work performed. These forms were available for inspection by <strong>the</strong> DHS<br />
Project Officer between submittals.<br />
2.2 Phase I Demo1 ition and Drum Yard Preoaration<br />
2.2.1 Demolition<br />
This section covers <strong>the</strong> work performed to clear and remove all concrete,<br />
rubble, weeds, debris, timbers, scrap metal, fencing, posts, sheet metal,<br />
gates and drums within <strong>the</strong> drum yard. This work was performed as required<br />
by Sections 02020, 02102, and 01037 of <strong>the</strong> technical specifications or as<br />
described herein.<br />
Prior to implementation of <strong>the</strong> ERAS by Canonie, DHS contacted <strong>the</strong> former<br />
operator of <strong>the</strong> BAD facility and arranged to remove many of <strong>the</strong> drums and<br />
equipment from <strong>the</strong> drum yard area. This work was performed before final<br />
pricing of <strong>the</strong> Canonie work, and reduced costs were reflected in <strong>the</strong><br />
authorized amount in <strong>the</strong> task order.<br />
All material within <strong>the</strong> drum yard with <strong>the</strong> exception of <strong>the</strong> boiler tank and<br />
<strong>the</strong> open-top sludge tank was collected by laborers, operators and a Case<br />
580 backhoe. The backhoe was equipped with a backhoe arm and bucket and a<br />
1 oader bucket.
All materials not resting on <strong>the</strong> ground surface were removed from <strong>the</strong>ir<br />
existing locations with <strong>the</strong> backhoe arm and bucket. The backhoe loader<br />
bucket <strong>the</strong>n picked up <strong>the</strong>se materials and placed <strong>the</strong>m into roll-off boxes.<br />
Materials which could not be picked up with <strong>the</strong> backhoe were picked up by<br />
hand and <strong>the</strong>n loaded into <strong>the</strong> backhoe loader bucket for placement into <strong>the</strong><br />
roll-off boxes. Occasionally, due to <strong>the</strong> size and shape of <strong>the</strong> debris,<br />
hand loading into <strong>the</strong> roll-off boxes was required. After <strong>the</strong>se loading<br />
operations were completed, <strong>the</strong> surface of <strong>the</strong> drum site was scraped with<br />
<strong>the</strong> backhoe bucket and small bulldozer, and small debris and rubble was<br />
collected and loaded into a roll-off box.<br />
All personnel performed <strong>the</strong> demolition work under <strong>the</strong> level of protection<br />
specified in Section 4.7 of this report. Before any activity for debris<br />
removal and site grading, <strong>the</strong> ground surface was moistened to reduce <strong>the</strong><br />
creation of and exposure to dust.<br />
2.2.2 Additional Excavation and Drum Removal<br />
During demo1 ition of <strong>the</strong> wood fencing dividing <strong>the</strong> drum yard and <strong>the</strong> vacant<br />
lot, several drums were uncovered beneath <strong>the</strong> surface of <strong>the</strong> drum yard.<br />
Upon fur<strong>the</strong>r investigation (excavation along <strong>the</strong> fence1 ine) additional<br />
drums were found with capacities of about 30 gallons and filled with fluids<br />
and gravel. These drums were excavated using <strong>the</strong> Case 580 backhoe, placed<br />
in empty 55-gallon drums, and <strong>the</strong>n stored inside <strong>the</strong> building.<br />
During excavation of <strong>the</strong> drums Health and Safety personal protective<br />
equipment was upgraded to Level B protection. In addition to <strong>the</strong> drum<br />
removal, additional contaminated soil within this area was also removed.<br />
2.2.3 Utility Protection<br />
The utilities identified within <strong>the</strong> drum yard were above ground power<br />
poles, <strong>the</strong>ir guide wires, monitoring wells, and an underground gas 1 ine.<br />
During site construction activities, equipment maintained a safe distance
from all power 1 ines, monitoring wells, guy wires, and gas lines. All work<br />
performed near any utilities was done by hand, if it was felt that safe<br />
distances could not be maintained with construction equipment. In<br />
addition, a protective casing made of cinder blocks was placed around <strong>the</strong><br />
monitoring well in <strong>the</strong> vacant lot to prevent damage during fill operations.<br />
During <strong>the</strong> course of <strong>the</strong> work, one gas line not previously located was<br />
uncovered and struck by <strong>the</strong> backhoe bucket. PG&E was notified, and after<br />
an inspection, indicated that no damage to <strong>the</strong> line had occurred.<br />
Accordingly PG&E authorized completion of <strong>the</strong> backfill operation.<br />
2.2.4 Site grad in^ and Surface Preoaration<br />
The site grading and surface preparation within <strong>the</strong> drum yard was performed<br />
concurrent with demolition operations and as was required by Section 02232<br />
of <strong>the</strong> technical specifications or as specified herein. Activities for<br />
site grading included:<br />
o Excavation of soil required to bring <strong>the</strong> existing surface of <strong>the</strong> drum<br />
yard to grade;<br />
o Excavation of drainage ditch areas;<br />
o Equipment decontamination;<br />
o Placement and compaction of three inches of cover material;<br />
o Placement and lining of roll-off boxes.<br />
Subgrade preparation and protection complied with Section 02232,<br />
Subsections 3.1 and 3.3 of <strong>the</strong> technical specifications.<br />
2.2.4.1 Soil Excavation<br />
The excavation of soil in <strong>the</strong> drum yard needed to bring <strong>the</strong> surface to <strong>the</strong><br />
required grade was performed using <strong>the</strong> Case 580 bucket and a CAT D-3<br />
bulldozer (equivalent).
A grid system was established along <strong>the</strong> curbs and <strong>the</strong> building, and <strong>the</strong><br />
surface of <strong>the</strong> yard was surveyed periodically to control elevation<br />
requirements. Surveying was performed after excavation, subgrade<br />
preparation, and backfilling. Excess material over that required to grade<br />
<strong>the</strong> site was stockpiled on <strong>the</strong> surface of <strong>the</strong> drum yard. This stockpiled<br />
material was loaded into trucks during removal of residential soils and in<br />
accordance with <strong>the</strong> procedures presented in Section 2.5 of <strong>the</strong> Work Plan.<br />
Drums containing drill cuttings, which had been transferred from <strong>the</strong> drum<br />
yard to <strong>the</strong> building, were brought back out to <strong>the</strong> stockpile, opened and<br />
dumped into <strong>the</strong> pile. The emptied drums were <strong>the</strong>n carried back into <strong>the</strong><br />
building. The emptied contents were disposed with <strong>the</strong> residential soils.<br />
2.2.4.2 Drainaqe Ditch Excavation<br />
Excavation of <strong>the</strong> drainage ditch areas conformed to Section 2200, and to<br />
<strong>the</strong> As-built Construction Drawings in Appendix A of this implementation<br />
report. The position of <strong>the</strong> ditch along Thomas Street was altered slightly<br />
to accommodate two monitoring wells. This excavation was performed with<br />
<strong>the</strong> backhoe and dozer. Grade was checked and controlled by periodic<br />
surveying.<br />
All materials excavated in <strong>the</strong> drainage ditch area were stockpiled for<br />
disposal along with <strong>the</strong> residential soils. Use of hand tools and labor was<br />
required to protect utilities during construction.<br />
2.2.4.3 Eouipment Decontamination<br />
Equipment used during Phase I work was decontaminated when this equipment<br />
was required to cross between contaminated areas and noncontaminated areas,<br />
and when site grading operations were completed.<br />
The decontamination was performed by placing plastic in an area between <strong>the</strong><br />
contaminated area and <strong>the</strong> noncontaminated area. The equipment was <strong>the</strong>n<br />
driven slowly onto <strong>the</strong> plastic, steam cleaned, and <strong>the</strong>n driven slowly onto<br />
<strong>the</strong> noncontaminated area. The steam cleaning water was allowed to drain
off <strong>the</strong> plastic onto <strong>the</strong> drum yard. This water helped in dust suppression<br />
and contributed to moisture content for compaction. All workers wore<br />
safety glasses, PVC rain pants or polycoated Tyveks, and rubber boots<br />
during steam cleaning operations.<br />
2.2.4.4 Placement of Cover<br />
After <strong>the</strong> site grading and drainage ditch excavation, a three-inch<br />
(compacted thickness) lift of fill material was placed over <strong>the</strong> drum yard.<br />
This cover was graded by Esquivel Grading and Paving and was compacted by<br />
Canonie personnel. The fill was placed to provide a clean surface for<br />
operation of equipment and personnel, to cover any sharp objects or o<strong>the</strong>r<br />
protrusions which might affect <strong>the</strong> performance of <strong>the</strong> liner, and to provide<br />
a roadway surface between <strong>the</strong> vacant lot and <strong>the</strong> drum yard. The cover<br />
material was dumped in <strong>the</strong> vacant lot and <strong>the</strong>n spread with <strong>the</strong> dozer to <strong>the</strong><br />
required thickness. The cover material met <strong>the</strong> specifications for fine<br />
fill of Section 2200, Subsection 2.5 of <strong>the</strong> technical specifications. The<br />
results of compliance testing are provided in Appendix B.<br />
Once <strong>the</strong> cover material had reached <strong>the</strong> drum yard, a test section for<br />
compaction was constructed. The purpose of <strong>the</strong> test section was to verify<br />
that <strong>the</strong> compaction required by Section 02200, Subsection 1.4.1 could be<br />
achieved by compacting <strong>the</strong> cover surface.<br />
2.2.4.5 Orphan Drums<br />
During this phase of implementation, fifteen 55-gallon drums were left in<br />
<strong>the</strong> street outside <strong>the</strong> Hawes Street gate. These drums were brought into<br />
<strong>the</strong> drum yard where <strong>the</strong>y were inspected by <strong>the</strong> DHS Enforcement Division.<br />
The drums were <strong>the</strong>n moved inside <strong>the</strong> building. Samples were taken from <strong>the</strong><br />
drums, tested by Canonie and profiled by CWM, or sent to DHS laboratories.
2.2.4.6 Preoaration of Roll-Off Boxes<br />
The roll-off boxes were lined with 5-mil thick plastic sheets before<br />
placement of any waste materi a1 s.<br />
2.3 Removal of Liauids and Sludqes<br />
To expedite <strong>the</strong> removal process, samples of <strong>the</strong> liquid and sludge materials<br />
for <strong>the</strong> on-site tanks and <strong>the</strong> sump were obtained before implementation of<br />
<strong>the</strong> work plan. The samples were obtained and tested for compatibility and<br />
chemical content. Chemical compatibility testing conformed to <strong>the</strong> testing<br />
requirements as outlined in Section 2.10. Chemical content testing was<br />
performed as required for <strong>the</strong> determination of <strong>the</strong> disposal profile and for<br />
acceptance by <strong>the</strong> Kettleman Hills disposal facility. The results of <strong>the</strong>se<br />
tests are provided in Appendix C.<br />
2.3.1 Sludae Tank<br />
The liquids were removed from <strong>the</strong> sludge tank by being pumped into 55-<br />
gallon drums. After pumping, solids and sludges were removed and placed<br />
into 55-gallon drums using <strong>the</strong> Case 580 backhoe with a twelve-inch bucket.<br />
The outside surface of <strong>the</strong> 55-gallon drums were shea<strong>the</strong>d in plastic so that<br />
this surface would be kept clean. The drums were placed in a berm<br />
constructed of plastic sheeting and absorbant in case spillage occurred.<br />
Residual sol ids were removed by hand excavations. After cleaning, <strong>the</strong> tank<br />
was loaded with yard debris, placed on a flatbed truck, and transported to<br />
<strong>the</strong> Kettleman Hills disposal facility. The tank was picked up by a crane<br />
with steel cables wrapped around each end of <strong>the</strong> tank and connected in <strong>the</strong><br />
middle. The cables were <strong>the</strong>n secured to <strong>the</strong> lifting arm of <strong>the</strong> crane and<br />
<strong>the</strong> tank was lifted onto <strong>the</strong> truck.<br />
2.3.2 Boiler Tank<br />
The 1 iquid from <strong>the</strong> boiler tank was collected into 55-gallon drums. The<br />
liquid was drained through a valve at <strong>the</strong> bottom of <strong>the</strong> tank and into 5-
gallon buckets. These buckets were <strong>the</strong>n emptied into 55-gallon drums.<br />
After <strong>the</strong> liquids from <strong>the</strong> boiler tank had been removed, <strong>the</strong> boiler tank<br />
was lifted onto a truck and transported to Levin Scrap for metal salvage.<br />
2.3.3 Sumo and Dio Tanks<br />
The liquids from <strong>the</strong> sump area and dip tanks (inside <strong>the</strong> building) were<br />
removed in <strong>the</strong> same way as liquids from <strong>the</strong> sludge tank.<br />
2.3.4 Worker Protection<br />
During liquid removal operations and cleaning of <strong>the</strong> inside<br />
materials/supply storage areas and sump areas, all workers wore protection<br />
equipment as required by Section 4.7 of this report. In addition, all work<br />
was performed under <strong>the</strong> direction of a construction supervisor with<br />
demonstrated experience in similar operations.<br />
2.4 Phase I1 Demo1 ition and Residential Yard Preoaration<br />
2.4.1 Demolition<br />
This section covers <strong>the</strong> work that was required to clear and remove all<br />
concrete rubble, weeds, debris, timbers, scrap metal, fencing, posts,<br />
trees, shrubs, and <strong>the</strong> structure (woodshed) within <strong>the</strong> work area. This<br />
work was performed as required by Sections 02020, 02102, and 01037 of <strong>the</strong><br />
technical specifications or as described herein.<br />
All material within <strong>the</strong> residential lots was handled or o<strong>the</strong>rwise collected<br />
using laborers, operators and a Case 580 backhoe. The backhoe was equipped<br />
with a backhoe arm and bucket and a loader bucket.<br />
All materials not resting on <strong>the</strong> ground surface, with <strong>the</strong> exception of <strong>the</strong><br />
trees, shrubs, and weeds, were removed from <strong>the</strong>ir existing location by <strong>the</strong><br />
backhoe arm. The material was <strong>the</strong>n picked up by hand and loaded into <strong>the</strong><br />
loader bucket. The backhoe <strong>the</strong>n transported <strong>the</strong> materials to <strong>the</strong> roll-off
ox marked "nonhazardous materials" (prepared according to Section 2.2.3).<br />
Any materials that were stained or o<strong>the</strong>rwise considered hazardous were<br />
separated from nonhazardous materials and loaded into roll-off boxes marked<br />
as "hazardous materials. " Table 2 provides a summary of <strong>the</strong> hazardous<br />
materials which were transported off-site.<br />
Trees and shrubs were cut flush with <strong>the</strong> ground surface, loaded into <strong>the</strong><br />
loader bucket, and placed into <strong>the</strong> nonhazardous roll -off boxes. All<br />
personnel performed <strong>the</strong> demo1 i tion work under levels of protection required<br />
by Section 4.7. Before performing any activities during debris removal and<br />
excavation operations, <strong>the</strong> surface of <strong>the</strong> ground was moistened to reduce<br />
creation of and exposure to dust.<br />
2.4.2 Surface Preoaration<br />
After demolition operations, a three-inch lift of fill material was placed<br />
by Canonie and graded by Esquivel Grading and Paving over <strong>the</strong> drum yard<br />
surface. The material was placed to provide a clean surface for operation<br />
of equipment and personnel. An additional thickness of fill was placed as<br />
required to produce a level surface for operation of excavation equipment.<br />
The cover material was dumped in <strong>the</strong> vacant lot and spread by <strong>the</strong> bulldozer<br />
until <strong>the</strong> required thickness and a level surface were achieved. The<br />
surface of <strong>the</strong> fill was compacted only as necessary to allow operation of<br />
equipment over <strong>the</strong> surface.<br />
2.5 Soil Excavation and Backfill Placement<br />
2.5.1 Site Clearinq and Gradinq<br />
Site clearing and grading was performed before excavation ofdesignated<br />
soils with procedures similar to those outlined in Section 2.2. This work<br />
was performed using equipment and personnel as presented in Section 5.0 of<br />
<strong>the</strong> Work Plan or as shown in <strong>the</strong> project financial reports.
2.5.2 Excavation<br />
The excavation of designated soils and buried debris was performed to meet<br />
<strong>the</strong> requirements of Section 02200, Subsection 3.1 of <strong>the</strong> technical<br />
specifications, or as specified herein. Equipment used to perform <strong>the</strong> work<br />
is listed in Section 5.0 of <strong>the</strong> Work Plan and/or in <strong>the</strong> project financial<br />
reports, and as is outlined in this section. The soil was excavated and<br />
placed directly into waiting dump trucks and transported to <strong>the</strong> disposal<br />
facility along <strong>the</strong> route presented in Section 3.0. Soils were dampened as<br />
necessary to reduce <strong>the</strong> potential for exposure to dust particles during<br />
excavation operations.<br />
Cut slopes within <strong>the</strong> excavated areas were maintained at slopes no steeper<br />
than 1H:lV or as was required by safety and as designated by <strong>the</strong> on-site<br />
engineer and approved by <strong>the</strong> site Health and Safety Officer.<br />
The excavation began in Yard 3. To prevent spillage, <strong>the</strong> backhoe excavated<br />
<strong>the</strong> soil keeping <strong>the</strong> bucket not more than three-quarters full of soil. The<br />
backhoe rotated in a counter clockwise direction (toward <strong>the</strong> drum yard) and<br />
placed <strong>the</strong> material in <strong>the</strong> truck.<br />
The truck was backed up directly beside <strong>the</strong> backhoe to limit <strong>the</strong> distance<br />
<strong>the</strong> material was carried before placement. Once <strong>the</strong> truck was loaded, <strong>the</strong><br />
plastic 1 iner (placed in <strong>the</strong> truck before loading) was folded over <strong>the</strong><br />
material and securely tied down. The truck would <strong>the</strong>n leave <strong>the</strong> area<br />
through <strong>the</strong> drum yard as shown on Figure 3.<br />
The excavation proceeded away from Yard 3. When <strong>the</strong>re was no longer enough<br />
room for <strong>the</strong> trucks to maneuver behind <strong>the</strong> backhoe, <strong>the</strong> trucks entered by<br />
<strong>the</strong> Hawes Street entrance and parked alongside <strong>the</strong> backhoe as shown on<br />
Figure 3. When <strong>the</strong> backhoe reached <strong>the</strong> edge of <strong>the</strong> building, it turned and<br />
proceeded into <strong>the</strong> vacant lot. Any areas of contaminated soil which could<br />
not be excavated with <strong>the</strong> backhoe were removed by hand.
After <strong>the</strong> excavation had been completed, <strong>the</strong> bucket areas of <strong>the</strong> backhoe<br />
arm that came in contact with <strong>the</strong> contaminated soil were steam cleaned over<br />
a plastic berm. This rinsate was collected in a 55-gallon drum. Air<br />
monitoring was performed prior to and during <strong>the</strong> excavation operation. The<br />
procedures and results of <strong>the</strong> air monitoring are provided in Section 4.5.<br />
2.5.3 Loadinq. Transoortation and Disoosal<br />
Excavated soil was loaded directly into waiting dump trucks (as described<br />
in Section 2.5.2) for transportation to <strong>the</strong> disposal facility. The<br />
equipment and personnel used to perform <strong>the</strong>se tasks were as provided for in<br />
Section 5.0 of <strong>the</strong> Work Plan and/or listed in <strong>the</strong> project financial<br />
reports. Transportation of loaded soils was carried out in accordance with<br />
<strong>the</strong> transportation plan provided in Section 3.0 of <strong>the</strong> Work Plan.<br />
During <strong>the</strong> excavation activities, <strong>the</strong> presence of vinyl chloride was<br />
suspected because of air monitoring results. Increased Health and Safety<br />
precautions, project standby time, and o<strong>the</strong>r delays resulted during <strong>the</strong><br />
period that <strong>the</strong> presence or absence of vinyl chloride was being evaluated.<br />
The procedures and results of <strong>the</strong> air monitoring for vinyl chloride are<br />
presented in Section 4.5.<br />
Laboratory analyses on <strong>the</strong> soils for determination of vinyl chloride are<br />
provided in Appendix C.<br />
2.5.4 Backfill Placement<br />
Backfill operations were performed as required by Section 02200 of <strong>the</strong><br />
technical specifications or as described herein.<br />
Backfilling began in <strong>the</strong> vacant lot, where <strong>the</strong> deep PCB pit was first<br />
brought up to <strong>the</strong> same grade as <strong>the</strong> excavation in <strong>the</strong> residential lot.<br />
Backfill soil in <strong>the</strong> vacant lot was placed in 8-inch thick lifts and
compacted with <strong>the</strong> backhoe bucket and by wheel rolling. Compaction near<br />
foundations and monitoring wells was performed with a hand-held Wacker<br />
rammer-type compactor.<br />
From <strong>the</strong> vacant lot <strong>the</strong> backfill operations proceeded into Yard #1, and<br />
<strong>the</strong>n into Yards #2 and #3. The backfill soil was pushed in front of <strong>the</strong><br />
backhoe so that <strong>the</strong> backhoe was only in contact with <strong>the</strong> clean imported<br />
soil .<br />
In <strong>the</strong> vacant lot and in <strong>the</strong> residential lots, <strong>the</strong> backfill soil below a<br />
depth of two feet from finish grade was common fill, as described in<br />
Section 02200, Subsection 2.4. Between <strong>the</strong> depths of 1 foot and 2 feet,<br />
<strong>the</strong> backfill soil was topsoil as described in Section 02200, Subsection<br />
2.1, compacted by wheel rolling. At depths from finish grade to 1 foot,<br />
<strong>the</strong> backfill was uncompacted topsoil.<br />
The trench separating <strong>the</strong> vacant lot from <strong>the</strong> drumyard was backfilled using<br />
common fill. This soil was placed in 12-inch lifts and was compacted by<br />
using <strong>the</strong> backhoe bucket and by wheel rolling.<br />
2.6 Cao Construction<br />
The placement of <strong>the</strong> HDPE Syn<strong>the</strong>tic Membrane was performed as required by<br />
Sections 02200, 02232, 02400, 03300, and 07114 of <strong>the</strong> technical<br />
specifications except that <strong>the</strong> precleaning of <strong>the</strong> existing concrete slab<br />
and sump areas was performed before final site grading and cap placement.<br />
The concrete slab shown in Figure 2 was scraped with <strong>the</strong> Case 580 backhoe<br />
and was <strong>the</strong>n steam cleaned. Steam cleaning water was allowed to flow onto<br />
<strong>the</strong> ground surface.<br />
2.6.1 Liner Placement<br />
The syn<strong>the</strong>tic 1 iner was supplied and <strong>the</strong> instal lation supervised by Nilex<br />
USA, Inc. All submittals required by Section 07114, Subsection 1.5 and
1.6, Section 07115, Subsection 1.4 and 1.5, specific methodology for liner<br />
placement field scanning, and placement of boots for monitoring wells,<br />
telephone poles, guide wires, fence posts, and o<strong>the</strong>r structures penetrating<br />
<strong>the</strong> liner were prepared by Canonie with cooperation and information from<br />
Nilex. This information was submitted to DHS two weeks before liner<br />
installation and is included as Appendix D.<br />
Upon delivery, <strong>the</strong> HDPE liner was stored in <strong>the</strong> area shown on Figure 4.<br />
When it was determined that <strong>the</strong> drum yard subgrade was completed, <strong>the</strong> liner<br />
was removed from <strong>the</strong> storage area and placed onto <strong>the</strong> drum yard using an<br />
extended arm crane. The 1 iner was rolled out and placed into position by<br />
laborers. A Nilex field technician <strong>the</strong>n fused <strong>the</strong> sheets of HDPE toge<strong>the</strong>r<br />
as per <strong>the</strong> working details that Nilex had provided. Nilex suggested that a<br />
better seal around <strong>the</strong> monitoring wells could be achieved if <strong>the</strong> concrete<br />
utility boxes were replaced with sono tubes. This would allow <strong>the</strong><br />
performed pipe boots to be used instead of using a field weld. This method<br />
was determined to be acceptable by Canonie, DHS, and CH2M HILL so long as<br />
<strong>the</strong> utility boxes were replaced and accessiblity to <strong>the</strong> monitoring wells<br />
maintained. Plans were made for utility box replacement so that <strong>the</strong> sono<br />
tubes could be used.<br />
Field vacuum testing and laboratory destructive testing of <strong>the</strong> liner seams<br />
were performed. Any seams that proved to be inadequately welded were re-<br />
welded and tested again to insure <strong>the</strong>ir integrity.<br />
2.6.2 Concrete Placement<br />
The placement of <strong>the</strong> concrete curb and catch basin conformed to Section<br />
03300 of <strong>the</strong> Construction Specifications and as is shown on <strong>the</strong><br />
construction drawings. The concrete curb was placed and allowed to cure<br />
five days before placement of final subsurface cover material and HDPE<br />
liner. The existing curb around <strong>the</strong> sump was removed and <strong>the</strong> sump<br />
backfilled with concrete so that <strong>the</strong> newly constructed curb could be<br />
extended over <strong>the</strong> sump. After <strong>the</strong> curb had been cured, <strong>the</strong> HDPE liner was<br />
fastened to <strong>the</strong> curb with Hilti concrete anchorages.
The concrete catch basin was purchased from <strong>the</strong> Santa Rosa Cast Products<br />
Company. The catch basin was installed after <strong>the</strong> placement of <strong>the</strong> liner.<br />
Tommy Lee of <strong>the</strong> San Francisco Department of Public Works (SFDPW) was<br />
present during <strong>the</strong> placement of <strong>the</strong> basin and approved <strong>the</strong> basin connection<br />
to <strong>the</strong> city sewer system.<br />
2.6.3 Drainaqe Pioe<br />
The drainage pipe was installed after completion of <strong>the</strong> liner installation.<br />
All pipe was installed as required by <strong>the</strong> construction drawings and<br />
according to Section 02400 of <strong>the</strong> technical specifications, except for <strong>the</strong><br />
length of pipe running parallel to Thomas Street. Because of <strong>the</strong> position<br />
of <strong>the</strong> monitoring wells, this section of pipe was positioned five feet from<br />
<strong>the</strong> curb instead of <strong>the</strong> three feet as originally provided by <strong>the</strong> plans.<br />
2.6.4 Permeable Sand<br />
Samples of <strong>the</strong> sand required for placement above <strong>the</strong> liner were obtained<br />
and tested as required by Section 02200 of <strong>the</strong> technical specifications.<br />
The results of <strong>the</strong>se tests were provided to DHS before delivery of <strong>the</strong> sand<br />
to <strong>the</strong> site and are included in Appendix B.<br />
The sand was end-dumped in <strong>the</strong> vacant lot and spread (full thickness) with<br />
<strong>the</strong> backhoe. The sand was completely spread over <strong>the</strong> liner but compaction<br />
was not completed until winter rains had subsided and <strong>the</strong> sand had dried.<br />
After <strong>the</strong> sand had dried sufficiently, <strong>the</strong> grade was checked and some<br />
additional sand was added and distributed with a Bobcat where needed.<br />
Compaction of <strong>the</strong> sand was performed with hand-held vibrating plate<br />
compactors. Water was added as necessary to achieve <strong>the</strong> compaction<br />
required.<br />
In order to prevent subgrade ponding at <strong>the</strong> drain inlet prior to <strong>the</strong><br />
completion of <strong>the</strong> cap seal coat, holes were drilled into <strong>the</strong> side of <strong>the</strong><br />
drain box beneath <strong>the</strong> drain box inlet and above <strong>the</strong> syn<strong>the</strong>tic membrane.
2.6.5 Geotextile Placement<br />
Geotextile fabric was placed as required by Section 07115 of <strong>the</strong> technical<br />
specifications and as described herein. Correspondence from <strong>the</strong><br />
manufacturer provided additional instructions regarding storage, handling<br />
and installation, and is included in Appendix D (James M. Cramer, Vice<br />
President, Nilex USA Inc., California Branch, letter dated February 13,<br />
1988). Following <strong>the</strong> manufacturer's instructions, <strong>the</strong> seams of <strong>the</strong><br />
geotextile were not bonded, but were overlapped two feet to provide proper<br />
continuity of <strong>the</strong> fabric.<br />
2.6.6 Gravel Placement<br />
The Class 2 aggregate base layer for <strong>the</strong> top 6 inches of <strong>the</strong> cap was placed<br />
as required by Section 02200 of <strong>the</strong> technical specifications. The<br />
aggregate was dumped and spread with a Massey Ferguson loader and compacted<br />
with a Bomag 100 roller. Moisture was added as required to achieve proper<br />
compaction. The base was spread and compacted so that <strong>the</strong> trucks always<br />
ran over <strong>the</strong> compacted base and did not disturb <strong>the</strong> liner. Compaction<br />
around <strong>the</strong> wells, fence tubes and Christy boxes was achieved with a hand-<br />
held Wacker rammer-type compactor.<br />
2.6.7 Pavinq of <strong>the</strong> Drivewav and Surface chi^ Seal<br />
Paving of <strong>the</strong> driveway and installation of <strong>the</strong> chip seal coating on <strong>the</strong> cap<br />
was performed as required by Sections 02510 and 02605 of <strong>the</strong> technical<br />
specifications. Inspection of <strong>the</strong> site after rainfall indicated that<br />
drainage from <strong>the</strong> site was working effectively and no ponding was evident.<br />
Some additional work was performed to protect <strong>the</strong> DHS monitoring wells on<br />
site and provide ease of access to <strong>the</strong>se wells. Christy boxes were<br />
installed around five monitoring wells within <strong>the</strong> cap area, flush with <strong>the</strong><br />
final grade. Structural concrete was used to cement inside <strong>the</strong> box and<br />
bring <strong>the</strong> well grout back up to final grade.
O<strong>the</strong>r additional work was performed to control drainage and prevent surface<br />
runoff from getting under <strong>the</strong> liner at <strong>the</strong> edge of <strong>the</strong> drum yard. Asphalt<br />
concrete berms were installed at several locations. These included <strong>the</strong><br />
following: adjacent to <strong>the</strong> Bay Area Drum and machine shop/plating shop<br />
buildings; across <strong>the</strong> former driveway and across <strong>the</strong> asphalt walkways by<br />
<strong>the</strong> building and machine shop; and between <strong>the</strong> drum yard and <strong>the</strong> vacant<br />
1 ot.<br />
2.7 Fence Reconstruction<br />
Because of rain delays, only Phase I of <strong>the</strong> fence reconstruction was<br />
performed. Phase I reconstruction included replacing <strong>the</strong> fences in <strong>the</strong><br />
residential lots and placing <strong>the</strong> sono tubes in <strong>the</strong> drum yard area. This<br />
work was performed after placement of <strong>the</strong> three inches of cover over <strong>the</strong><br />
drum yard and <strong>the</strong> excavation and backfilling of <strong>the</strong> residential lots.<br />
Phase I fencing was provided and installed by With Fencing, Inc. according<br />
to Section 02445 of <strong>the</strong> technical specifications.<br />
Sono tubes were placed using a hand auger or <strong>the</strong> Case 580 backhoe.<br />
Excavated soils were collected and disposed of with <strong>the</strong> residential soils.<br />
The excavated area around each sono tube was backfilled with fine soil and<br />
compacted with a hand-held Wacker rammer-type compactor.<br />
Final permanent fencing work is expected to be completed in <strong>the</strong> near<br />
future.<br />
2.8 Drum Handlina and Disoosal<br />
Drum handling and disposal will be performed at a later I date.<br />
2.9 Comoatibilitv Testinq<br />
Compatibility testing will be performed at a later date.
2.10 Winterization and Demobilization<br />
Winterization of <strong>the</strong> site was performed to prevent rain damage to <strong>the</strong> site<br />
during <strong>the</strong> seasonal rains.<br />
Site winterization consisted of sealing <strong>the</strong> site against rainwater<br />
infiltration, securing <strong>the</strong> site against outside intrusion, and removing<br />
rainwater that had collected in <strong>the</strong> building.<br />
To protect <strong>the</strong> site from rain, visquene was placed over <strong>the</strong> street curb to<br />
liner joint, <strong>the</strong> HDPE liner was completely covered with sand, <strong>the</strong> sono<br />
tubes were sealed with visquene and duct tape, and plywood was propped over<br />
<strong>the</strong> gap between <strong>the</strong> building and <strong>the</strong> concrete containment curb.<br />
The site perimeter was secured by placing temporary fencing along <strong>the</strong><br />
backyard of <strong>the</strong> Madison residence, by wiring shut <strong>the</strong> gap in <strong>the</strong> Shafter<br />
Street access gate, and by securely locking all site doors and gates.<br />
Samples of water were collected from <strong>the</strong> drum storage area inside <strong>the</strong><br />
building and sent to DHS laboratories for chemical analyses. These results<br />
have been forwarded to Tommy Lee of <strong>the</strong> SFDPW. A temporary sump pump has<br />
been placed in <strong>the</strong> drum storage area, and Mr. Lee has approved <strong>the</strong><br />
discharge of any water collected into <strong>the</strong> city sewer system.
3.1 Introduction<br />
3.0 TRANSPORTATION PLAN<br />
The transportation phase of <strong>the</strong> Bay Area Drum ERA was critical in that it<br />
represented <strong>the</strong> portion of <strong>the</strong> project which had, although limited, <strong>the</strong><br />
greatest potential for public exposure outside of <strong>the</strong> immediate project<br />
area. Therefore, Canonie had developed a plan for loading and<br />
transportation of <strong>the</strong> hazardous waste to <strong>the</strong> Kettleman Hills disposal<br />
facility with <strong>the</strong> assistance of Chemical Waste Management, Enrac Division<br />
(CWM) and DHS. In <strong>the</strong> development of this plan, Canonie had considered<br />
issues of personnel and pub1 ic safety, regulatory compliance, and<br />
operational efficiency. The plan was presented in Section 3.0 of <strong>the</strong> Work<br />
Plan.<br />
3.2 Imolementation<br />
During implementation of <strong>the</strong> ERA for Bay Area Drum, <strong>the</strong> transportation plan<br />
was followed. No spill or need for emergency response occurred during <strong>the</strong><br />
performance of <strong>the</strong> work.
4.1 Introduction<br />
4.0 SITE AND COMMUNITY HEALTH AND SAFETY<br />
The work performed in implementing <strong>the</strong> Health and Safety Plan was designed<br />
as a practical approach to accomplishing <strong>the</strong> ERA activities considering <strong>the</strong><br />
occupational and public health hazards anticipated at <strong>the</strong> site. The Health<br />
and Safety procedures applied to all site activities carried out under <strong>the</strong><br />
Expedited Response Action (ERA) at <strong>the</strong> BAD site.<br />
All on-si te personnel, enforcement agency personnel, and visitors were<br />
required to familiarize <strong>the</strong>mselves with and comply with provisions of <strong>the</strong><br />
Health and Safety Plan. Canonie provided health and safety equipment for<br />
Canonie employees and subcontractors. All o<strong>the</strong>r personnel provided equal<br />
or greater levels of protection for <strong>the</strong>mselves.<br />
4.2 Revisions to <strong>the</strong> Health and Safety Plan<br />
Because conditions varied, <strong>the</strong> original plan presented in Section 4.0 of<br />
<strong>the</strong> work plan was upgraded and downgraded, as appropriate, depending on<br />
site conditions. All changes to <strong>the</strong> Health and Safety Plan were determined<br />
or approved by <strong>the</strong> site Health and Safety Officer and discussed with <strong>the</strong><br />
Project Officer.<br />
4.3 Kev Personnel and Their Res~onsi bil ities<br />
The following list names <strong>the</strong> key personnel who were assigned to <strong>the</strong> project<br />
for implementation of <strong>the</strong> ERA. Details of <strong>the</strong>ir experience and technical<br />
levels were provided in Appendix C of <strong>the</strong> work plan. Additional personnel<br />
required to implement <strong>the</strong> ERA were determined after approval of <strong>the</strong> work<br />
plan and pricing proposal and before performance of <strong>the</strong> work required by<br />
such personnel.
1. Richard J. Greenwood, P.E.: Mr. Greenwood was <strong>the</strong> Canonie project<br />
manager; he was responsible for <strong>the</strong> overall project management<br />
including <strong>the</strong> Health and Safety Plan.<br />
2. Jack Isley: Mr. Isley was <strong>the</strong> project construction manager and<br />
was responsible for technical assistance during handling of<br />
hazardous materi a1 s.<br />
3. Keith Pushaw: Mr. Pushaw was <strong>the</strong> project construction<br />
superintendent and was responsible for review of profiling and<br />
disposal procedures and for verification of all work in accordance<br />
with state and Federal requirements for disposal of hazardous<br />
wastes. Mr. Pushaw was also responsible for preparation and<br />
review of drum handling and compatibility testing procedures.<br />
4. Arlen Saxton: Mr. Saxton was <strong>the</strong> project construction supervisor<br />
and was responsible for on-site activities including handling of<br />
hazardous materials; he was directly responsible for personnel<br />
compliance with <strong>the</strong> Health and Safety Plan; Mr. Saxton is<br />
certified in first aid and CPR and was designated as agent to<br />
notify paramedics and <strong>the</strong> fire department in <strong>the</strong> event of an<br />
emergency.<br />
5. Brian Hickam and Mike Endicott: Mr. Hickam and Mr. Endicott were<br />
<strong>the</strong> project construction foremen. They were responsible for<br />
assisting <strong>the</strong> project work, for directing project laborers, and<br />
for taking over <strong>the</strong> responsibilities of <strong>the</strong> project supervisor in<br />
<strong>the</strong> event that Mr. Saxton was not available.<br />
6. Michael Strebeck: Mr. Strebeck is a Level 3 professional and<br />
assisted in <strong>the</strong> project during <strong>the</strong> course of <strong>the</strong> work. Mr.<br />
Strebeck's responsibilities were to act as <strong>the</strong> agent for <strong>the</strong><br />
project manager in <strong>the</strong> event that <strong>the</strong> project manager was not<br />
available.
James Babcock: Mr. Babcock is a Level 4 professional and assisted<br />
in <strong>the</strong> project during winterization activities and completion of<br />
<strong>the</strong> site cap. Mr. Babcock's responsibilities were to act as <strong>the</strong><br />
agent for <strong>the</strong> project manager in <strong>the</strong> event that <strong>the</strong> project<br />
manager was not available.<br />
Susan Walker: Certified Industrial Hygienist (CIH) : Ms. Walker<br />
was <strong>the</strong> site Health and Safety Officer; she was responsible for<br />
implementation and management of <strong>the</strong> site Health and Safety Plan.<br />
Kurt Ahlich: Mr. Ahlich was responsible for on-site quality<br />
control, maintaining site records, and engineering activities<br />
required during field activities.<br />
Albert Elizondo: Mr. Elizondo is a Level 2 professional and<br />
assisted in <strong>the</strong> project during winterization activities and<br />
completion of <strong>the</strong> cap. Mr. Elizondo's responsibilities were to<br />
assist in completion of <strong>the</strong> work and assist Mr. Ahlich in his<br />
responsibilities.<br />
Michael Klein: Mr. Klein is a Level 1 professional and assisted<br />
in <strong>the</strong> project during <strong>the</strong> course of <strong>the</strong> work. Mr. Klein's<br />
responsibilities were to assist Mr. Ahlich in his<br />
responsibilities.<br />
4.4 ~ o Hazard b Analysis<br />
4.4.1 Phvsical Hazards<br />
The major physical hazards at <strong>the</strong> site included <strong>the</strong> following:<br />
1. Noise<br />
2. Potential heat stress<br />
3. Construction equipment<br />
4. Uneven terrain
5. Unstable stacking of containers (inside building)<br />
6. Manual material handl ing<br />
7. Drum handl ing<br />
8. Drum overpacking operations<br />
9. Potential exposure to vinyl chloride<br />
4.4.1.1 Noise<br />
Where excessive noise was encountered, employees were provided with E.A.R.<br />
ear plugs.<br />
4.4.1.2 Heat Stress<br />
All on-site personnel were instructed in <strong>the</strong> symptoms of heat stress.<br />
Where site conditions warranted, <strong>the</strong> site Health and Safety Officer<br />
monitored for heat stress. Potable water was available on-site, and<br />
Gatorade was provided as needed.<br />
4.4.1.3 Construction Eouioment<br />
Trucks, excavation equipment, and drum handl ing equipment were issued at<br />
<strong>the</strong> site. On-site personnel were made aware of <strong>the</strong> presence of this<br />
equipment. All personnel operating such equipment were made aware of <strong>the</strong><br />
presence of o<strong>the</strong>r site personnel. Backup alarms and roll -over protection<br />
were used, as appropriate. The excavation area was examined by a utilities<br />
locator.<br />
Personnel operating construction equipment were experienced in <strong>the</strong><br />
operation of such equipment and continuous supervision was provided during<br />
<strong>the</strong> operation of that equipment.<br />
4.4.1.4 Uneven Terrain<br />
All open excavations and ground openings were protected from inadvertent<br />
entry. Any openings left open overnight were barricaded and covered to
prevent entry by off-site personnel. Security guards were provided during<br />
off-hours to prevent entry by off-si te personnel.<br />
4.4.1.5 Unstable Stackinq of Containers<br />
Drums were stacked inside <strong>the</strong> building. All employees were warned to<br />
approach <strong>the</strong>se areas with caution. No one was permitted to walk or climb<br />
on drums. Any obviously unstable drums were restacked or o<strong>the</strong>rwise moved<br />
to eliminate <strong>the</strong> potential of falling.<br />
4.4.1.6 Manual Material Handling<br />
Wherever possible, material handling was done mechanically. Fork1 ift<br />
trucks for drum handling were used on-site. Where manual handling was<br />
necessary, personnel were instructed in techniques of safe handling.<br />
4.4.1.7 Confined Soaces<br />
The drainage sump, sludge tank, dip tanks, and boiler tank were pumped<br />
and/or cleaned during site activities. Entry into sump, sludge tank, dip<br />
tanks, or boiler tank was required during cleaning. Confined space entry<br />
and monitoring procedures were implemented during <strong>the</strong>se activities, as<br />
described in Section 4.5.<br />
4.4.2 Chemical Hazards<br />
Chemical hazards were encountered during <strong>the</strong> excavation activities and in<br />
handling unknown materials found in containers on-site. The drum yard<br />
soils were considered to be contaminated to varying degrees. All personnel<br />
wore steel toed neoprene boots while working in <strong>the</strong> yard. Kneeling and/or<br />
sitting directly on <strong>the</strong> ground was prohibited. Special procedures,<br />
including air monitoring and upgrading of health and safety protection<br />
levels, were implemented during excavating, cleaning and drum hand1 ing<br />
activities.
4.5 Air Monitoring<br />
4.5.1 Air Monitorinq Durinq Liquid Removal Activities<br />
The air monitoring at Bay Area Drum consisted of organic vapor<br />
concentration determination using an organic vapor analyzer (OVA).<br />
Monitoring was done at <strong>the</strong> beginning of each work activity to evaluate<br />
potential exposure levels. The chemical constituents of <strong>the</strong> liquids to be<br />
removed had previously been identified as styrene, methylene chloride, and<br />
C3benzene.<br />
Styrene has a threshold limit value of 50 ppm for an eight-hour time<br />
weighted average. The threshold limit value for methylene chloride is<br />
being lowered to 50 ppm, and it is considered a suspect carcinogen.<br />
C3benzene has not had a threshold limit value established by <strong>the</strong> American<br />
Conference of Governmental Industrial Hygienists. None of <strong>the</strong>se compounds<br />
are readily absorbed through <strong>the</strong> skin.<br />
Work at <strong>the</strong> Bay Area Drum facility was initiated on August 20, 1987. The<br />
OVA was calibrated using zero hydrocarbon air and methane in air at 6.7<br />
ppm. The background readings obtained outside <strong>the</strong> fence and upwind of <strong>the</strong><br />
site indicated 3.6 ppm.<br />
The first activity, pumping <strong>the</strong> liquids from <strong>the</strong> open tank, was monitored.<br />
The personal protective equipment worn by <strong>the</strong> employees was Level C with<br />
full face Scott respirators, chemical-resistant gloves (inner and outer),<br />
polytyveks, and rubber boots. The OVA readings during this activity were<br />
as follows:<br />
Pum~inq Tank<br />
Outside plastic sheet 3.6<br />
Above drum 70<br />
Above tank 20
Later in <strong>the</strong> day <strong>the</strong> OVA was re-calibrated and background established at<br />
1.6 ppm. The next activity was <strong>the</strong> pumping of <strong>the</strong> sump. The same level of<br />
protection, previously noted, was utilized by <strong>the</strong> employees. The OVA<br />
readings during this activity were as follows:<br />
Pumoinq sum^<br />
Top of sump<br />
Above drum<br />
Concentration (om)<br />
The next activity to be monitored involved <strong>the</strong> shoveling of <strong>the</strong> sludge in<br />
<strong>the</strong> sump. Re-calibration of <strong>the</strong> OVA was not possible due to a low battery.<br />
All activity was stopped and postponed until <strong>the</strong> next day.<br />
On August 21, 1987, <strong>the</strong> work activity centered on <strong>the</strong> shoveling and steam<br />
cleaning of <strong>the</strong> sump. The level of protection utilized was Level C. The<br />
OVA was calibrated and <strong>the</strong> background level established at 2.5 ppm. All<br />
employees noted an odor through <strong>the</strong>ir respirator at <strong>the</strong> beginning of <strong>the</strong><br />
shoveling activity. Re-adjustment of <strong>the</strong> respirator face piece alleviated<br />
<strong>the</strong> problem. The OVA readings during <strong>the</strong> day were as follows:<br />
40<br />
3.0<br />
Shovelinq Sumo Concentration (porn1<br />
Top of sump 4.2<br />
Shovel ing to bucket 2 5<br />
Bucket transfer to drum 82<br />
Removing motor 11<br />
Sludge trap inside 70<br />
Steam Cleanins Sumo Concentration (oomr<br />
Inside trap 150<br />
Outside 40<br />
Due to <strong>the</strong> extremely high moisture content in <strong>the</strong> air during <strong>the</strong> steam<br />
cleaning operation, <strong>the</strong> OVA readings are not considered val id.
On August 24, 1987, <strong>the</strong> removal of <strong>the</strong> sludge from open tank was begun. A<br />
backhoe with a small bucket attachment was utilized to fill <strong>the</strong> drums. The<br />
OVA was calibrated and background was established at 2.0 ppm. The<br />
protection levels initially were set for <strong>the</strong> employee guiding <strong>the</strong> sludge<br />
from <strong>the</strong> backhoe bucket to <strong>the</strong> drums at Level B with an airline respirator,<br />
polytyveks, chemical-resistant gloves (inner and outer), and rubber boots.<br />
The o<strong>the</strong>r employees were at Level C with a full face respirator. The OVA<br />
readings during this activity were as follows:<br />
Cleaninq Tank Concentration (om)<br />
Above tank 4.2<br />
Above tank after breaking<br />
sludge crust 400<br />
Inside barrel berm-top of<br />
barrel 70-150<br />
Backhoe operator seat 4.2<br />
Outside barrel berm 5.0<br />
Following this evaluation, <strong>the</strong> protection levels for <strong>the</strong> backhoe operator,<br />
forklift operator, and <strong>the</strong> barrel steam cleaner were downgraded to a<br />
modified Level D with polytyveks, rubber boots, chemical -resi stant gloves<br />
(inner and outer), and a hardhat with faceshield. The employee guiding <strong>the</strong><br />
sludge from <strong>the</strong> backhoe bucket to <strong>the</strong> drums remained at Level B.<br />
Additional OVA readings were obtained throughout <strong>the</strong> day and <strong>the</strong> ranges<br />
obtained were as follows:<br />
Cleaninq Tank Concentration ( om1<br />
Above tank 400-500<br />
Inside barrel berm-top of<br />
barrel 50-150<br />
Outside berm 3-5<br />
On August 25, 1987, <strong>the</strong> work activity of cleaning <strong>the</strong> tank continued with<br />
<strong>the</strong> same protection levels as <strong>the</strong> previous day. The OVA readings were as<br />
follows:
Cleaninu Tank Concentration (om)<br />
Above tank<br />
Inside barrel berm - top<br />
of barrel<br />
Outside berm<br />
Backhoe<br />
Some final clean up in <strong>the</strong> sump area was also conducted. The employees<br />
wore Level C with a full face respirator for this activity. The OVA<br />
readings were as follows:<br />
Cl eanina Sumo Concentration (ooml<br />
Outside sump area<br />
Sump trap inside<br />
During <strong>the</strong> day, it became necessary for an employee to enter <strong>the</strong> open tank<br />
to shovel <strong>the</strong> residual sludge into <strong>the</strong> backhoe bucket. Confined Space<br />
Entry procedures were utilized for this activity. The employee entering<br />
<strong>the</strong> tank wore an airline respirator with an escape bottle, saranex suit,<br />
rubber boots, chemical-resistant gloves (inner and outer), and a safety<br />
harness with a safety line attached. A stand-by observer was equipped with<br />
a SCBA, saranex suit, rubber boots, and chemical-resistant gloves (inner<br />
and outer). The OVA was re-cal i brated and <strong>the</strong> background established at<br />
0.8 ppm. The OVA readings obtained were as follows:<br />
Tank Entry Concentration (o~rn)<br />
Above tank<br />
Outside berm<br />
Backhoe<br />
After lunch, cleaning inside <strong>the</strong> tank continued with <strong>the</strong> same level of<br />
protection as noted above. Upon completion of <strong>the</strong> sludge removal, <strong>the</strong><br />
inside of <strong>the</strong> tank was steam-cleaned. The OVA was re-calibrated and <strong>the</strong><br />
background established at 2.0 ppm. The OVA readings were as follows:
Tank Entry Concentration (oom)<br />
Above tank 200<br />
Outside perimeter of tank 5.0<br />
Backhoe 2.0<br />
Inside barrel berm - top of barrel 120<br />
Outside berm 2.0<br />
Above tank - after steam clean 5.0<br />
During <strong>the</strong> tank entry activities, two employees, Jeff Buhl and Scott<br />
Freiwald, experienced direct skin contact with <strong>the</strong> sludge material. A<br />
small area on <strong>the</strong>ir neck and jaw indicated contact. The sludge was washed<br />
off with water. Since <strong>the</strong> known constituents are not readily absorbed<br />
through <strong>the</strong> skin, this contact would not be considered a significant source<br />
of exposure.<br />
The final activities during <strong>the</strong> liquid removal phase of this project<br />
involved <strong>the</strong> pumping of <strong>the</strong> liquid from a trough inside <strong>the</strong> building and<br />
<strong>the</strong> draining of <strong>the</strong> water from <strong>the</strong> boiler tank. The OVA reading for both<br />
operations were at background 1 eve1 s.<br />
4.5.2 Air Monitorinq Durinq Soil Excavation Activities<br />
4.5.2.1 Summarv of Excavation Activities<br />
During <strong>the</strong> week of October 5, 1987, air monitoring was conducted at <strong>the</strong> Bay<br />
Area Drum site. The site activities during this time period included<br />
uncovering of buried drums, excavation of contaminated soi 1 s, and grading<br />
of site yard. Direct reading instrumentation, consisting of an Organic<br />
Vapor Analyzer (OVA) and Draeger tubes for vinyl chloride were utilized at<br />
various steps throughout <strong>the</strong> activities. In addition, integrated ambient<br />
air samples were obtained from <strong>the</strong> site perimeter. Personal exposure<br />
monitoring of employees was conducted based on <strong>the</strong>ir assigned job func-<br />
tions. The ambient and employee samples collected were full duration<br />
samples and <strong>the</strong> results are considered time weighted averages.
The integrated samples were analyzed by an independent laboratory which<br />
maintains certification by <strong>the</strong> American Industrial Hygiene Association, <strong>the</strong><br />
National Institute for Occupational Safety and Health, and <strong>the</strong> Environ-<br />
mental Protection Agency.<br />
The direct reading instrumentation indicated potential exposure to vinyl<br />
chloride monomer based on <strong>the</strong> Draeger tube length of stain. With this<br />
indication, personnel protective equipment was upgraded to minimize <strong>the</strong><br />
potential exposure. The Draeger tube method is subject to several<br />
interferences and is not considered as accurate as <strong>the</strong> integrated samples.<br />
The integrated samples were specific for determining airborne concentra-<br />
tions of vinyl chloride monomer, polychlorinated biphenyl, lead, and total<br />
dust. The analytical results indicated no detectable levels of vinyl<br />
chloride or polychlorinated biphenyl on any of <strong>the</strong> ambient or personal<br />
samples. One sample indicated a measurable concentration for lead. This<br />
sample was obtained along <strong>the</strong> sou<strong>the</strong>rn perimeter fence on <strong>the</strong> final day of<br />
3<br />
activity monitoring. The result reported was 0.004 mg/m . All <strong>the</strong> remain-<br />
ing samples submitted for lead analysis indicated no detectable levels.<br />
Several of <strong>the</strong> samples analyzed for total dust concentrations reported<br />
detectable concentrations. For those samples which did indicate total dust<br />
3 3<br />
concentration, <strong>the</strong> range was reported between 0.1 mg/m and 0.6 mg/m .<br />
The Occupational Safety and Health Administration (OSHA) has established<br />
Permissible Exposure Limits for occupational exposure to each of <strong>the</strong> in-<br />
tegrated sample analytes. In all instances <strong>the</strong> reported concentration<br />
levels were well below <strong>the</strong> permissi ble exposure 1 imits.<br />
4.5.2.2 Direct Readinq Instrumentation<br />
The direct reading instrumentation used during <strong>the</strong> excavation phase at Bay<br />
Area Drum consisted of an organic vapor analyzer (OVA) and Draeger tubes<br />
for vinyl chloride. The range for <strong>the</strong> vinyl chloride tubes was 0.5 parts<br />
per million (ppm) to 6 ppm with 10 pump strokes.
On Friday, October 2, 1987, old drums which were buried along <strong>the</strong> east side<br />
of <strong>the</strong> yard were uncovered. The OVA was calibrated using zero hydrocarbon<br />
air and methane at 6.7 ppm. Background level was established outside <strong>the</strong><br />
exclusion area and upwind of <strong>the</strong> site. Background level was 1.8 ppm. OVA<br />
reading and vinyl chloride tubes evaluated levels before and during <strong>the</strong><br />
removal of <strong>the</strong> buried drums.<br />
Above drums -<br />
prior to removal 1.8<br />
Above open drum 1.8<br />
East pit - after some drums<br />
removed and fresh soil<br />
uncovered 3.0<br />
Leaking drum 3.0<br />
East pit - after drums removed 3.0<br />
General yard 1.8<br />
Sump area 3.2<br />
OVA Vinyl Chloride<br />
Concentration (porn1 Concentration (oomr<br />
None detected<br />
None detected<br />
0.5<br />
None detected<br />
None detected<br />
N/A<br />
N/A<br />
During <strong>the</strong> drum removal activities <strong>the</strong> protection levels utilized were<br />
Level C, with full face Scott respiratory protection, chemical resistant<br />
gloves (inner and outer), rubber boots, hard hat, and polytyveks for <strong>the</strong><br />
employee in <strong>the</strong> pit hooking up <strong>the</strong> drums and <strong>the</strong> employee unhooking <strong>the</strong><br />
drums. The remaining personnel on site utilized Level D protection with<br />
boots, tyveks, gloves, and hard hats.<br />
On Monday, October 5, 1987, <strong>the</strong> activities centered around preparing for<br />
excavation and grading of <strong>the</strong> general yard area. No OVA or vinyl chloride<br />
Draeger tubes were used. All employees in <strong>the</strong> yard area wore Level D<br />
protection with boots, tyveks, gloves and hard hats. Dust suppression<br />
methods were employed during <strong>the</strong> grading activities.
On Tuesday, October 6, 1987, <strong>the</strong> excavation activities started. The OVA<br />
was calibrated using zero hydrocarbon air and methane at 6.7 ppm. Back-<br />
ground was established outside <strong>the</strong> exclusion area and upwind of <strong>the</strong> site.<br />
Background level was 1.0 ppm. During <strong>the</strong> majority of <strong>the</strong> day, <strong>the</strong> OVA did<br />
not register any significant levels above background in <strong>the</strong> area of excava-<br />
tion or <strong>the</strong> general yard. When <strong>the</strong> excavation started along <strong>the</strong> building<br />
foundation, <strong>the</strong> employee providing dust suppression to <strong>the</strong> excavation<br />
reported a strong odor. Excavation activities were stopped while OVA and<br />
Draeger tube readings could be obtained.<br />
OVA Vinyl Chloride<br />
Concentration Imml Concentration (~oml<br />
Foundation 2 5 6.0<br />
Top of excavation pit None detected None detected<br />
Based on <strong>the</strong> positive detector tube reading, it was determined that fur<strong>the</strong>r<br />
excavation would be continued with continuous reading being taken at <strong>the</strong><br />
top of <strong>the</strong> excavation pit near <strong>the</strong> backhoe operator. Due to <strong>the</strong> moist<br />
soil, it was determined that dust suppression during excavation would be<br />
discontinued. For <strong>the</strong> remainder of <strong>the</strong> day, <strong>the</strong> OVA reading at <strong>the</strong> top of<br />
<strong>the</strong> excavation pit did not indicate any sustained levels above <strong>the</strong><br />
background level of 1.0 ppm. Instantaneous levels up to 1.4 ppm were<br />
noted. The level of protection utilized was Level D with boots, tyveks,<br />
gloves, and hard hats.<br />
On Wednesday, October 7, 1987, <strong>the</strong> excavation activities continued. The<br />
OVA was calibrated using zero hydrocarbon air and methane at 6.7 ppm.<br />
Background was established outside <strong>the</strong> exclusion area and upwind of <strong>the</strong><br />
site. Background level was 1.5 ppm. Continuous OVA readings were taken at<br />
<strong>the</strong> top of <strong>the</strong> excavation pit. The initial protection level for <strong>the</strong> back-<br />
hoe operator was Level D with boots, tyveks, gloves, and hard hats. When<br />
<strong>the</strong> OVA registered sustained levels of 1 ppm above background, in this<br />
instance 2.5 ppm, a Draeger tube reading for vinyl chloride was taken. The
-<br />
.- -<br />
Draeger tube indicated a vinyl chloride level of 0.5 ppm at <strong>the</strong> top of <strong>the</strong><br />
excavation pit. The protection level for <strong>the</strong> backhoe operator was upgraded<br />
to Level B with boots, tyveks, gloves, hard hat and airline respirator.<br />
The remaining employees kept away from <strong>the</strong> excavation pit. The OVA was<br />
used to establish a line when <strong>the</strong> levels were reported at <strong>the</strong> background<br />
1 eve1 .<br />
A survey of <strong>the</strong> yard during grading indicated a sustained level of 4 ppm on<br />
<strong>the</strong> OVA. A Draeger tube for vinyl chloride indicated that no detectable<br />
vinyl chloride was in <strong>the</strong> grading area. The protection level for grading<br />
<strong>the</strong> yard remained at Level D with boots, tyveks, gloves, and hard hats.<br />
The truck loaded with excavated material was checked with <strong>the</strong> OVA. The<br />
level indicated 7.5 ppm. A vinyl chloride Draeger tube taken in <strong>the</strong> same<br />
area of <strong>the</strong> truck indicated 1 ppm.<br />
At <strong>the</strong> end of <strong>the</strong> day's activity, <strong>the</strong> OVA reading at <strong>the</strong> top of <strong>the</strong><br />
excavation was at background and a Draeger tube for vinyl chloride<br />
indicated no detectable level.<br />
On Thursday, October 8, 1987, <strong>the</strong> excavation activities continued. The OVA<br />
was calibrated using zero hydrocarbon air and methane at 6.7 ppm.<br />
Background was established outside <strong>the</strong> exclusion area and upwind of <strong>the</strong><br />
site. Background level was 2.3 ppm. Continuous OVA readings were taken at<br />
<strong>the</strong> top of <strong>the</strong> excavation pit. The initial protection level for <strong>the</strong><br />
backhoe operator was Level D with boots, tyveks, gloves, and hardhat. When<br />
<strong>the</strong> OVA registered sustained levels of 3.3 ppm, <strong>the</strong> protection level for<br />
<strong>the</strong> operator was upgraded to Level B with <strong>the</strong> addition of airline<br />
respiratory protection. The remaining employees were kept away from <strong>the</strong><br />
excavation pit by establishing a 1 ine where <strong>the</strong> OVA readings were at<br />
background level s.<br />
A survey of <strong>the</strong> yard identified one area where <strong>the</strong> OVA readings were at<br />
14.3 ppm. The vinyl chloride Draeger tube reported no detectable level.
The equipment operator and <strong>the</strong> employee providing dust suppression were<br />
required to upgrade <strong>the</strong>ir protection level to Level C with boots, gloves,<br />
tyveks, hard hat and a half-mask respirator with organic vapor cartridges<br />
and a dust pre-filter. The area was re-evaluated an hour later with <strong>the</strong><br />
OVA. The levels reported were 5.3 ppm. At this time, <strong>the</strong> employees<br />
working in this area were advised that <strong>the</strong> continued use of <strong>the</strong> respiratory<br />
protection was optional.<br />
At <strong>the</strong> end of <strong>the</strong> day's activity, <strong>the</strong> OVA reading at <strong>the</strong> top of <strong>the</strong><br />
excavation pit was at background levels.<br />
On Friday, October 9, 1987, <strong>the</strong> excavation activities were completed. The<br />
last part of <strong>the</strong> contaminated soil was stockpiled to await transportation.<br />
The stockpile was covered with plastic and backfill material. The OVA was<br />
calibrated using zero hydrocarbon air and methane at 6.7 ppm. Background<br />
was established outside <strong>the</strong> exclusion area and upwind of <strong>the</strong> site.<br />
Background level was 1.6 ppm. Readings taken surrounding <strong>the</strong> covered<br />
stockpile were reported at background levels. The level at <strong>the</strong> top of <strong>the</strong><br />
excavation pit was also at background.<br />
A series of soil samples were collected in <strong>the</strong> excavation pit. The<br />
protection level utilized during collection was Level B with boots, hard<br />
hat, chemical resistant gloves (inner and outer), tyveks, and airline<br />
respiratory protection.<br />
After <strong>the</strong> samples were collected, <strong>the</strong> excavation pit was backfilled with<br />
clean fill material.<br />
4.5.2.3 Intesrated Sam~le Collection and Analysis<br />
The sampling procedures utilized corresponded with specific National Insti -<br />
tute for Occupational Safety and Health (NIOSH) methods for collection.<br />
The pumps used to collect <strong>the</strong> samples were Gilian models. The pumps were<br />
calibrated prior to and after sample collection. Calibration methods were
ased on a primary standard of volumetric displacement using a buck<br />
calibrator with <strong>the</strong> appropriate sample media in <strong>the</strong> sample train. Each<br />
pump was fully charged prior to monitoring.<br />
The ambient sample stations were located along <strong>the</strong> temporary fence sur-<br />
rounding <strong>the</strong> site. The west fence station was approximately halfway be-<br />
tween <strong>the</strong> building and <strong>the</strong> end of <strong>the</strong> yard on Thomas Street. The sou<strong>the</strong>rn<br />
fence station was on <strong>the</strong> open gate panel on Hawes Street. The resident<br />
fence station was on <strong>the</strong> east side of <strong>the</strong> excavation area. All <strong>the</strong> fence<br />
stations had <strong>the</strong> pumps and sample media located approximately 4.5 feet off<br />
<strong>the</strong> ground. The predominant wind direction was from <strong>the</strong> northwest. The<br />
ambient temperatures ranged from 95'~ on Monday and Tuesday to 70' F during<br />
<strong>the</strong> latter part of <strong>the</strong> week.<br />
The employee samples were all collected from <strong>the</strong> breathing zone of <strong>the</strong><br />
individual wearing <strong>the</strong> monitoring equipment.<br />
The monitoring equipment was checked frequently throughout <strong>the</strong> sample<br />
period to ensure that an adequate flow rate was being maintained. The<br />
monitoring duration was for approximately seven hours or <strong>the</strong> duration of<br />
<strong>the</strong> activity. The sampling media was chilled prior to shipment to <strong>the</strong><br />
analytical laboratory. Field blanks for each sample media were submitted<br />
with <strong>the</strong> samples. Tables 3 and 4 indicate <strong>the</strong> sampling summaries for <strong>the</strong><br />
employee and ambient air monitoring.<br />
The analysis of <strong>the</strong> samples was conducted according to NIOSH methods speci-<br />
fic for constituent of interest. Tables 5 and 6 indicate <strong>the</strong> analytical<br />
results of <strong>the</strong> samples.<br />
4.6 Personal Protective Eaui~ment<br />
The minimum level of protection for exclusion area personnel included <strong>the</strong><br />
following:
1. Hardhat<br />
2. Calf length steel-toed neoprene boots<br />
3. Tyvek coveralls or PVC rainpants and safety glasses (for work<br />
where splash hazards and upper body skin contact were not expected<br />
to occur)<br />
During activities where upper body skin contact was a potential exposure<br />
mechanism, pol ycoated Tyvek coverall s were used, as appropriate, in place<br />
of <strong>the</strong> rainpants.<br />
Fur<strong>the</strong>r discussion of personal protective equipment during liquid removal<br />
and soil excavation activities is provided in Section 4.5.<br />
Eyewash bottles were maintained in <strong>the</strong> drum handling and support areas.<br />
The site first aid kit was located in <strong>the</strong> support area. Twenty pound ABC<br />
fire extinguishers were maintained in <strong>the</strong> drum handling area and in <strong>the</strong><br />
support area. Specific use of and changes in protection equipment were as<br />
required by <strong>the</strong> site Health and Safety Officer in consideration of site<br />
conditions and construction activities.<br />
4.7 Decontamination Procedures<br />
4.7.1 Personal Decontamination<br />
All disposable clothing was deposited in containers on-site for off-site<br />
disposal. Wash tubs with soap and water and rinse tubs were provided for<br />
decontamination of boots and outer gloves. Respirators were cleaned with<br />
sanitizing wipes unless gross contamination required submersion in a<br />
wash/rinse tub. All decontamination was performed in <strong>the</strong> area shown on<br />
Figure 3.<br />
Soap and water were provided for personnel to wash up with after work or if<br />
any skin contamination occurred during <strong>the</strong> work day.
4.7.2 Eauioment Decontamination<br />
All construction and drum handling equipment which had been in contact with<br />
contaminated materials was steam cleaned before leaving <strong>the</strong> site. Waste<br />
hauling trucks which became contaminated during loading were steam cleaned<br />
before leaving <strong>the</strong> site. Steam cleaning operations were performed by<br />
placing plastic in an area large enough to contain <strong>the</strong> equipment to be<br />
decontaminated. Steam cleaning water was allowed to flow onto contaminated<br />
areas to assist in dust suppression and to provide moisture for compaction.<br />
At no time was <strong>the</strong> steam cleaning water allowed to leave <strong>the</strong> site.<br />
Emergency berms were constructed, if required, to contain <strong>the</strong> water.<br />
4.8 General Site Health and Safetv and Work Rules<br />
No drinking, gambling, or illegal drugs were allowed on-site.<br />
Personal protective equipment was required in designated areas.<br />
Such equipment included, but was not limited to, respiratory<br />
protection, earplugs, hardhat, rainsuits, boots, gloves, and<br />
chemical goggles.<br />
Eating, drinking, smoking, and chewing gum or tobacco were allowed<br />
only in designated areas.<br />
Changes in work practice or work rules were implemented only after<br />
approval by <strong>the</strong> Project Manager and <strong>the</strong> site Health and Safety<br />
Officer.<br />
Construction equipment always had <strong>the</strong> right-of-way over regular<br />
vehicles.<br />
All employees entering <strong>the</strong> Exclusion Area completed <strong>the</strong> required<br />
decontamination procedure before leaving <strong>the</strong> Exclusion Area.<br />
41
7. All protective clothing worn inside <strong>the</strong> Exclusion Area was<br />
supplied. None of this equipment was permitted to leave <strong>the</strong> site<br />
until completion of <strong>the</strong> project.<br />
4.9 Traininq<br />
All on-site personnel had prior experience and training in compliance with<br />
29 CFR 1910.120.<br />
Project-specific training was provided before startup of on-site<br />
activities. This training included <strong>the</strong> following:<br />
site health and safety plan<br />
decontamination<br />
personnel protection levels<br />
chemical hazards<br />
medical monitoring<br />
air monitoring<br />
use and maintenance of personal protective equipment<br />
work zones<br />
site safety rules and conditions of employment<br />
10. emergency provisions<br />
11. buddy system<br />
On-site tailgate meetings on health and safety were held as appropriate.<br />
The site Health and Safety Officer conducted <strong>the</strong>se meetings.<br />
4.10 Medical Monitoring<br />
All on-site personnel participated in a medical monitoring program.<br />
Canonie staff or contractor personnel who are involved in <strong>the</strong> annual<br />
corporate medical program received a blood chemistry test and blood lead<br />
analysis before starting work at <strong>the</strong> site.
All on-site and trucking personnel hired specifically for <strong>the</strong> work at <strong>the</strong><br />
site received a pre-employment physical which included <strong>the</strong> following:<br />
medical history<br />
physical exam<br />
pulmonary function test<br />
EKG<br />
audiogram<br />
blood lead<br />
CBC with differential and platelets urinalysis with dipstick and<br />
microscopic morphology<br />
chest X-rays - P/A and lateral<br />
lumbar sacral X-rays - three views<br />
Post project exams were conducted at <strong>the</strong> discretion of <strong>the</strong> site Health and<br />
Safety Officer considering site conditions and exposures.<br />
4.11 Work Zone and Site Security<br />
4.11.1 Exclusion Area<br />
All of <strong>the</strong> drum yard and <strong>the</strong> excavation area were considered <strong>the</strong> exclusion<br />
area prior to cover placement. Access to this area was restricted to site<br />
personnel who had completed <strong>the</strong> training and medical exam requirements, and<br />
who were using appropriate protective equipment.<br />
Once <strong>the</strong> first layer of capping material had been applied to <strong>the</strong> drum yard,<br />
personal protective equipment was downgraded and exclusion areas revised,<br />
as appropriate.<br />
4.11.2 Decontamination Area<br />
The eastern area of <strong>the</strong> site as shown in Figure 3 was designated as <strong>the</strong><br />
decontamination or contamination reduction area. As personnel ei<strong>the</strong>r left
<strong>the</strong> drum yard or <strong>the</strong> site, <strong>the</strong>y passed through this area to <strong>the</strong> support<br />
area inside <strong>the</strong> building.<br />
4.11.3 Suo~ort Area<br />
The existing office and toilet facilities inside <strong>the</strong> building was used as a<br />
support area for <strong>the</strong> project.<br />
4.11.4 Site Security<br />
The perimeter of <strong>the</strong> site was surrounded by fencing with locked gates. The<br />
site was secured in this manner during <strong>the</strong> project. Security guards were<br />
used during implementation of <strong>the</strong> ERA until <strong>the</strong> HDPE liner and sand cover<br />
were placed.<br />
Daytime personnel access to <strong>the</strong> site was only through <strong>the</strong> personnel<br />
entrance shown on Figure 3. Equipment access was through <strong>the</strong> gate along<br />
Shafter Avenue. No personnel access was allowed through this gate except<br />
as required to deliver or operate equipment.<br />
4.12 Communitv Health and Safety<br />
The potential community hazards included <strong>the</strong> excavation of <strong>the</strong> residential<br />
backyards, airborne dust or organic vapors, <strong>the</strong> presence of construction<br />
equipment, and higher than normal truck traffic around <strong>the</strong> site.<br />
Temporary fencing was placed around <strong>the</strong> site during <strong>the</strong> ERA activities and<br />
will remain in place until final fencing has been installed. Any open<br />
excavation was fenced or barricaded to prevent entrance by off-site<br />
personnel. Warning tape or signs were posted to advise offsite personnel<br />
to stay out of <strong>the</strong> construction areas. Only authorized personnel were<br />
admitted onto <strong>the</strong> site.
Exposures to dust and/or organic vapors were minimized through wetting<br />
techniques, as appropriate. In addition, plastic sheeting was placed on<br />
temporary fencing in <strong>the</strong> residential yards to restrict migration of<br />
excavated materials. Residents were advised to keep windows and doors<br />
closed if <strong>the</strong>se openings face <strong>the</strong> excavation area.<br />
Air monitoring was conducted during several of <strong>the</strong> work activities as<br />
described in detail in Section 4.5.<br />
Truck traffic included del ivery and removal of construction materi a1 s,<br />
equipment and supplies, and trailers containing excavated materials and<br />
debris for off-site disposal. Vehicles were decontaminated before leaving<br />
ing <strong>the</strong> site, as necessary. Traffic control was not provided and was not<br />
considered necessary to prevent street congestion or traffic hazards to<br />
local residents or businesses. Site entrances were controlled to eliminate<br />
pedestrian traffic.<br />
45
TABLES
TXBLE I<br />
SUBCONTRACTOR LIST<br />
NAME REPRESENTATIVE PHONE<br />
West Coast Locators<br />
Nilex<br />
.AAA Fence<br />
Roscoe Moss<br />
American Soil Products<br />
Raisch Products<br />
Levine Metal<br />
Anchor Fence<br />
Wells Security Service<br />
Esquivel Grading<br />
and Paving<br />
Dolan Concrete<br />
Herzog & Associates<br />
Chemical Waste Management<br />
Frank Zamira<br />
James Cramer<br />
scott<br />
Dorothy<br />
Adam Dauls<br />
Bob Renna<br />
Gary<br />
Tony Chapman<br />
Donna Wells<br />
Jon Walsh<br />
Dan Blamer<br />
Wayne Oakley<br />
Keith Pushaw<br />
With Fencing Bob With<br />
NUMBER TASK RESPONSIBILITY<br />
Utility Location<br />
Geotextile & HDPE Lining<br />
Temporary Fence<br />
PUC Pipe<br />
Fine Soil., Fill, Sand, Topsoil<br />
Aggregate Base<br />
Boiler Tank Removal<br />
Chain Link Fence Installation<br />
Security Guard<br />
Asphalt Construction<br />
Concrete Construction<br />
Soil Testing<br />
Transportation and Disposal of<br />
Waste Materials<br />
Wood Fence Installation
OR4 INVOICE #445<br />
OISWSllL<br />
- - - - - - - - -- - - -<br />
MANIFEST No. DATE<br />
.--....----. .. . . -.-..---.<br />
87341403-51 :: 10/6/87<br />
87341404-51 :: 10/6/87<br />
87341405-51 :: 10/6/87<br />
87341406-51 : : 10/6/87<br />
87341407-51 :: 10/6/87<br />
87341408-51 :: 10/6/87<br />
TABLE 2<br />
SUMMRRY OF HAZRRWUS WASTE OISWSAL<br />
BAY ARE& DRUM<br />
10/87<br />
YRRDAGE : WEIGHT : PROFILE :DISPOSAL<br />
10/87 10/87 10/87 10/87<br />
TRANSPORT : DEMURRAGE: LINERS : TAX ::<br />
-<br />
BAY RREA DRUM 87-035.21<br />
EXTENTION<br />
CWM<br />
---------.<br />
3.133.43<br />
3,511.93<br />
3,490.90<br />
3,511.93<br />
3,448.84<br />
3,427.82<br />
3,469.87<br />
3,385.76<br />
3,133.43<br />
3.133.43
3W INVOICE Y446<br />
OISWSAL<br />
------.-----<br />
------------<br />
MANIETST No. :: DATE : YARDAGE<br />
. . .<br />
87080611-51 :: 9/29/87 : 20.00<br />
87080612-51 :: 9/29/87 : 20.00<br />
81080596-51 :: 1011187 : 20.00<br />
i3W4 INVOICE a473<br />
DISWSAL<br />
------------<br />
.<br />
TABLE 2 (CONTINUED)<br />
SUHMARY OF HAZAROOUS WASTE DISPOSAL<br />
BAY ARFA DRUM<br />
WEIGHT : PROFILE<br />
0 :ENR-G57146<br />
0 :m-G5714b<br />
13,080 :m-G51146<br />
19,300 :EMR-G57146<br />
8,760 :ERR-G5714b<br />
0 :W-G51146<br />
20,660 :FBI-G57146<br />
0 :Ern-G57146<br />
61800<br />
MANIFEST No. DATE : YARDAGE : WEIGHT : PROFILE<br />
.<br />
87341238-51 : : 10/27/87 : 15 : 0 :ENR-G98113<br />
87341239-51 :: 10/27/87 : 15 : 0 :ENR-G98713<br />
87440407-51 :: 10/27/87 : 15 : 0 :ENR-G98713<br />
87440408-51 :: 10/27/87 : 15 : 0 :ENR-G98713<br />
87341240-51 :: 10/29/87 : 15 : 0 :ENR-G98713<br />
87341241-51 :: l0/29/87 : 15 : 0 :ENR-G98713<br />
87341242-51 :: 10/29/87 : 15 : 0 :ENR-G98713<br />
87341243-51 :: 10129187 : 15 : 0 :Em-G98713<br />
10/87 10/87 10187<br />
:DISPOSAL : TRANSPORT : DEMURRAGE:<br />
:DISPOSAL : TRANSPORT : DEMURRAGE:<br />
.<br />
: 1,800.00 : 1.093.43 :<br />
: 1.800.00 : 1.093.43 :<br />
10/87<br />
LINERS :<br />
10/87<br />
TAX : :<br />
. . .<br />
240.00 ::<br />
240.00 ::<br />
240.00 ::<br />
192.00 ::<br />
240.00 ::<br />
240.00 ::<br />
240.00 ::<br />
240.00 ::<br />
. .<br />
. .<br />
.............<br />
1,872.00<br />
BAY RRWL DRUM 87-035.21<br />
EXTENTION<br />
LINERS : TAX : : CWM<br />
36,000.00 21,868.60 315.42 1,200.00 3,600.00 62,984.02<br />
Environmental
CWH INVOICE W515<br />
TABLE 2 (CONTINUED)<br />
SUMMARY OF HAZRRWUS WASTE DISPOSAL<br />
BAY AREA DRUH<br />
DISWSAL<br />
------------<br />
MANIFEST No. :: DATE : YARDAGE : WEIGHT : PROFILE<br />
.----------- . .<br />
10/87<br />
:DISPOSAL<br />
10187 10/87 10187<br />
: TRANSPORT : DEMURRAGE: LINERS :<br />
10/87<br />
TAX<br />
' EXTENTION<br />
:: cnn<br />
. .<br />
87341214-51 :: 11/24/87 : 15 : 0.00 :EN-G98713 : 1,800.00 : 1,093.43 : 84.11 : 60.00 : 180.00 :: 3,217.54<br />
.. ---------- . -----------<br />
. . . .<br />
. .<br />
. . 0.00<br />
. . 0.00<br />
---------~~~~~~~~~.....~~-~~~----------~--~~~<br />
1,800.00 1,093.43 84.11 60.00 180.00 3,217.54<br />
Environmental
Sample<br />
Number<br />
87035-25<br />
87035-26<br />
87035-27<br />
87035-28<br />
87035-41<br />
87035-42<br />
87035-43<br />
87035-56<br />
87035-57<br />
87035-58<br />
87035-59<br />
87035-60<br />
87035-61<br />
I I]<br />
Sample<br />
Enolovee Media<br />
TABLE 3<br />
EMPLOYEE A IR MONITORING COLLECTION SUMMARY<br />
Flow Rate Dvration<br />
Supervisor, Charcoal Tube 11934 47 cc/m 452 min.<br />
General Site Fluorsil Tube 200 cc/m<br />
Glass Fiber Filter 200 cc/m<br />
Laborer, Pre-Wei hted 17840 1.9l/m 443 min.<br />
Excavation Area MCEF ~iqter<br />
Equipment Charcoal Tube 5067-10 46 cc/m 429 min.<br />
Operator, Fluosil Tube 200 cc/m<br />
Grading Area Glass Fiber Filter 200 cc/m<br />
Equipment Charcoal Tube 5067-10 46 cc/m 434 min.<br />
Operator, Fluorsil Tube 200 cc/m<br />
Excavation Area Glass Fiber Filter 200 cc/m<br />
Equipment Charcoal Tube 5067-10 46 cc/m 434 min.<br />
Operator, Fluorsil Tube 200 cc/m<br />
Excavation Area Glass Fiber Filter 200 cc/m<br />
NIOSH<br />
Method Chemical<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
S262 Total Dust<br />
PlCAM173 Lead<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
I Environmental
TABLE 4<br />
AMBIENT AIR MONITORING COLLECTION SUMMARY<br />
NlOSH<br />
Flow Rate Duration Volume Method Chemical<br />
10/5 87035-01 West Fence Pre-Wei hted 17840 2.1 l/m 49 min. 1.0 M3 S262 Total Dust<br />
MCEF ~igter PLCAM173 Lead<br />
87035-02 Charcoal Tube 5 47 cc/m 480 min. 23 1 S25 Vinyl Chloride<br />
87035-03 Fluorsil Tube 200 cc/m 87 1 5503 PCB-vapor<br />
87034-04 Glass Fiber Filter 200 cc/m 87 1 5503 PCB-particulate<br />
10/5 87035-05 Resident Pre-Weighted 17839 2.1 1/m 479 min. 1.0 M~ 5262 Total Dust<br />
Fence MCEF filter PtCAM173 Lead<br />
87035-06 Charcoal Tube 11934 48 cc/m 480 min. 23 1 525 Vinyl Chloride<br />
87035-07 Fluorsil Tube 200 cc/m 94 1 5503 PCB-vapor<br />
87035-08 Glass Fiber Filter 200 cc/m 94 1 5503 PCB-particulate<br />
10/5 87035-09 Plating Shop Pre-Weighted 17841 2.2 1/m 480 min. 1.1 M3 5262 Total Dust<br />
MCEF filter PLCAM173 Lead<br />
87035-10 Charcoal Tube 11935 49 cc/m 440 min. 22 1 525 Vinyl Chloride<br />
87035-1 1 Fl uorsi 1 Tube 210 cc/m 92 1 5503 PCB-vapor<br />
87035-12 Glass Fiber Filter 210 cc/m 92 1 5503 PCB-particulate<br />
10/5 87035-13 Sou<strong>the</strong>rn Pre-Wei hted 17842 2.2 1/m 478 min. 1.0 M~ S262 Total Oust<br />
Fence MCEF fii'ter P&CAM173 Lead<br />
87035-14 Charcoal Tube 5067-10 49 cc/m 488 min. 24 1 S25 Vinyl Chloride<br />
87035-15 Fluorsil Tube 200 cc/m 98 1 5503 PCB-vapor<br />
87035-16 Glass Fiber Filter 200 cc/m 98 1 5503 PCB-particulate<br />
I Environmental
Sample<br />
e e f s E B r & & ?<br />
10/7 87035-33 Sou<strong>the</strong>rn<br />
Fence<br />
87035-34<br />
87035-35<br />
87035-36<br />
Sample<br />
TABLE 4<br />
AMBIENT AIR MONITORING COLLECTION SUMMARY<br />
(Continued)<br />
Pre-Uei hted 17841<br />
MCEF filter<br />
Charcoal Tube 11935<br />
Fluorsil Tube<br />
Glass Fiber Filter<br />
10/7 87035-37 West Fence Pre-Wei hted 17842<br />
MCEF fi7ter<br />
Charcoal Tube 11935<br />
Fluorsil Tube<br />
Glass Fiber Filter<br />
10/B 87035-14 West Fence Pre-Uei hted 17839<br />
MCEF filter<br />
Charcoal Tube 5<br />
Fluorsil Tube<br />
Glass Fiber Filter<br />
10/8 87035-48 Sou<strong>the</strong>rn<br />
Fence<br />
87035-49<br />
87035-50<br />
87035-51<br />
Pre-Wei hted 17839<br />
NCEF fiyter<br />
Charcoal Tube 11934<br />
Fluorsil Tube<br />
Glass Fiber Filter<br />
&p Flow Rate<br />
2.2 l/m<br />
Ouration<br />
393 min.<br />
392 min.<br />
438 min.<br />
442 min.<br />
425 min.<br />
428 min.<br />
418 min.<br />
421 min.<br />
NIOSH<br />
--<br />
Method Chemical<br />
S262 Total Dust<br />
PllCAM173 Lead<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
S262 Total Dust<br />
P&CAH173 Lead<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
5262 Total Dust<br />
PtCAM173 Lead<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
S262 Total Dust<br />
P&CAM173 Lead<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate
Sample<br />
t&!w<br />
87035-66<br />
87035-67<br />
87035-68<br />
87035-69<br />
87035-70<br />
87035-71<br />
87035-72<br />
87035-73<br />
87035-52<br />
87035-53<br />
87035-54<br />
87035-55<br />
87035-62<br />
87035-63<br />
87035-64<br />
87035-65<br />
fmIQw2<br />
Sou<strong>the</strong>rn<br />
Fence<br />
Sou<strong>the</strong>rn<br />
Fence<br />
Resident<br />
Fence<br />
Resident<br />
Fence<br />
Sample<br />
TABLE 4<br />
AMBIENT AIR MONlTORlNG COLLECTION SUMMARY<br />
(Continued)<br />
m<br />
Pre-Weighted 17840<br />
MCEF filter<br />
Charcoal Tube 11935<br />
Fluorsil Tube<br />
Glass Fiber Filter<br />
Pre-Wei hted 17842<br />
MCEF fi'i'ter<br />
Charcoal Tube 11934<br />
Fl uorsi 1 Tube<br />
Glass Fiber Filter<br />
Pre-Weighted 17841<br />
REF filter<br />
Charcoal Tube 11935<br />
Fluorsil Tube<br />
Glass Fiber Filter<br />
Pre-Weighted 17839<br />
MCEF filter<br />
Charcoal Tube 5<br />
Fluorsil Tube<br />
Glass Fiber Filter<br />
Flow Rate<br />
1.9 l/m<br />
46 cc/m<br />
200 cc/m<br />
200 cc/m<br />
2.1 l/m<br />
46 cc/m<br />
200 cc/m<br />
200 cc/m<br />
2.0 l/m<br />
46 cc/m<br />
200 cc/m<br />
200 cc/m<br />
2.1 l/m<br />
38 cc/m<br />
200 cc/m<br />
200 cc/m<br />
Duration<br />
429 min.<br />
428 min.<br />
425 min.<br />
429 min.<br />
416 min.<br />
417 min.<br />
455 min.<br />
460 min.<br />
SZ62 Total Dust<br />
PKAM173 Lead<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
S262 Total Dust<br />
PaCAM173 Lead<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
5262 Total Dust<br />
PKAM173 Lead<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
S262 Total Dust<br />
PaCAM173 Lead<br />
S25 Vinyl Chloride<br />
5503 PCB-vapor<br />
5503 PCB-particulate<br />
I Environmental
Sample Sample<br />
~~~~<br />
TABLE 4<br />
AMBIENT AIR MONlTORING COLLECTION SUMMARY<br />
(Continued)<br />
NIOSH<br />
Flow Rate Duration Volume Method Chemical<br />
10/6 87035-21 Resident Pre-Wei hted 17842 2.1 1/m 615 min. 1.3 M3 S262 Total Dust<br />
Fence MCEF filter P&CAH173 Lead<br />
87035-22 Charcoal Tube 5 39 cc/m 617 min. 24 1 S25 Vinyl Chloride<br />
87035-23 Fluorsil Tube 200 cc/m 125 1 5503 PCB-vapor<br />
87035-24 Glass Fiber filter 200 cc/m 125 1 5503 PCB-particulate<br />
10/7 87035-29 Resident Pre-Wei hted 17839 2.1 1/rn 394 min. 830 1 S262 Total Dust<br />
Fence HCEF fii'ter P&CAM173 Lead<br />
87035-30 Charcoal Tube 5 40 cc/m 397 rnin. 16 1 S25 Vinyl Chloride<br />
87035-31 Fluorsil Tube 200 cc/m 79 1 5503 PCB-vapor<br />
87035-32 Glass Fiber Filter 200 cc/m 79 1 5503 PCB-particulate
TABLE 6<br />
AMBIENT AIR MONlTORlNG ANALYTICAL RESULTS<br />
Date- K - PCB Lead fMs/m31<br />
10/5 Sou<strong>the</strong>rn Fence BDL BDL<br />
West Fence BDL BDL<br />
Resident Fence BDL BDL<br />
Plating Shop BDL BDL<br />
BDL<br />
BDL<br />
BDL<br />
BDL<br />
10/6 Resident Fence BDL BDL BDL<br />
10/7 Sou<strong>the</strong>rn Fence BDL BDL<br />
West Fence BDL BDL<br />
Resident Fence BDL BDL<br />
10/8 Sou<strong>the</strong>rn Fence BDL BDL<br />
West Fence BDL BDL<br />
Resident Fence BDL BDL<br />
10/9 Sou<strong>the</strong>rn Fence<br />
West Fence<br />
Resident Fence<br />
BDL BDL<br />
BDL BDL<br />
BDL BDL<br />
BDL<br />
BDL<br />
BDL<br />
BDL<br />
BDL<br />
BDL<br />
BDL<br />
BDL<br />
BDL<br />
Limit of Detection: 0.001 nq 0.05 ug tubes 0.002 mg<br />
0.3 ug-filters<br />
NIOSH Method: S25 5503 PllCAM173<br />
BDL: Below Detection Limit<br />
Total ~ust (ns/m3)<br />
0.2<br />
BDL<br />
0.3<br />
0.4<br />
BDL<br />
BDL<br />
BDL<br />
0.2<br />
BDL<br />
0.1<br />
0.2<br />
BDL<br />
BDL<br />
I<br />
I Environmental<br />
, ,~ .. .....m?.......... ~~.., ~~~ , ~~ ~.<br />
~. ... ,.... ..-~.
FIGURES
APPENDIX A<br />
Environmental
APPENDIX B<br />
Environmental
100 50 10 5<br />
GRAIN SlZE IN MILLIMETERS<br />
:OBBLES<br />
GRAVEL<br />
coARs, 1 FINE<br />
I SAND<br />
ICOARSE~ MEDIUM I FINE I SILT OR CLAY 1<br />
Symbol Sample Source I Classiflcatlon<br />
0<br />
%<br />
Felton Sand<br />
Sand 95.8 Light Brown Silty<br />
American Soils Products, Inc. % Silt 1.2 Clayey Sand (SP)<br />
% Clay 3.0<br />
Job No:<br />
DONALD 5674.3-0-8 PARTICLE SIZE ANALYSIS PLATE<br />
HERZGG Appr:<br />
& ASSEIATES. INC. 0G-o Canonie Engineers<br />
CEOTECH\IC+L C0'.51( T.\'.rS<br />
Aug. 1987<br />
1
(Common F ill) % Clay 24.5<br />
and 38.2 Light Brown Clayey<br />
% silt 37.3 Sandy S ilt (ML)<br />
Canonie Engineers
TEST MET OD: ASTM 0 1 57-70 (C)<br />
I 50 60<br />
MOISTURE CONTENT<br />
' ShMPLE DEPTH I CLASSIFICATION I SOURCE<br />
/ BULK A 0.00 '<br />
OONALO<br />
'iERZO[j<br />
ASSCCIFITES<br />
GEOTECHNICfiL CONSULTANTS<br />
LIGHT BROWN GRAVELLY SANO
' SAMPLE DEPTH I<br />
CLASSIFICATION<br />
20 38 48 50<br />
MOISTURE CONTENT (%I<br />
BULK B 0.88 LIGHT BROWN CLAYEY SILT(ML> COMMON FILL 118<br />
DONALD<br />
YERZCG<br />
ASSOCIATES<br />
GEOTECHNICAL CONSULTANTS<br />
Job No:<br />
5674.03.ee.8<br />
Date:<br />
w<br />
Septembar 1987<br />
COMPACTION TEST DATA<br />
BAY AREA DRUM<br />
Bay firma, California<br />
OPTIMIUM<br />
'IOISTURE (%)<br />
PLATE<br />
5
20 30 40 50<br />
MOISTURE CONTENT (%)<br />
MAXIMUM DRY OPTIMUM<br />
SAMPLE CLASSIFICATION SOURCE DENSITY f~cfl MOISTURE I%)<br />
DONALD<br />
HERZOG<br />
& ASSmIATES<br />
GEOTECHNICAL AND<br />
ENVIRONMENTAL CONSULTANTS<br />
Job No:<br />
Date:<br />
56'74.03.00.8<br />
November 1987<br />
COMPACTION TEST DATA<br />
CANONIE ENVIRONMENTAL<br />
Mountain View, California<br />
PLATE<br />
1
NUCLEw<br />
t<br />
RELATIVE<br />
COMPACTION<br />
PRoJECT NAME A RL-A DRUM TESTED BY G ~ t e h ) ~ ~<br />
PROJECT No A7 -03-r CALCULATED BY -J.&<br />
DATE CHECKED BY w ~uo(/i TEST DATA<br />
WET DENSITY<br />
(PCF) )24. 5 123.L 123 /<br />
YOIGTWIE<br />
COUNT<br />
STANMRD COUNT REMARKS :<br />
DOI$ITY I MOISTURE<br />
-.<br />
I<br />
-<br />
,~
PROJECT NAME 3.b 1'<br />
PROJECT No. 87 - n 7.7<br />
PGk, PW TESTED 8. Y A 'dl -<br />
DATE 1 I//() 1 Q J ~<br />
WBER OF<br />
PASSES<br />
-.<br />
LIFT<br />
THICKNESS<br />
DENSITY<br />
CWNT<br />
,. 7. .<br />
DRY DENSITY<br />
(PCF)<br />
CALCULATED BY ii /c l<br />
CHECKED BY A4 AX; 5,~ ct<br />
Y,P<br />
I IS: 0-<br />
sh<br />
/ 1-1<br />
/ci%<br />
90.2%<br />
I1 :<br />
. NUCLEkcc<br />
RELATIVE<br />
TEST DATA<br />
-<br />
"7
E-W COORD. /+s: 1<br />
ELEVATION 1 I I I<br />
.<br />
LIFT<br />
THICKNESS<br />
ENSITY<br />
MUNT 2 853- -, , .<br />
SrANDARD COUNT REMARKS :<br />
DDI8ITY I MOISTURE<br />
x-<br />
I<br />
I I<br />
- -<br />
. .<br />
I C<br />
NUCLEA,~<br />
RELATIVE<br />
COMPACTION<br />
TEST DATA<br />
J/' 4
PROJECT NAME TESTED BY ___.----<br />
PROJECT No. CALCULATED BY<br />
DATE CHECKED BY<br />
N-8 COORD.<br />
I<br />
i E-W COOAD.<br />
ELNATION<br />
YOOE DEPTH<br />
WET DENSITY<br />
IPCF)<br />
MOISTURE<br />
C U T<br />
I C (-1 9<br />
NUCLEkn<br />
I<br />
RELATIVE<br />
COMPACTION<br />
TEST DATA
APPENDIX C
I DATE<br />
PROJ. NO. PROJECr NAME<br />
L.P. NO. I SAMPLERS: Lipnafura)<br />
NO.<br />
-- UP<br />
I SAMPLE ID.<br />
CON<br />
TAINERS<br />
Relinquishad by: lsignatvrsl DatelTlme Recdned by: l~@nalural<br />
I<br />
12:~Flf<br />
Relinquished by: lslgnalure)<br />
I<br />
DatelTlms<br />
I<br />
Re~dved by: (Slg~lurs)<br />
I<br />
Relinquishsd by: ISipnslurd Daleilime Re~slved lor Laboratory by:<br />
(Sipnalure)<br />
Remarks<br />
Stockton, Ca. 95207<br />
Canary Aetu r TO snipper v~nk Lab Copy<br />
s !'
TO: R. Greenwood<br />
FROM: J. Buerger<br />
MEMO<br />
Bay Area Orum Compositinq<br />
e 4 3 O<br />
July 20, 1987<br />
The following table defines which of <strong>the</strong> 12 individual samples taken from Bay<br />
Area Orum were composited toge<strong>the</strong>r (according to compatibility). The table<br />
also includes a sample ID assigned to <strong>the</strong> composites as per <strong>the</strong> request of<br />
Keith Pushaw of Chem Waste Management. The composited samples were Federal<br />
Expressed out Friday July 17, 1987, to be delivered to Chem Waste Management<br />
on Saturday July 18. 1987.<br />
Associated charges for compositing and shipping w i l l be billed to Laboratory<br />
Project Number 87-0/5-2430. If <strong>the</strong>re are any questions please give me a call.<br />
JB/RR<br />
cc : J. Bartell<br />
K. Chirbas<br />
7
Bay Area Drum Compositing Scheme<br />
Assigned Individual<br />
Composite No. Sample ID Sample ID'S on<br />
Original Chain<br />
Custody<br />
1 ENRG 98713 Appletree<br />
Lead<br />
Sump Pit<br />
ENRG 98714 Cylinder Cut-off<br />
Trough<br />
Cement<br />
ENRG 98715 Barrel 1<br />
Barrel 2<br />
Barrel 3<br />
Union O i l<br />
ENRG 98716 Sump<br />
Boi 1 er
Laboratory Report for<br />
Mr. Rich Greenwood<br />
Canonie Environmental<br />
1825 S. Grant Street. Suite 260<br />
San Mateo. CA 94402<br />
August 4. 1987<br />
Canonie Environmental<br />
212 Frank West Circle. Suite A<br />
Stockton. CA 95206<br />
(209) 983-1340
Bay Area Drum<br />
87-035-2430<br />
Lab ID No Observations Sample ID<br />
Color: white<br />
Odor: strong paint<br />
Layers: single phased<br />
pH: 7.<br />
Semi-Sol i d<br />
Color: black<br />
Odor: strong hydrocarbons<br />
Layers: single phased<br />
pH: 10.<br />
Semi-Solid<br />
Color: whitelblack stripes<br />
Odor: strong paint<br />
Layers: black & white swirled<br />
pH: 7.<br />
Semi-Solid<br />
-<br />
(bi lavered)<br />
Color: honey<br />
Odor: strong motor oil<br />
Layers: single phased<br />
pH: 7.<br />
Liquid<br />
Color: beige<br />
Odor: strong rotten motor oil<br />
Layers: single phased<br />
pH:
Bay Area Drum<br />
87-035-2430<br />
Lab ID No Observations Sample ID<br />
Color: brown (fine,dry)<br />
Odor: none<br />
Layers: single phased<br />
pH: 6.<br />
Semi-Solid<br />
Appletree<br />
Brass Tube<br />
Color: dark brown/black (moist) Lead<br />
Odor: mild petroleum Brass Tube<br />
Layers: single phased<br />
pH: 6.<br />
Sol id<br />
Color: brown (fine, dry)<br />
Odor: none<br />
Layers: single phased<br />
pH: 6.<br />
Sol id<br />
Sump Pit<br />
Brass Tube<br />
Color: dark gray/white specks (paint) Cylinder Cut-off<br />
Odor: strong paint Mason Jar<br />
Layers: mostly solid. small amount<br />
liquid (bilayered)<br />
pH: 5.<br />
Moist Rubbery<br />
10% free liquid<br />
Color: rusty with purple & gray Trough<br />
pockets Mason Jar<br />
Odor: none<br />
Layers: single phased<br />
pH: 9.<br />
Solid (dry)<br />
Color: brown with green tint<br />
Odor: none<br />
Layers: single phased<br />
pH: 8.<br />
Solid. Moist<br />
Cement<br />
Mason Jar
. .<br />
Bay Area Drum<br />
87-035-2430<br />
Lab ID No Observations Sample I0<br />
Corposite of<br />
71 1382<br />
71 1383<br />
71 1384<br />
Corposite of<br />
71 1379<br />
71 1381<br />
Color: black<br />
Odor: strong petroleum<br />
Layers: single phased<br />
pH: 10.<br />
Semi-Sol i d<br />
Immiscible in water<br />
ENRG98715<br />
Mason Jar<br />
Color: dirty gray/orange ENRG98716<br />
Odor: we respect <strong>the</strong> potential Idason Jar<br />
hazards associated with <strong>the</strong><br />
inhalation of this composite<br />
Layers: single phased<br />
pH: 3.<br />
Liquid<br />
Miscible in water<br />
Produced off-gas upon compositing<br />
No noticeable heat generation
Client ID: BAY ARE?? DRUM Data Fi la:>1940V<br />
Sample ID: 87-035-2478 SAMPLE TOPSOIL 711940<br />
Matrix : SOIL<br />
COMPOUND NAME<br />
--_11-.--11----1---__II<br />
DICHLORODIFLUOROMETHANE<br />
CHLOROMETHANE<br />
BROMOMETHANE<br />
VINYL CHLORIDE<br />
CHLOROETHGNE<br />
METHYLENE CHLORIDE<br />
TRICHLOROFLUOROMETHANE<br />
1,l-DICHLOROETHENE<br />
Ill-DICHLOROETHANE<br />
TOTAL 1,2-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHRNE<br />
1,1,1-TRICHLOROETHANE<br />
CRRBON TETRACHLORIDE<br />
BROMODICHLOROMETHANE<br />
1,2-DICHLOROPROPANE<br />
TRANS-1,3-DICHLOROPROPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
DIBROflOCHLOROMETH~NE<br />
1,1,2-TRICHLOROETHANE<br />
CIS-1,3-OICHLOROPROPANE<br />
2-CHLOROETHYL VINYL ETHER<br />
BROMOFORM<br />
1,1,2,2-TETRKHLOROETHANE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,3-DICHLOROBENZENE<br />
1,2-DICHLOROBENZENE<br />
1,4-DICHLOROBEMZENE<br />
I;C/MS<br />
VOLATILE ANALYSIS<br />
AMOUNT<br />
P19111-I-l-<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
NO<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
KRECOUERY<br />
1.1111=----<br />
84.9<br />
93.8<br />
87.4<br />
DET, LIMIT<br />
.1.--====-<br />
629 ug/'kg<br />
1250 ug/kg<br />
1290 ug/kg<br />
1250 ug,'kg<br />
1250 ug/kg<br />
625 uglkq<br />
625 ugAg<br />
625 ugf'kg<br />
62hg/kg<br />
625 ug.'kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
62% ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/'kg<br />
625 ug/k.g<br />
625 ug/kg<br />
625 ug/lrg<br />
625 ug/kg<br />
625 ug/kg<br />
1250 ug/kg<br />
625 ugj'kg<br />
625 ugx'kg<br />
625 ugfkg<br />
625 ug/kg<br />
625 ,ug/kg<br />
,625 ug/kq<br />
625 ug/kg<br />
ii25 ug/kg<br />
625 ug/kg<br />
------------ ---me-----....<br />
Analyst Checked By<br />
03-lo-** THU 19:13:42 G 3 ** **** NO. 03<br />
~ -~<br />
~- ~<br />
\
C!ient ID: RAY AREA DRUM Data File:>194lU<br />
Sem~ la ID: 07-035-2478 SAMPLE COMMERFILL 711941<br />
Matrix : SOIL<br />
COMPOUND NAME<br />
1--1---1I----111---1111<br />
DICHLORODIFLUOROMETHANE<br />
CHLOROMETHANE<br />
BROMOMETHANE<br />
UINYL CHLORIDE<br />
CHLOROETHANE<br />
ETHYLENE CHLORIDE<br />
TRICHLOROFLUOROMETHANE<br />
1,l-DICHLOROETHENE<br />
Ill-DICHLOROETHANE<br />
TOTGL 1,2-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHAME<br />
1,1,1-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICHLOROMETHANE<br />
1,P-DICHLOROPROPANE<br />
TRANS-1,3-DICHLOROPROPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
DIBRONOCHLOROMETHANE<br />
1,1,2-TRICHLOROETHANE<br />
CIS-1,3-DICHLOROPROPANE<br />
2-CHLOROETHYL UIMYL ETHER<br />
BROMOFORM<br />
1,1,2,2-TETRACHLOROETHeNE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,3-DICHLOROBENZENE<br />
1,Z-DICHLOROBENZENE<br />
1,4-DICHLOROBENZENE<br />
GC/MS<br />
UOLAT I LE ANALYS 19<br />
AMOUNT<br />
IP-II-1I.D-<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
NW<br />
ND<br />
rm<br />
ND<br />
NO<br />
ND<br />
ND<br />
. ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
NO<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
1.10<br />
ND<br />
t.ID<br />
NP<br />
ND<br />
ND<br />
------------<br />
Analyst<br />
03-lo-** THU 19:12:48 G 3 ** ****<br />
DET. LIMIT<br />
I-I-=-3===<br />
625 ua/kg<br />
1250 ug/kg<br />
1250 ug/kg<br />
1250 ugj'kg<br />
1250 ug/kg<br />
625 ug./kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ugfkg<br />
625 ,ug/kg<br />
625 ug*kg<br />
625 ug/kg<br />
625 ug4.g<br />
625 ug/kg<br />
625 ug/'kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
1250 ug/kg<br />
625 ugfkg<br />
625 irgikg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
629 ug/kg<br />
------------<br />
Checked By
August 11. 1987<br />
Mr. Rich Greenwood<br />
Canonie Environmental<br />
1825 S. Grant Street, Suite 260<br />
San Mateo. CA 94402<br />
Dear Mr. Greenwood:<br />
Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />
Canonie Environmental Analytical Laboratory.<br />
Canonie Environmental SeMces Corp.<br />
212 Frank West Circle<br />
Suite A<br />
Stockton. Califomla 95206<br />
Unless o<strong>the</strong>rwise instructed by you samples will be returned or disposed of<br />
two weeks from <strong>the</strong> date of this letter.<br />
If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />
Very puly yours,<br />
Kenneth C. Wahl<br />
Manager of Laboratory Services<br />
Enclosure
Laboratory Report for<br />
Mr. Rich Greenwood<br />
Canonie Environmental<br />
1825 S. Grant Street. Suite 260<br />
San Mateo, CA 94402<br />
August 11, 1987<br />
Canonie Environmental<br />
212 Frank West Circle. Suite A<br />
Stockton, CA 95206<br />
(209) 983-1340
Sampler ID<br />
Analysis: Toxic Metals<br />
Table 1<br />
Codes of Samples Received<br />
From Bay Area Drum<br />
Project: 87-035<br />
Date Date<br />
Sampled Received Lab ID# Sample T ~ E<br />
Commerfi 11 bag 07-17-87 07-21-87 711943 Soi 1<br />
Topsoi 1 bag 07-17-87 07-21-87 711942 Soi 1<br />
08-10-1987<br />
87-035-2478<br />
Page 1<br />
Container<br />
Plastic bag<br />
Plastic bag
Sampler ID:<br />
Lab ID#:<br />
Analyte(s)<br />
Arsenic<br />
Antimony<br />
Bari um<br />
Beryllium<br />
Cadmi um<br />
Chromium<br />
Cobalt<br />
Copper<br />
Lead<br />
Mercury<br />
Molydbenum<br />
Nickel<br />
Selenium<br />
Silver<br />
Thal 1 i um<br />
Vanadium<br />
Zinc<br />
Table 2<br />
Results of Toxic Metals Analysis on Soil<br />
Samples Received From Bay Area Drum<br />
Results in mg/kg<br />
[Checked by<br />
Topsoi 1<br />
bag<br />
71 1942<br />
08-10-1987<br />
87-035-2478<br />
Page 2<br />
Note:<br />
ND X denotes none detected to a level of X.<br />
'VD X denotes none detected to a level of X due t In interfering peak. CarrorrieEnvironmental
Client ID: BAY AREA DRUM Data F~le:>1940U<br />
Sample ID: 87-035-2478 SAMPLE TOPSOIL 711940<br />
Matrlx : SOIL<br />
COMPOUND NAME<br />
.......................<br />
DICHLORODIFLUOROMETHANE<br />
CHLOROMETHANE<br />
BROMOMETHANE<br />
UINYL CHLORIDE<br />
CHLOROETHANE<br />
METHYLENE CHLORIDE<br />
TRICHLOROFLUOROMETHANE<br />
1,l-DICHLOROETHENE<br />
1,l-DICHLOROETHANE<br />
TOTAL 1,2-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHANE<br />
1,1,1-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICHLOROMETHANE<br />
1,2-DICHLOROPPOPANE<br />
TRANS-1,3-DICHLOROPROPENE<br />
TPICHLOPOETHENE<br />
BENZENE<br />
DIBRONOCHLORO~ETHANE<br />
1 ,1,2- TR I CHLOROETHANE<br />
CIS-1,3-DICHLOROPROPANE<br />
2-CHLOROETHYL VINYL ETHER<br />
BROMOFORM<br />
1,1,2,2-TETRACHLOROETHANE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,3-DICHLOROBENZENE<br />
1,2 -D I CHLOROBENZENE<br />
1,0-DI CHLOROBENZENE<br />
GC.'MS<br />
VOLATILE ANALYSIS<br />
AMOUNT<br />
-----------<br />
N D<br />
ND<br />
ND<br />
ND<br />
NCI<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
NU<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
NC<br />
ND<br />
ND<br />
ND<br />
ND<br />
DET. LIMIT<br />
----------<br />
----------<br />
625 ~ ~ / k g<br />
1250 ugjkg<br />
1250 ugx'kg<br />
1250 ugfkg<br />
1250 ug/kg<br />
625 ug4.g<br />
625 ug/kg<br />
625 ug.'ka<br />
625 ugfkg<br />
625 uq/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/kg<br />
625 ug/k.g<br />
625 ug/kg<br />
625 ug/kg<br />
625 ugikg<br />
625 ug4g<br />
625 ug/kg<br />
625 ug/kg<br />
625 uq/! g<br />
625 ug/kg<br />
1250 ug.,'kg<br />
625 ug.'kg<br />
625 ug/kg<br />
625 ug.'kg<br />
625 ug/kg<br />
625 ug&g<br />
625 ug/kg<br />
625 ug4q<br />
625 ug.'kg<br />
625 ug/kg<br />
Checked B<br />
" &honie~rwironrne&
Tlient ID: BAY AREA DRUM Data Flle:,1?41U<br />
Sarno le ID: 87-035-2478 SAMPLE COMMERFILL 711941<br />
Matrix : SOIL<br />
COMPOUND NAME<br />
.......................<br />
DICHLORODIFLUOROMETHANE<br />
CHLOROMETHANE<br />
BROROMETHANE<br />
VINYL CHLORIDE<br />
CHLOROETHANE<br />
METHYLENE CHLORIDE<br />
TRICHLOROFLUOROMETHANE<br />
. 1 ,1-D ICHLOROETHENE<br />
1,1-DICHLOROETHANE<br />
TOTAL 1,2-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLORUETHANE<br />
1,1,1-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMOOICHLOROMETHANE<br />
1,2-DICHLOROPROPANE<br />
TRANS-1,3-DICHLOROPPOPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
DIBROMOCHLOPOMETHANE<br />
1,1,2-TRICHLOROETHANE<br />
CIS-1,3-DICHLOROPROPANE<br />
2-CHLOROETHYL VINYL ETHER<br />
BROMOFORM<br />
1,1,2,2-TETRACHLOROETHQNE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,s-DICHLOROBENZENE<br />
1,2-DICHLOROBENZENE<br />
1,4-DICHLOROBENZENE<br />
D4-1,2-DICHLOROETHANE (SURF!)<br />
D8 - TOLUENE<br />
4-BROMOFLUOROBENZEl4E<br />
GUMS<br />
VOLATILE ANALYSIS<br />
AMOUNT<br />
-----------<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
tJC1<br />
DET.<br />
=====<br />
625<br />
1250<br />
125 0<br />
1250<br />
1250<br />
625<br />
625<br />
625<br />
625<br />
625<br />
625<br />
625<br />
625<br />
625<br />
625<br />
625<br />
625<br />
625<br />
025<br />
625<br />
625<br />
625<br />
1250<br />
625<br />
625<br />
625<br />
625<br />
625<br />
Ana 1 st Checked By<br />
bnonie~nvironrnental
Client ID: BAY RREA DRUM<br />
Sample ID: 87-035-2478 COMMERF I LL TUBE<br />
Matrix : SOIL<br />
COMPOUND NAME<br />
.......................<br />
N-Nitrosodimethylamine<br />
Pheno 1<br />
his(-2-Chloroethyl )E<strong>the</strong>r<br />
2-Ch loropheno 1<br />
1,3-Dichlorobenzene<br />
1,4-Dichlorobenzene<br />
1,2-Dichlorobenzene<br />
bis(2-chloroisopropy1)E<strong>the</strong>r<br />
N-Nitroso-Di-Propylamine<br />
Hexachloroethane<br />
Nitrobenzene<br />
fsophorone<br />
2-Ni t ropheno 1<br />
2,4-Dimethylphenol<br />
his(-2-Ch1oroethoxy)Methane<br />
2;4-Dichlorophenol<br />
1,2,4-Tr ich lorobenzene<br />
Naphthalene<br />
Hexachlorobutadiene<br />
4-Chloro-3-Methylphenol<br />
Hexachlorocyclopentadiene<br />
2,4,6-Trlch lorophenol<br />
2-Chloronaphthalene<br />
Dimethyl Phthalate<br />
Acenaphthylene<br />
2,6-Dlnitrotoluene<br />
Acenaph<strong>the</strong>ne<br />
2,4-Dinitrophenol<br />
4-Nitrophenol<br />
2,4-Dinitrotoluene<br />
Diethylphthalate<br />
4-Chlorophenyl-phenyle<strong>the</strong>r<br />
Fluorene<br />
Benzidine<br />
4,6-Dlnit ro-2-Methylphenol<br />
N-Nitrosodiphenylarn~ne<br />
4-Brornophenyl-phenyle<strong>the</strong>r<br />
Hexachlorobenzene<br />
Pentach lorophenol<br />
Phenanthrene<br />
Ant hracene<br />
Di-N-Butylphthalate<br />
Fluoran<strong>the</strong>ne<br />
GC/MS<br />
SEMI-UDLATILE ANALYSIS<br />
Data File:>B1941<br />
71 1941
BAY AREA DRUM<br />
711941 LP-2478<br />
PAGE 2<br />
Pyrene<br />
Butylbenzylphthalate<br />
3,3'-Dichlorobenzidine<br />
Benzo(a)Anthracene<br />
bis-(2-Ethylhexy1)Phthalate<br />
Chrysene<br />
Di-N-Octyl Phthalate<br />
Benzo(b)Fluoran<strong>the</strong>ne<br />
Benzo(k)Fluoran<strong>the</strong>ne<br />
Benzo(a )Pyrene<br />
Indeno(l,2,3-cd)Pyrene<br />
DibenzoCa ,h )Anthracene<br />
Benzo(g,h,i)Perylene<br />
Analyst Checked By
Tllent ID: BAY AREA DRUM<br />
Sarno le ID: 87-035-2478 TOPSOIL TUBE<br />
natr~x : SOIL<br />
L<br />
- COMPOQND NAME<br />
.......................<br />
N-Nitrosodirnethylarnine<br />
Pheno 1<br />
his(-2-Chloroethy1)E<strong>the</strong>r<br />
2-Chlorophenol<br />
1,3-Dichlorobenzene<br />
l,4-Dichlorobenzene<br />
1,2-Dichlorobenzene<br />
bis(2-chloroisopropy1)E<strong>the</strong>r<br />
N-Nitroso-Di-Propylarnlne<br />
Hexach lo roethane<br />
Nitrobenzene<br />
Isophorone<br />
2-Nitrophenol<br />
2,4-Dlrnethylphenol<br />
b is(-2-Ch1oroethoxy)Methane<br />
2,4-Dichlorophenol<br />
1,2,4-Tr ichlorobenzene<br />
Naphthalene<br />
Hexachlorobutadiene<br />
4-Ch loro-3-Methylphenol<br />
Hexachlorocyclopentadiene<br />
2,4,6-Tr~chlorophenol<br />
2-Chloronaphthalene<br />
Dirnethyl Phthalate<br />
Acenaphthylene<br />
2,6-Dinitrotoluene<br />
Acenaph<strong>the</strong>ne<br />
2,4-Dinitrophenol<br />
4-Ni t ropheno 1<br />
2,4-Dinitrotoluene<br />
D~ethylphthalate<br />
4-Chlorophenyl-phenyle<strong>the</strong>r<br />
Fluorene<br />
Benz id ine<br />
4,6-Dinitro-2-Methylphenol<br />
N-Nitrosodiphenylamine<br />
4-Brornophenyl-phenyle<strong>the</strong>r<br />
Hexach lorobenzene<br />
Pentachlorophenol<br />
Phenanthrene<br />
Anthracene<br />
Di-N-Butylphthalate<br />
Fluoran<strong>the</strong>ne<br />
GC/MS<br />
SEMI-VOLATILE ANALYSIS<br />
Data File:>B1940<br />
711840
ND<br />
~thalate -<br />
- ND<br />
obenz~dlne<br />
ND<br />
racene<br />
ND<br />
'xyl )Phthalate ND<br />
hthalate<br />
tn t hene<br />
lnt hene<br />
ie<br />
d)Pyrene<br />
thracene<br />
'erylene<br />
& &&+ /<br />
---- -_--__ --- ------<br />
Analyst Checked By
-<br />
Water<br />
Soi 1<br />
Reference Methods<br />
Volatile Organic Analysis<br />
Preparation Analysis<br />
x - EPA 5030<br />
ANALYST RGP<br />
1) Eisenberg. Don M. et al. "Guidelines for<br />
Addressing Fuel Leaks". California Regional<br />
Water Quality Control Board.<br />
Bay Region. Sept. 1985.<br />
San Francisco<br />
EPA 601<br />
-EPA - 602<br />
- EPA 624<br />
- EPA 8010<br />
- EPA 8020<br />
AEPA 8240<br />
Project # 87-035-2478<br />
Date fompieted 08-1 0-1 987<br />
- Guidelines for<br />
Addressing<br />
Fuel Leaks 1
Preparation<br />
Water - EPA 3510<br />
- EPA 3520<br />
- EPA 3540<br />
&PA 3150<br />
Reference Methods<br />
Semi-volatile Organics<br />
(BNA's)<br />
Analysis<br />
- EPA 625<br />
Project # 87-035-2478<br />
Date Completed m-in-1982<br />
ANALYST b
-<br />
Preparation:<br />
Reference Methods<br />
Metals<br />
Project # 87-035-2478<br />
Acid Digestion - EPA 3010<br />
- EPA 3020<br />
- EPA 3030<br />
Date Completed 08-10-1 987<br />
- EPA 3040<br />
J EPA 3050<br />
-<br />
Mercury Digestion - EPA 7470 Water<br />
-<br />
$/ EPA 7471 Soil<br />
Alkaline Digestion - EPA 3060<br />
EP Toxicity - EPA 1310<br />
CAM STLC - T itle 22 CAC<br />
ANALYST a??-
Reference Methods<br />
Metals<br />
Soi 1<br />
Atomic Absorption Metals Analysis<br />
Project # 87-035-2478<br />
Date Completed 08-10-1- ~.<br />
Graph~te Hydride Cold<br />
Element Flame Furnace Generation Vapor ICP<br />
- -<br />
A1 umi num<br />
Antimony<br />
Arsenic<br />
Barium<br />
Bery 11 ium<br />
Cadmi um<br />
Calcium<br />
Chromi urn (Total)<br />
Cobalt<br />
Copper<br />
Iron<br />
Lead<br />
Magnesium<br />
Manganese<br />
Mercury<br />
Molybdenum<br />
Nickel<br />
Potassiuii;<br />
Selenium<br />
Silver<br />
Sodium<br />
Strontium<br />
Thal 1 i urn<br />
Vanadi urn<br />
Zinc<br />
- EPA 7040<br />
- EPA 7080<br />
- EPA 7090<br />
- EPA 7130<br />
- EPA 7190<br />
- EPA 7210<br />
- EPA 7380<br />
- EPA 7420<br />
- EPA 7460<br />
- EPA 7520<br />
- EPA 7760<br />
EPA 7770<br />
- EPA 7840<br />
- EPA 7910<br />
- EPA 7950<br />
VEPA 7041<br />
>PA - 7060<br />
- EPA 7081<br />
- EPA 7091<br />
EPA 7131<br />
- EPA 7191<br />
- EPA 7211<br />
- EPA 7381<br />
- EPA 7421<br />
- EPA 7461<br />
- EPA 7521<br />
- iEPA 7740<br />
- EPA 7761<br />
,&PA 7841<br />
-EPA - 7911<br />
- EPA 7951<br />
- EPA 7061<br />
- EPA 7741<br />
- L
. . .~ tianary. netmrcmy-r~snipp~r<br />
SL(3NIVl<br />
vv<br />
'11'1 3ldWVS 31VO<br />
NO3<br />
30 IW"ls"BtS1 :SU3ldWVS 'ON 'd'l<br />
ON<br />
'-'. . - -?<br />
i 1<br />
Pl"k Lab copy<br />
.<br />
---
ILUTIDN -<br />
YORKER
I DATE ANAL: I t a m , - I
CLIENT: I. j v FIt-ee Drd!:<br />
PROJECT r: L-!-
LLIENT: hty R ~ E C P:.ur'.<br />
PROJECT *: E;7-G35-ATE .<br />
>ILUTION<br />
NORKER<br />
.A8 I.D.<br />
:lNAL<br />
-
Water<br />
Soi 1<br />
Reference Methods<br />
Grganochlorine Pesticides<br />
And PCB's<br />
Pre~aration Analysis<br />
- EPA 3510 - ~ E P A 608<br />
- *?A 3520 - EPA 625<br />
Date Completed 08-27-1987
.- -<br />
Water<br />
Soi 1<br />
Reference Methods<br />
Volatile Organic Analysis<br />
Preparation Analysis<br />
- EPA 601<br />
EPA 602<br />
~ E P 624 A<br />
- EPA 5030 - EPA 8010<br />
- EPA 8020<br />
- EPA 8240<br />
- Guidelines for<br />
Addressing<br />
Fuel Leaks 1<br />
ANALYST fi 6-4'<br />
.-<br />
1) Eisenberg. Don M. et al, "Guidelines for<br />
Addressing Fuel Leaks", California Regional<br />
Water Quality Control Board, San Francisco<br />
Bay Region, Sept. 1985.<br />
-
Water<br />
Soi 1<br />
Preparation<br />
- EPA 3510<br />
>PA 3520<br />
- EPA 3540<br />
EPA 3550<br />
Reference Methods<br />
Semi-volatile Organics<br />
(BNA's)<br />
Analysis<br />
- EPA 8270<br />
project # 87-035-03-2652<br />
Date Completed 08-37-1 9~<br />
ANALYST hq
Element<br />
A1 umi num<br />
Antimony<br />
Arsenic<br />
Barium<br />
Beryllium<br />
Cadmi um<br />
Cal ci um<br />
Chromium ( Total)<br />
Cobalt<br />
Copper<br />
Iron<br />
Lead<br />
Magnesi um<br />
Manganese<br />
Mercury<br />
Molybdenum<br />
Nickel<br />
Potassi um<br />
Selenium<br />
Silver<br />
Sod i urn<br />
Strontium<br />
Thal 1 ium<br />
Vanadi um<br />
Zinc<br />
Reference Methods<br />
Metals<br />
Water<br />
Atomic Absorption Metals Analysis<br />
Graphite Hydride<br />
- Flame Furnace Generation<br />
- EPA 202.1 EPA 202.2<br />
- EPA 204.1 TEPA - 204.2<br />
Cold<br />
Vapor<br />
&PA 206.2 EPA 206.3<br />
- -<br />
EPA 208.1 - EPA 208.2<br />
EPA 210.1 EPA 210.2<br />
-. A<br />
- EPA 213.1 - EPA 213.2<br />
- EPA 215.1<br />
- EPA 218.1 - EPA 218.2<br />
- EPA219.1 EPA219.2<br />
A EPA 220.1 - EPA 220.2<br />
- EPA 236.1 - EPA 236.2<br />
- EPA 239.1 - EPA 239.2<br />
- EPA 242.1<br />
- EPA 243.1 - EPA 243.2<br />
- EPA 246.1 - EPA 246.2<br />
EPA 249.1 EPA 249.2<br />
-EPA A 258.1 -<br />
JEPA 270.2 EPA 270.3<br />
- EPA 272.1 - -EPA 272.2 -<br />
- EPA 273.1<br />
- EPA 279.1 - JEPA 279.2<br />
- EPA 286.1 - EPA 286.2<br />
- EPA 289.1 - EPA 289.2<br />
ANALYST 98<br />
Project # 87-035-03-2652<br />
Date Completed 08-27-1987<br />
- JEPA 245.1<br />
- ICP<br />
- EPA 200.7<br />
- EPA 200.7<br />
- EPA 200.7<br />
- JEPA 200.7<br />
- /EPA 200.7<br />
- &PA 200.7<br />
- EPA 200.7<br />
- YEPA 200.7<br />
- /€PA 200.7<br />
- JEPA 200.7<br />
- EPA 200.7<br />
- r/EPA 200.7<br />
- EPA 200.7<br />
- EPA 200.7<br />
- JEPA 200.7<br />
- &PA 200.7<br />
- EPA 200.7<br />
- EPA 200.7<br />
- /EPA 200.7<br />
- EPA 200.7<br />
EPA 200.7<br />
~ E P A 200.7<br />
&PA 200.7
Sampler ID:<br />
Lab ID#:<br />
Anal yte(s)<br />
Arsenic<br />
Antimony<br />
Barium<br />
Beryllium<br />
Cadmium<br />
Chromium<br />
Cobalt<br />
Copper<br />
Lead<br />
Mercury<br />
Molybdenum<br />
Nickel<br />
Selenium<br />
Silver<br />
Thallium<br />
Vanadium<br />
Zinc<br />
Table 2<br />
Results of CAM Metals TTLC Analysis on Water<br />
Samples Received From Bay Area Drum<br />
Results in mg/l<br />
Boiler<br />
Tank<br />
71 4054<br />
08-27-1987<br />
87-035-03-2652<br />
Page 2<br />
Note:<br />
ND X denotes none detected to a level of X.<br />
ND X denotes none detected to a level of X due an interfering peak. @an~ouieEnvironrnental
Sampler ID:<br />
Lab ID#:<br />
I I<br />
Table 3<br />
Results of Organochlorine Pesticides Analysis on Water<br />
Samples Received From Bay Area Drum<br />
Results in ug/l<br />
Analyte(s)<br />
Aldrin<br />
Alpha BHC<br />
Beta-BHC<br />
Del ta-BHC<br />
Gamma-BHC<br />
Chlordane<br />
4.4'-DDD<br />
4,4'-DDE<br />
4,4'-DDT<br />
Dieldrin<br />
Endosulfan I<br />
Endosulfan I1<br />
Endosulfan Sulfate<br />
Endrin<br />
Endrin Aldehyde<br />
Heptachlor<br />
Heptachlor Epoxide<br />
Toxaphene<br />
PCB quantified as 1242<br />
PCB quantified as 1254<br />
PCB quantified as 1260<br />
T plr<br />
Analyst C ecked by<br />
Boi 1 er<br />
Tank<br />
714054<br />
08-27-1 987<br />
87-035-03-2652<br />
Page 3<br />
Note:<br />
ND X denotes none detected to a level of X.<br />
YD X denotes none detected to a level of X due t in interfering peak. Call~~~ieEnvironmental
Ciient ID: BAY WEA DRUM Data File:>4053U<br />
Samole ID: 87-035-03-2652 SAMPLE ST-1 714053<br />
Matrix : LIQUID<br />
COMPOUND NAME<br />
GC/MS<br />
VOLATILE ANALYSIS<br />
-I-*---------------____<br />
--I-------=<br />
DICHLORODIFLUOROMETHANE<br />
CHLOROMETHANE<br />
BROMOMETHANE<br />
VINYL CHLORIDE<br />
CHLOROETHANE<br />
METHYLENE CHLORIDE<br />
TRICHLOROFLUORONETHANE<br />
1,l-DICHLOROETHENE<br />
1 -1-D I CHLOROETHANE<br />
TOTAL 1, 2-D I CHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHANE<br />
1,1,1-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICHLDROMETHANE<br />
1,2-DICHLOROPROPANE<br />
TRANS-1,3-DICHLOROPROPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
DIBROMOCHLOROMETHANE<br />
1,1,2-TRICHLOROETHANE<br />
CIS-1,3-DICHLOROPROPANE<br />
2-CHLOROETHYL VINYL ETHER<br />
BROMOFORM<br />
1,1,2,2-TETRACHLORDETHANE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,3-DICHLOROBENZENE<br />
1 ,2-Dl CHLOROBENZENE<br />
1,4-DICHLOROBENZENE<br />
SURROGATE STANDARD<br />
-====-========m=======m-===<br />
D4-1,2-DICHLOROETHANE (SURR)<br />
DB-TOLUENE (SURR<br />
4-BROMOFLUOROBENZENE (SURR)<br />
AMOUNT<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
470.<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
2500.<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
DETECTION LIMIT RAISED DUE TO MATRIX INTERFERENCE<br />
DET. LIMIT<br />
----=----P<br />
250 ug/L<br />
500 ug/L<br />
500 ug/L<br />
500 ug/L<br />
500 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
500 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
Analyst Checked By<br />
CanonieErwironmenta1
Client ID: BAY AREA DRUM Data File:>4054U<br />
Sample ID: 87-035-03-2652 SAMPLE BOILER TANK 714054<br />
Matrix : LIQUID<br />
COMPOUND NAME<br />
DICHLORODIFLUOROHETHANE<br />
CHLOROMETHANE<br />
BROMOMETHANE<br />
VINYL CHLORIDE<br />
CHLOROETHANE<br />
METHYLENE CHLORIDE<br />
TRICHLOROFLUOROMETHANE<br />
1,l-DICHLOROETHENE<br />
1 ,1-D I CHLOROETHANE<br />
TOTAL 1,2-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHANE<br />
1,1,1-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICHLOROHETHANE<br />
1,2-DICHLOROPROPANE<br />
TRANS-1,3-DICHLOROPROPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
DIBROMOCHLOROMETHANE<br />
1,1,2-TRICHLOROETHANE<br />
CIS-1,3-DICHLOROPROPANE<br />
2-CHLOROETHYL VINYL ETHER<br />
BROMOFORN<br />
1,1,2,2-TETRACHLOROETHANE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,3-DICHLOROBENZENE<br />
1,2-DICHLOROBENZENE<br />
1,4-DICHLOROBENZENE<br />
SURROGATE STANDARD<br />
D4-1,2-DICHLOROETHANE (SURR)<br />
D8-TOLUENE ( SURR<br />
4- BROMOFLUOROBENZENE ( SUR~ )<br />
GC/MS<br />
VOLATILE ANALYSIS<br />
AMOUNT<br />
__-=m-__L--<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
1100.<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
DETECTION LIMIT RAISED DUE TO MATRIX INTERFERENCE<br />
DET. LIMIT<br />
----==----<br />
250 ug/L<br />
500 ug/L<br />
500 ug/L<br />
500 ug/L<br />
500 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
500 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 . ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
250 ug/L<br />
Analyst Checked By
Client ID: RAY AREA DPUU<br />
Sample ID: 87-035-2652 ST1<br />
Matrix : WATER<br />
COMPOUND NAME<br />
.......................<br />
Y-Nitrosodimethylamine<br />
Pheno 1<br />
his(-2-Chloroethyl )E<strong>the</strong>r<br />
2-Ch loropheno 1<br />
1,3-Dich lorobenzene<br />
1,4-Dich lorobenzene<br />
l,2-Dichlorobenzene<br />
bis(2-chloroisopropyl>E<strong>the</strong>r<br />
N-Nitroso-Di-Propylamine<br />
Hexachloroethane<br />
Nitrobenzene<br />
Isophorone<br />
2-Ni t ropheno 1<br />
2;4-Dimethylphenol<br />
his(-2-Ch1oroethoxy)Methane<br />
2:d-Dichlorophenol<br />
1,2,4-Trichlorobenzene<br />
Naphthalene<br />
Hexachlorobutadiene<br />
4-Chloro-3-Methylphenol<br />
Henachlorocyclopentadiene<br />
2:4;6-Trichloropheno1<br />
2-Chloronaphthalene<br />
Dimethyl Phthalate<br />
Acsnaphthylene<br />
2;6&Dinitrotoluene<br />
Acenaph<strong>the</strong>ne<br />
2,4-Dinitrophenol<br />
4-Nitrophenol<br />
2.4-Dinitrotoluene<br />
~ieth~lphthalate<br />
4-Chlorophenyl-phenyle<strong>the</strong>r<br />
Fluorene<br />
Benzidine<br />
4,6-Dinitro-2-Methylphenol<br />
N-Nitrosodiphenylamine<br />
4-Bromoohenyl-phenyle<strong>the</strong>r<br />
Hexachlorobenzene<br />
Pentachlorophenol<br />
Phenanthrene<br />
Anthracene<br />
Di-N-Butylphthalate<br />
Fluoran<strong>the</strong>ne<br />
GC/MS<br />
SEMI-VOLATILE ANALYSIS
BAY QREQ DRUM<br />
714053 LP-2652<br />
PAGE 2<br />
,Irene<br />
p ,-<br />
Butylbenzylphthalate<br />
3:3'-Dichlorobenzidine<br />
Benzo(a1Anthracene<br />
bis-(2-Ethylhexy1)Phthalate<br />
Chrysene<br />
Di-N-Octyl Phthalate<br />
Benzo(b1Fluoran<strong>the</strong>ne<br />
Benzo(k IFluoran<strong>the</strong>ne<br />
Benzo (a )Pyrene<br />
Indeno(l,2,3-cd)Pyrene<br />
Dibenzo(a,h)Anthracene<br />
Benzo(q:h:i)Perylene<br />
Analyst Checked Bu
Cl~ent ID: EQY APEA DRUM<br />
Sam@ le ID: 57-035-2652 BOILER TQYW<br />
Matr~x : UATEP<br />
COMPOUND NPYE<br />
.......................<br />
N-Ni t rosodimethylamine<br />
Pheno 1<br />
bisl-2-Chloroethy1)E<strong>the</strong>r<br />
2-Chlorophenol<br />
1 :3-Dich lorobenzene<br />
1,4-Dich lorobenzene<br />
1 ,2-Dichlorobenzene<br />
bis(2-chloroisopropyl>E<strong>the</strong>r<br />
N-Ni t roso-Di-Propylarnine<br />
Hexachloroethane<br />
Nitrobenzene<br />
Isophorone<br />
2-Nitrophenol<br />
2,4-Dimethylphenol<br />
his(-2-Ch1oroethoxy)Methane<br />
2,4-Dichlorophenol<br />
1,2,4-Trichlorobenzene<br />
Naphthalene<br />
Herachlorobutadiene<br />
4-Ch loro-3-Methylphenol<br />
Hexach lorocyc lopentadiene<br />
2,4,6-Trichlorophenol<br />
2-Chloronaphthalene<br />
Pirnethyl Phthalate<br />
Acenaphthulene<br />
2:6-Dinitrotoluene<br />
Acenaph<strong>the</strong>ne<br />
2,4-Dinitrophenol<br />
4-Ni t ropheno 1<br />
2,4-Dinitrotoluene<br />
Diethylphthalate<br />
4-Chlorophenyl-phenyle<strong>the</strong>r<br />
Fluorene<br />
Benzidine<br />
4,6-Dinitro-2-Methylphenol<br />
N-Ni t rosod ipheny larnine<br />
4-Bromopheny 1-phenyle<strong>the</strong>r<br />
Hexachlorobenzene<br />
Pentachlorophenol<br />
Phenant hrene<br />
Anthracene<br />
Di-N-Butylphthalate<br />
Fluoran<strong>the</strong>ne<br />
r;C/US<br />
SEMI-VOLATILE ANALYSIS<br />
Data File:>R4054<br />
714054
BAY AREA DRUM<br />
714054 LP-2652<br />
PAGE 2<br />
Py~rene<br />
Butylbenzylphthalate<br />
3:3'-Dichlorobenzidine<br />
Benzo(a!Anthracene<br />
bis-(2-Ethy1hexyl)Phthalate<br />
Chrysene<br />
Di-N-Octyl Phthalate<br />
Benzo(b )Fluoran<strong>the</strong>ne<br />
Renzo(k!Fluoran<strong>the</strong>ne<br />
Benzo (a )Pyrene<br />
Indeno
BAY ARER DRUM<br />
714054 LP-2652<br />
PAGE 2<br />
Pyrene<br />
Butylbenzylphthslate<br />
3,3'-Diehlorobenzld~ne<br />
Benzo(a)Anthrscene<br />
bis-(2-Ethylhexy1)Phthalate<br />
Chryaene<br />
bi-N-Octyl Phthalate<br />
Benzotb)Fluoran<strong>the</strong>ne<br />
Benzo(k)Fluoran<strong>the</strong>ne<br />
Benzo(s)Pyrene<br />
Indeno(l,2,3-cd)Pyrcnc<br />
Dibanzo(a,h)Anthrecens<br />
Benzo(g,h,i)Perylene
October 21, 1987<br />
- Environmental<br />
Ms. Irene Fanelli<br />
Canonie Environmental<br />
1825 S. Grant Street. Suite 260<br />
San Mateo. CA 94402<br />
Dear Ms. Fanelli:<br />
Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />
Canonie Environmental Analytical Laboratory.<br />
Canonw Enwronmental Se~ces Corp<br />
212 Frank West Clrcie<br />
Suite A<br />
Stockton. Caiifomia 95206<br />
Phone: 209-983-1340<br />
Unless o<strong>the</strong>rwise instructed by you samples will be returned or disposed of<br />
two weeks from <strong>the</strong> date of this letter.<br />
If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />
Very truly yours,<br />
Kenneth C. Wahl<br />
Manager of Laboratory Services<br />
Enclosure
Laboratory Report for<br />
Ms. Irene Fanelli<br />
Canonie Environmental<br />
1825 S. Grant Street, Suite 260<br />
San Mateo. CA 94402<br />
October 21, 1987<br />
Canonie Environmental<br />
212 Frank West Circle. Suite A<br />
Stockton, CA 95206<br />
(209) 983-1 340
N<br />
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L a<br />
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F a .. n E a+<br />
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MVIVI<br />
VlLoLo<br />
a m a<br />
L L L<br />
mmm
Sampler ID:<br />
Lab ID#:<br />
Analyte(s)<br />
Bromodichloromethane<br />
Bromof orm<br />
Bromomethane<br />
Carbon tetrachloride<br />
Chlorobenzene<br />
Chloroethane<br />
2-Chloroethylvinyl e<strong>the</strong>r<br />
Chloroform<br />
Chloromethane<br />
Dibromochloromethane<br />
1.2-Dichlorobenzene<br />
1.3-Dichlorobenzene<br />
1,4-Dichlorobenzene<br />
Dichlorodifluoromethane<br />
1.1-Dichloroethane<br />
1.2-Dichloroethane<br />
1,l-Dichloroe<strong>the</strong>ne<br />
trans-1.2-Dichloroe<strong>the</strong>ne<br />
1,2-Dichloropropane<br />
cis-1.3-Dichloropropene<br />
trans-1,3-Dichloropropene<br />
1.1.2.2-Tetrachloroethane<br />
Tetrachloroe<strong>the</strong>ne<br />
l.l,l-Trichloroethane<br />
1,1.2-Trichloroethane<br />
Trichloroe<strong>the</strong>ne<br />
Trichlorofluoromethane<br />
Vinyl chloride<br />
Methylene chloride<br />
51 mp<br />
AnBlyst Chec ed by<br />
Table 2<br />
Results of Purgeable Halocarbons Analysis on Soil<br />
Samples Received From Bay Area Drum<br />
Results in mg/kg<br />
10-20-1987<br />
87-035-2872<br />
Page 2
u<br />
-<br />
Water<br />
Soi 1<br />
Reference -Methods<br />
Volatile Organic Analysis<br />
Preparation Analysis<br />
ANALYST<br />
- 1) Eisenberg. Don M.. et al, "Guidelines for<br />
Addressing Fuel Leaks", California Regional<br />
Water Qua1 ity Control Board. San Francisco<br />
Bay Region, Sept. 1985.<br />
EPA 601<br />
-EPA - 602<br />
EPA 624<br />
- Guidelines for<br />
Addressing<br />
Fuel Leaks 1
ili3NlVl 0'1 3ldWVS 3110<br />
NO3<br />
do x 4117/ii/)2/<br />
I*ml."81Sl :Sli3ldWIS 'ON 'dl<br />
'ON
October 19, 1987<br />
Mr. Rich Greenwood<br />
Canonie Environmental<br />
1825 S. Grant Street, Suite 260<br />
San Mateo, CA 94402<br />
Dear Mr. Greenwood:<br />
Environmental<br />
Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />
Canonie Environmental Analytical Laboratory.<br />
Canonie Enviionmenta Sewices Cop.<br />
212 Frank West Circle<br />
Suite A<br />
Stockton, Caiiiomia 95206<br />
Unless o<strong>the</strong>rwise instructed by you samples w i l l be returned or disposed of<br />
two weeks from <strong>the</strong> date of this letter.<br />
If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />
Very truly yours,<br />
Kenneth C. Wahl<br />
Manager of Laboratory Services<br />
Enclosure
Laboratory Report for<br />
Mr. Rich Greenwood<br />
Canonie Environmental<br />
1825 S. Grant Street, Suite 260<br />
San Mateo, CA 94402<br />
October 19, 1987<br />
Canonie Environmental<br />
212 Frank West Circle, Suite A<br />
Stockton, CA 95206<br />
(209) 983-1340
m<br />
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mw<br />
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0<br />
"lmm<br />
"lmm<br />
a m a<br />
L L L<br />
mmm
Sampler ID:<br />
- Andlyte(s)<br />
Bron~od ichloroniethane<br />
bromof or111<br />
Bru~~~ol~~ul.t~urle<br />
Curbun tetruchloride<br />
Chlorobenzene<br />
Chloroethane<br />
2-Chloroethylvinyl e<strong>the</strong>r<br />
Chlorof'orm<br />
Chlorosiethane<br />
Oi bron~ochlorornethane<br />
1,2-Dichlorobenzene<br />
1,3-Dichlorobenzene<br />
1.4-Oichlorobenzene<br />
Dichlorodif luoroo~ethane<br />
1,l-Oichloroethane<br />
1.2-Oichloroethane<br />
1.1-Oicliloroe<strong>the</strong>ne<br />
trans-'I. 2-Dichloroe<strong>the</strong>ne<br />
1,Z-Dichloropropane<br />
cis-1.3-Dichloropropene<br />
trans-1,3-Dichloropropene<br />
1.1.2.2-Tetrachloroethane<br />
Tetrachloroe<strong>the</strong>ne<br />
l.l,l-Trichloroethane<br />
1,1.2-Trichloroethane<br />
Trichloroe<strong>the</strong>ne<br />
Trichlurof luoron~ethane<br />
Vinyl chloride<br />
Methylene chloride<br />
Sj ma-<br />
AndI)-st Checked by<br />
Table 2<br />
Results of Purgeable Halocarbons Analysis on Soil<br />
Samples Received From Bay Area Drum<br />
Results in nlg/kg<br />
10-16-1987<br />
87-035-2865<br />
Page 2
u<br />
-<br />
Water<br />
Soi 1<br />
Reference Methods<br />
Volatile Organic Analysis<br />
Preparation Analysis<br />
EPA 601<br />
-EPA - 602<br />
- EPA 624<br />
- EPA 5030 $PA 8010<br />
- EPA 8020<br />
- EPA 8240<br />
ANALYST<br />
1) Eisenberg, Don M.. et al, "Guidelines for<br />
Addressing Fuel Leaks". California Regional<br />
- Water Quality Control Board. San Francisco<br />
Bay Region. Sept. 1985.<br />
5.p<br />
project # 87-035-2865<br />
Date Completeqo-16-1 q87<br />
- Guidelines for<br />
Addressing<br />
Fuel Leaks 1
Sampler ID:<br />
Lab ID#:<br />
Analyte(s)<br />
Antimony<br />
~rsenic-<br />
Bari urn<br />
Beryllium<br />
Cadmium<br />
Chromium<br />
Cobalt<br />
Copper<br />
Lead<br />
Mercury<br />
Molybdenum<br />
Nickel<br />
Selenium<br />
Silver<br />
Thallium<br />
Vanadium<br />
Zinc<br />
Table 2<br />
Results of Toxic Metals Analysis on Soil<br />
Samples Received From Bay Area Drum<br />
Results in mg/kg<br />
AG BASE PERM. SAND<br />
11-13-1987<br />
87-035-3020<br />
Page 2<br />
Note:<br />
ND X denotes none detected to a level of X.<br />
IN0 X denotes none detected to a level of X due to an interfering peak. Canonielh I!II.~ fl ilrxrlt
NOV 13 '87 15:40 CRNONIE, STOCKTON<br />
Client ID: BAY AREA DRUM<br />
Sample ID: 87-035-3020<br />
Matrix : SOIL<br />
Phenol<br />
bis(-2-Chloroethy1)E<strong>the</strong>r<br />
2-Chlorophenol<br />
1,3-Dicniorobenzene<br />
;,4-Dichiorobenzene<br />
1,2-Dichlorobenzene<br />
bis(2-chioroisopropy1)E<strong>the</strong>r<br />
N-Nitroso-Di-Propylamine<br />
Hexachloroethane<br />
Nitrobenzene<br />
Isophorone<br />
2-Nitrophenol<br />
2,4-Dimethylphenol<br />
bis(-2-Ch1oroethoxy)Methane<br />
2,4-Dichiorophenol<br />
1,2,4-Trichlorobenzene<br />
Naphthalene<br />
Hexachlorobutadiene<br />
4-Chioro-3-Methylphenol<br />
Hexachlorocyclopentadiene<br />
2,4,6-Trichlorophenol<br />
2-Chloronaphthalene<br />
Dimethyl Phthalate<br />
Acenaphthylene<br />
2,6-Dinitrotoluene<br />
Acenaph<strong>the</strong>ne<br />
2,4-Dinitrophenol<br />
4-Nitrophenol<br />
2,4-Dinitrotoluene<br />
Diethylphthalate<br />
4-Chlorophenyl-phenyle<strong>the</strong>r<br />
Fluorene<br />
Benzidine<br />
4.6-~initro-2-Methylphenol<br />
N-Nitrosodiphenylamine<br />
4-Bromophenyl-phenyle<strong>the</strong>r<br />
Hexachlorobenzene<br />
Pentachlorophenol<br />
Phenanthrene<br />
Anthracene<br />
Di-N-Butylphthalate<br />
Fluoran<strong>the</strong>ne<br />
AMOUNT<br />
===========<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
XD<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
Data ~ile:>B9153<br />
719153
BAY AREA DRUM<br />
719153 X87-035-3020<br />
PAGE 2<br />
Pyrexe<br />
Butylbenzylphthalate<br />
3,3'-Dichlorobenzidine<br />
L.<br />
- Benzo(a)Anthracene<br />
bis-(2-Ethy1hexyl)Phthalate<br />
Chrysene<br />
Di-N-Occyl Phthalaze<br />
bis-(2-Ethyihexy?)Phtkahte<br />
Chrysene<br />
Di-N-Octyl Phthalate<br />
Benzo(b)F:uorac<strong>the</strong>ce<br />
Benzo(k)Fluoran<strong>the</strong>ne<br />
Benzo(a)Pyrece<br />
Indeno(:,2,3-cd)Pyrene<br />
Dibenzo(a,h)Anthracene<br />
Benzo(g,h,i)Perylene<br />
Analyst Checked By
Client ID: BAY AREA DRUM<br />
Sample ID: 87-035-3020<br />
Matrix : SOIL<br />
COMPOUND NAME<br />
GC/MS<br />
SEMI-VOLATILE AANLYSIS<br />
.......................<br />
N-Nitrosodimethylamine<br />
Phenol -<br />
bis(-2-Chloroethy1)E<strong>the</strong>r<br />
2-Chlorophenol<br />
1,3-Dichiorobenzene<br />
1,4-Dichlorobenzene<br />
1,2-Dichlorobenzene<br />
bis(2-chloroisopropy1)E<strong>the</strong>r<br />
N-Nitroso-Di-Propylamine<br />
Hexachloroethane<br />
Nitrobenzene<br />
Isophorone<br />
2-Nitrophenol<br />
2,4-Dimethylphenol<br />
his(-2-Ch1oroethoxy)Methane<br />
2,4-Dichlorophenol<br />
1,2,4-Trichlorobenzene<br />
Naphthalene<br />
Hexachlorobctadiene<br />
4-Chloro-3-Methylphenol<br />
Hexachlorocyclopentadiene<br />
2,4,6-Trichlorophenol<br />
2-Chloronaphthaiene<br />
Dimethyl Phthalate<br />
- Acensphthylene<br />
2,6-Dinitrotoluene<br />
Acenaph<strong>the</strong>ne<br />
2,4-Dinitrophenol<br />
4-Nitrophenol<br />
2,4-Dinitrotoluene<br />
Diethylphthalate<br />
4-Chlorophenyl-phenyle<strong>the</strong>r<br />
Fluorene<br />
Benzidine<br />
4,6-Dinitro-2-Methylphenol<br />
N-Nitrosodiphenylamine<br />
4-Bromophenyl-phenyle<strong>the</strong>r<br />
Hexachlorobenzene<br />
Pentachlorophenol<br />
Phenanthrene<br />
Anthracene<br />
Di-N-Butylphthalate<br />
Fluoran<strong>the</strong>ne<br />
AMOUNT<br />
-----------<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
Data Filt:>R9152<br />
719152<br />
DET. LIMIT<br />
----------<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 uc/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 uq/kg<br />
660 ug/kg<br />
660 ug/kg<br />
3300 ug/kg<br />
3300 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
3300 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
3300 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg<br />
660 ug/kg
BAY AREA DRUM<br />
719152 W87-035-3020<br />
PAGE 2<br />
Pyrene<br />
Butylbenzylphthalate<br />
u 3,3'-Dichlorobenzidine<br />
- Benzo(a)Anthracene<br />
bis-(2-Ethylhexy1)Phthalate<br />
Chrysene<br />
Di-N-Octyl Phthalate<br />
bis-(2-Ezky1hexyi)Phthalate<br />
Chryse~e<br />
Di-N-Octyl Phthalate<br />
Benzo(b)Fluoran<strong>the</strong>ne<br />
Benzo(k)Fiuoran<strong>the</strong>ne<br />
Benzo(a)Pyrene<br />
Indeno(l,2,3-cd)Pyrene<br />
Dibenzo(a,h)Anthracene<br />
Benzo(g,h,i)Perylene<br />
Analyst Checked By
Client ID: BAY AREA DRUM<br />
Sample ID: 87-035-3020<br />
Matrix : SOIL SAMPLE: AG BASE<br />
COMPOUND NAME<br />
.......................<br />
DICHLORODIFLUOROMETHANE<br />
L<br />
- CHLOROMETHANE<br />
BROMOMETHANE<br />
VINYL CHLORIDE<br />
CHLOROETHANE<br />
METHYLENE CHLORIDE<br />
TRICHSOROFLUOROMETHANE<br />
1,i-DICHLOROETHENE<br />
1,l-DICHLOROETHANE<br />
TOTAL 112-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICHLOROMFTHANE<br />
TRANS- 1,3-DICHLOROPROPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
DIBROMOCHLOROKETHANE<br />
1,1,2-TRICHLOROEISANE<br />
CIS-1,3-DICHLORO?ROPAXE<br />
2-CHLOROE'THYL VINYL ETHER<br />
- BROMOFOFX<br />
l,i,2,2-TETFSCHLO3OET:iANE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,3-DICHLOROBENZENE<br />
1,2-DICHLOROBENZENE<br />
114-DICHLOROBENZENE<br />
TOTAL XYLENE<br />
2-PROPANONE (ACETONE)<br />
GC/MS<br />
VOLATILE ANALYSIS<br />
Data File:>9152V<br />
719152<br />
Checked By
Client ID: BAY AREA DRUM<br />
Sample ID: 87-035-3020<br />
Matrix : SOIL SAMPLE-: PER. SAND<br />
COMPOUND N WE<br />
.......................<br />
DICHLORODIFL,OROMETHANE<br />
.- - CHLOROMETHANS<br />
BROMOMETHWE<br />
VINYL CHLORIIE<br />
CHLOilOETHAtiF<br />
METHYLENE CELORIDE<br />
TRICELOROFKOXOMETHANE<br />
1,l-DICHLOROETHENE<br />
1,l-DICHLOROETHANE<br />
TOTAL 1,2-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHANE<br />
1,1,1-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICfiLOROMETHANE<br />
1,2-DICHLOR07ROPAKE<br />
TRAhS-1,3-DICHLOROPROPENE<br />
TRICELOROETEENE<br />
BENZENE<br />
DIBROMOCHLOROMETHANE<br />
1,1,2-TRICHLOXOETHANE<br />
CIS-Ij3-DICEIOROPROPANE<br />
2-CHLOROETEYL VINYL ETHER<br />
- BROXOFORM<br />
1,1,2,2-TEl.7-.CHLOROETEANE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
TOTAL XYLENE<br />
2-PROPANONE (ACETONE)<br />
GC/MS<br />
VOLATILE ANALYSTS<br />
AMOUNT<br />
-----------<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
N3<br />
ND<br />
ND<br />
ND<br />
ND<br />
Nrl<br />
N3<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
Data File:>9153V<br />
719153<br />
DE?. LIMIT<br />
----------<br />
125 ug/kg<br />
250 ug/kg<br />
250 ug/kg<br />
250 ug/kg<br />
258 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
250 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
i25 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
Checked By
November 14. 1987<br />
Mr. Kurt Ah1 ich<br />
Canonie Environmental<br />
1825 S. Grant Street, Suite 260<br />
San Mateo, CA 94402<br />
Dear Mr. Ahlich:<br />
Environmental<br />
Canonie Environmental Services COP<br />
212 Frank West Circle<br />
Suite A<br />
Stockton. California 95206<br />
Phone: 209.983-1340<br />
87-035-3020<br />
Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />
Canonie Environmental Analytical Laboratory.<br />
Unless o<strong>the</strong>rwise instructed by you samples will be returned or disposed of<br />
two weeks from <strong>the</strong> date of this letter.<br />
If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />
Very truly yours,<br />
Kenneth C. Wahl<br />
Manager of Laboratory Services<br />
Enclosure
Laboratory Report for<br />
Mr. Kurt Ahlich<br />
Canonie Environmental<br />
1825 S. Grant Street, Suite 260<br />
San Mateo, CA 94402<br />
November 14. 1987<br />
Canonie Environmental<br />
212 Frank West Circle, Suite A<br />
Stockton, CA 95206<br />
(209) 983-1 340
Sampler - ID<br />
Analysis: Toxic Metals<br />
Table 1<br />
Codes of Samples Received<br />
From Bay Area Drum<br />
Project: 87-035<br />
Date Date<br />
Sampled Received Lab ID# Sample Type<br />
AG BASE 11-04-87 11-06-87 7191 52 Soi 1<br />
PERM. SAND 11-04-87 11-06-87 719153 Soi 1<br />
11-13-1~87<br />
87-035-3020<br />
Page 1<br />
Container<br />
Mason Jar<br />
Mason Jar
PROJ. NO. I PROJECI NAME<br />
p-0~~3 -)jA)' A-pGn<br />
L.P. NO. SAMPLERS: ISlgnalur4<br />
DATE I SAMPLE 1.0<br />
j3P d w<br />
Recslvsd lor Laboratoq by:<br />
ISIgn.tur.)<br />
NO.<br />
CON^<br />
TAINERS<br />
Zanonle Environmental, 212 Frank West Circle, Sulte A, Stockton, CA 95206
Sampler ID:<br />
Lab ID#:<br />
Analyte(s)<br />
Antimony<br />
Arsenic<br />
Bari um<br />
Beryllium<br />
Cadmi um<br />
Chromium<br />
Cobalt<br />
Copper<br />
Lead<br />
Mercury<br />
Molybdenum<br />
Nickel<br />
Selenium<br />
Silver<br />
Thal 1 i urn<br />
Vanadium<br />
Zinc<br />
able 2<br />
Results of Toxic Metals Analysis on Soil<br />
Samples Received From Bay Area Drum<br />
Results in mg/kg<br />
AG BASE PERM. SAND<br />
11-13-1~d7<br />
87-035-3020<br />
Page 2<br />
Note:<br />
ND X denotes none detected to a level of X.<br />
#ND X denotes none detected to a level of X due to an interfering peak. CanonieEnvi ronmenbl
Client ID: BAY AREA DRUM<br />
Sample ID: 87-035-3020<br />
Matrix : SOIL<br />
COMPOUND NAME<br />
.......................<br />
N-Nitrosodimethylamine<br />
Phenol<br />
bis(-2-Chloroethy1)E<strong>the</strong>r<br />
2-Chlorophenol<br />
1,3-Dichlorobenzene<br />
1,4-Dichlorobenzene<br />
1,2-Dichlorobenzene<br />
bis(2-chloroisopropy1)E<strong>the</strong>r<br />
N-Nitroso-Di-Propylamine<br />
Hexachloroethane<br />
Nitrobenzene<br />
Isophorone<br />
2-Nitrophenol<br />
2,4-Dimethylphenol<br />
bis(-2-Ch1oroethoxy)Methane<br />
2,4-Dichlorophenol<br />
1,2,4-Trichlorobenzene<br />
Naphthalene<br />
Hexachlorobutadiene<br />
4-Chloro-3-Methylphenol<br />
Hexachlorocyclopentadiene<br />
2,4,6-Trichlorophenol<br />
2-Chloronaphthalene<br />
Dimethyl Phthalate<br />
Acenaphthylene<br />
2,6-Dinitrotoluene<br />
Acenaph<strong>the</strong>ne<br />
2,4-Dinitrophenol<br />
4-Nitrophenol<br />
2,4-Dinitrotoluene<br />
Diethylphthalate<br />
4-Chlorophenyl-phenyle<strong>the</strong>r<br />
Fluorene<br />
Benzidine<br />
4,6-Dinitro-2-Methylphenol<br />
N-Nitrosodiphenylamine<br />
4-Bromophenyl-phenyle<strong>the</strong>r<br />
Hexachlorobenzene<br />
Pentachlorophenol<br />
Phenanthrene<br />
Anthracene<br />
Di-N-Butylphthalate<br />
Fluoran<strong>the</strong>ne<br />
GC/MS<br />
SEMI-VOLATILE ANALYSIS<br />
AMOUNT<br />
-----------<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
Data File:>B9153<br />
719153<br />
DET. LIMIT<br />
----------<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
1650 ug/kg<br />
1650 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
1650 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
1650 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg<br />
330 ug/kg
BAY AREA DRUM<br />
719153 #87-035-3020<br />
PAGE 2<br />
Pyrene<br />
Butylbenzylphthalate<br />
3,3'-Dichlorobenzidine<br />
Benzo(a)Anthracene<br />
bis-(2-Ethylhexy1)Phth<br />
Chrysene<br />
Di-N-Octyl Phthalate<br />
ate<br />
bis-(~-~th~lhex~l)~hthalate<br />
Chrysene<br />
Di-N-Octyl Phthalate<br />
Benzo(b)Fluoran<strong>the</strong>ne<br />
Benzo(k)Fluoran<strong>the</strong>ne<br />
Benzo(a)Pyrene<br />
Indeno(l,2,3-cd)Pyrene<br />
Dibenzo(a,h)Anthracene<br />
Benzo(g,h,i)Perylene<br />
Checked By
Client ID: BAY AREA DRUM<br />
Sample ID: 87-035-3020<br />
Matrix : SOIL<br />
COMPOUND NAME<br />
.......................<br />
N-Nitrosodimethylamine<br />
Phenol<br />
bis(-2-Chloroethy1)E<strong>the</strong>r<br />
2-Chlorophenol<br />
1,3-Dichlorobenzene<br />
1,4-Dichlorobenzene<br />
1,2-Dichlorobenzene<br />
bis(2-chloroisopropy1)E<strong>the</strong>r<br />
N-Nitroso-Di-Propylamine<br />
Hexachloroethane<br />
Nitrobenzene<br />
Isophorone<br />
2-Nitrophenol<br />
2,4-Dimethylphenol<br />
bis(-2-Ch1oroethoxy)Methane<br />
2,4-Dichlorophenol<br />
1,2,4-Trichlorobenzene<br />
Naphthalene<br />
Hexachlorobutadiene<br />
4-Chloro-3-Methylphenol<br />
Hexachlorocyclopentadiene<br />
2,4,6-Trichlorophenol<br />
2-Chloronaphthalene<br />
Dimethyl Phthalate<br />
Acenaphthylene<br />
2,6-Dinitrotoluene<br />
Acenaph<strong>the</strong>ne<br />
2,4-Dinitrophenol<br />
4-Nitrophenol<br />
2,4-Dinitrotoluene<br />
Diethylphthalate<br />
4-Chlorophenyl-phenyle<strong>the</strong>r<br />
Fluorene<br />
Benzidine<br />
4,6-Dinitro-2-Methylphenol<br />
N-Nitrosodiphenylamine<br />
4-Bromophenyl-phenyle<strong>the</strong>r<br />
Hexachlorobenzene<br />
Pentachlorophenol<br />
Phenanthrene<br />
Anthracene<br />
Di-N-Butylphthalate<br />
Fluoran<strong>the</strong>ne<br />
GC/MS<br />
SEMI-VOLATILE ANALYSIS<br />
Data File:>R9152<br />
719152<br />
DET. LIMIT<br />
----------
BAY AREA DRUM<br />
719152 #87-035-3020<br />
PAGE 2<br />
Pyrene<br />
Butylbenzylphthalate<br />
3,3'-Dichlorobenzidine<br />
Benzo(a)Anthracene<br />
bis-(2-Ethylhexy1)Phthalate<br />
Chrysene<br />
Di-N-Octyl Phthalate<br />
bis-(2-Ethylhexy1)Phthalate<br />
Chrysene<br />
Di-N-Octyl Phthalate<br />
Benzo(b)Fluoran<strong>the</strong>ne<br />
Benzo(k)Fluoran<strong>the</strong>ne<br />
Benzo(a)Pyrene<br />
Indeno(l,2,3-cd)Pyrene<br />
Dibenzo(a,h)Anthracene<br />
Benzo(g,h,i)Perylene<br />
Checked By
Client ID: BAY AREA DRUM<br />
Sample ID: 87-035-3020<br />
Matrix : SOIL SAMPLE: PER. SAND<br />
COMPOUND NAME<br />
.......................<br />
DICHLORODIFLUOROMETHANE<br />
CHLOROMETHANE<br />
u<br />
- BROMOMETHANE<br />
VINYL CHLORIDE<br />
CHLOROETHANE<br />
METHYLENE CHLORIDE<br />
TRICHLOROFLUOROMETHANE<br />
TOTAL 1,2-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHANE<br />
1,1,1-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICHLOROMETHANE<br />
1,2-DICHLOROPROPANE<br />
TRANS-1,3-DICHLOROPROPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
DIBROMOCHLOROMETHANE<br />
1,1,2-TRICHLOROETHANE<br />
CIS-1,3-DICHLOROPROPANE<br />
2-CHLOROETHYL VINYL ETHER<br />
BROMOFORM<br />
1,1,2,2-TETRACHLOROETHANE<br />
- TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,3-DICHLOROBENZENE<br />
1,2-DICHLOROBENZENE<br />
1,4-DICHLOROBENZENE<br />
TOTAL XYLENE<br />
2-PROPANONE (ACETONE)<br />
GC/MS<br />
VOLATILE ANALYSIS<br />
AMOUNT<br />
-----------<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
Data File:>9153V<br />
719153<br />
DET. LIMIT<br />
----------<br />
125 ug/kg<br />
250 ug/kg<br />
250 ug/kg<br />
250 ug/kg<br />
250 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
250 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 .ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
125 ug/kg<br />
Checked By
Element<br />
Aluminum<br />
Antimony<br />
Arsenic<br />
Barium<br />
Beryllium<br />
Cadmi um<br />
Calcium<br />
Chromium (Total)<br />
Cobalt<br />
Copper<br />
Iron<br />
Lead<br />
Magnesium<br />
Manganese<br />
Mercury<br />
Molybdenum<br />
Nickel<br />
Potassium<br />
Selenium<br />
Si lver<br />
Sodi um<br />
Stronti um<br />
Thall ium<br />
Vanadium<br />
Zinc<br />
Reference Methods<br />
Metals<br />
Soi 1<br />
Atomic Absorption Metals Analysis<br />
Graphite Hydride<br />
F 1 ame Furnace Generation<br />
- I<br />
- EPA 7040 AA 7041<br />
ZA P A 7060 - EPA 7061<br />
- EPA 7080 - EPA 7081<br />
- EPA 7090 -EPA 7091<br />
- EPA 7130 - EPA 7131<br />
- EPA 7190 - EPA 7191<br />
-<br />
EPA 7210 EPA 7211<br />
A<br />
- EPA 7380 EPA 7381 -<br />
- EPA 7420 EPA 7421 -<br />
- EPA 7460 EPA 7461 -<br />
- EPA 7520 EPA 7521 -<br />
- .&PA 7740<br />
-<br />
- EPA 7760 EPA 7761<br />
- EPA 7770<br />
-<br />
- EPA 7840 YEPA 7841<br />
EPA 7910 - EPA 7911<br />
-EPA 7950 EPA 7951<br />
- -<br />
- EPA 7741<br />
ANALYST IL LS<br />
proJect # 87-035-3020<br />
Date Compf eted 1 1 -1j-19~<br />
Cold<br />
Vapor ICP<br />
-<br />
- EPA 6010<br />
- EPA 6010<br />
- EPA 6010<br />
- ,+PA 6010<br />
- EPA 6010<br />
- EPA 6010<br />
- YEPA 6010<br />
- EPA 6010<br />
- EPA 6010<br />
- 4 A 6010<br />
&PA 6010<br />
-
u<br />
Preparation:<br />
Reference Methods<br />
I"tetc1s<br />
Acid Digestion EPA 3010<br />
- EPA 3020<br />
- EPA 3030<br />
- EPA 3040<br />
/ EPA 3050<br />
-<br />
Mercury Digestion - EPA 7470 Water<br />
-<br />
EPA 7471 Soi 1<br />
Alkaline Digestion - EPA 3060<br />
EP Toxicity EPk 1310<br />
CAM STLC -<br />
OTHER<br />
Title 22 CAC
Preparation<br />
Water - EPA 3510<br />
- EPA 3520<br />
Soi 1 - EPA 3540<br />
Reference Methods<br />
Semi-volatile Organics<br />
(BNA's)<br />
Analysis<br />
- EPA 625<br />
Project # 87-035-3020<br />
Date Completed 11-13-1 987<br />
ANALYST DL-/
Water<br />
Soi 1<br />
Reference Methods<br />
Volatile Organic Analysis<br />
Preparation Analysis<br />
ANALYST ".c-v<br />
1) Eisenberg, Don M.. et al, "Guidelines for<br />
Addressing Fuel Leaks", California Regional<br />
Water Quality Control Board. San Francisco<br />
Bay Region, Sept. 1985.<br />
- EPA 601<br />
- EVA 602<br />
- EPA 624<br />
- EPA 8010<br />
- EPA 8015<br />
- EPA 8020<br />
EPA 8240<br />
i<br />
- Guidelines for<br />
Addressing<br />
Fuel Leaks 1
Client ID: BAY AREA DRUM Data ~ile:>9822V<br />
Sample ID: 87-035-03-3086 719822<br />
Matrix : SOIL SAMPLE: VCS2<br />
COMPOUND NAME<br />
P==P======PP======I=E==<br />
DICHLORODIFLUOROMETHANE<br />
CHLOROMETHANE<br />
BROMOMETHANE<br />
VINYL CHLORIDE<br />
CHLOROETHANE<br />
METHYLENE CHLORIDE<br />
TRICHLOROFLUOROMETHANE<br />
1, 1-DICHLOROETHENE<br />
1,l-DICHMROETHANE<br />
TOTAL 1,2-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHANE<br />
lIltl-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICIILOROMETHANE<br />
1,2-DICHLOROPROPANE<br />
TRANS-1,3-DICHLOROPROPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
CIS- 1,3-DICHLOROPROPANE<br />
2-CHLOROETHYL VINYL ETHER<br />
BROMOFORM<br />
1,1,2,2-TETRACHLOROETHANE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,4-DICHMROEENZENE<br />
TOTAL XYLENE<br />
2-PROPANONE (ACETONE)<br />
GC/MS<br />
VOLATILE ANALYSIS<br />
AMOUNT<br />
========PI=<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
730.<br />
ND<br />
ND<br />
150.<br />
ND<br />
ND<br />
ND<br />
ND<br />
1300.<br />
160.<br />
ND<br />
ND<br />
ND<br />
DET. LIMIT<br />
==E..i======<br />
25 ug/kg<br />
50 ug/kg<br />
50 ug/kg<br />
50 ug/kg<br />
50 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
50 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
Checked By
u<br />
-<br />
Client ID: BAY AREA DRUM Data File: >9822V<br />
Sample ID: 87-035-03-3086 719822<br />
Matrix : SOIL SAMPLE: VCS2<br />
COMPOUND NAME<br />
I I ~ I I I P I I I I I I P e P = m E p I L I<br />
DICHLORODIFLUOROMETHANE<br />
CHLOROMETHANE<br />
BROMOMETHANE<br />
VINYL CHLORIDE<br />
CHLOROETHANE<br />
METHYLENE CHLORIDE<br />
TRICHLOROFLUOROMETHANE<br />
Ill-DICHLOROETHENE<br />
lll-DICHMROETHANE<br />
TOTAL 112-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHANE<br />
1,1,1-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICHLOROMETHANE<br />
112-DICHLOROPROPANE<br />
TRANS-113-DICHLOROPROPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
DIBROMOCHLOROMETHANE<br />
1,1,2-TRICHLOROETHANE<br />
CIS-1,3-DICHLOROPROPANE<br />
2-CHLOROETHYL VINYL ETHER<br />
- BROMOFORM<br />
~I~,~,~-TETRACHLOROETHANE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,3-DICHLOROBENZENE<br />
1,2-DICHLOROBENZENE<br />
- - - - - - - -<br />
1 ; 4-DICHLOROBENZENE<br />
TOTAL XYLENE<br />
2-PROPANONE (ACETONE)<br />
GC/MS<br />
VOLATILE ANALYSIS<br />
AMOUNT<br />
P==EPII=ILI<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
730.<br />
ND<br />
ND<br />
150.<br />
ND<br />
ND<br />
ND<br />
ND<br />
1300.<br />
160.<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
26.<br />
490.<br />
ND<br />
370.<br />
ND<br />
DET. LIMIT<br />
IIPPIIPIII<br />
25 ug/kg<br />
50 ug/kg<br />
50 ug/kg<br />
50 ug/kg<br />
50 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
50 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
25 ug/kg<br />
Checked By
November 19, 1987<br />
Mr. Rich Greenwood<br />
Canonie Environmental<br />
1825 S. Grant Street, Suite 260<br />
San Mateo, CA 94402<br />
Dear Mr. Greenwood:<br />
Enclosed are <strong>the</strong> laboratory results for <strong>the</strong> samples submitted to <strong>the</strong><br />
Canonie Environmental Analytical Laboratory.<br />
Canonie Environmental Services Cop. -<br />
212 Frank Wen Circle<br />
Suite A<br />
Stockion. California 95206<br />
Phone: 209-983-1340<br />
Unless o<strong>the</strong>rwise instructed by you samples will be returned or disposed of<br />
two weeks from <strong>the</strong> date of this letter.<br />
If you have any questions please call Jon Bartell or me at (209) 983-1340.<br />
Very truly yours.<br />
~anhydr of- Laboratory Services<br />
Enclosure<br />
I
Laboratory Report for<br />
Mr. Rich Greenwood<br />
Canonie Environmental<br />
1825 S. Grant Street. Suite 260<br />
San Mateo, CA 94402<br />
November 19, 1987<br />
Canonie Environmental<br />
212 Frank West Circle, Suite A<br />
Stockton, CA 95206<br />
(209) 983-1 340
Client ID: BAY AREA DRUM<br />
Sample ID: 87-035-03-3086<br />
Matrix : SOIL SAMPLE: VCS2<br />
COMPOUND NAME<br />
.......................<br />
DICHLORODIFLUOROMETHANE<br />
L CHLOROMETHANE<br />
-<br />
BROMOMETHANE<br />
VINYL CHLORIDE<br />
CHLOROETHANE<br />
METHYLENE CHLORIDE<br />
TRICHLOROFLUOROMETHANE<br />
1,l-DICHLOROETHENE<br />
1,l-DICHLOROETHANE<br />
TOTAL 1,2-DICHLOROETHENE<br />
CHLOROFORM<br />
1,2-DICHLOROETHANE<br />
1,1,1-TRICHLOROETHANE<br />
CARBON TETRACHLORIDE<br />
BROMODICHLOROMETHANE<br />
1,2-DICHLOROPROPANE<br />
TRANS-1,3-DICHLOROPROPENE<br />
TRICHLOROETHENE<br />
BENZENE<br />
DIBROMOCHLOROMETHANE<br />
1,1,2-TRICHLOROETHANE<br />
CIS-1.3-DICHLOROPROPANE<br />
2-CHLOROETHYL VINYL ETHER<br />
BROMOFORM<br />
- 1,1,2,2-TETRACHLOROETHANE<br />
TETRACHLOROETHENE<br />
TOLUENE<br />
CHLOROBENZENE<br />
ETHYL BENZENE<br />
1,3-DICHLOROBENZENE<br />
1,2-DICHLOROBENZENE<br />
1,4-DICHLOROBENZENE<br />
TOTAL XYLENE<br />
2-PROPANONE (ACETONE)<br />
GC/MS<br />
VOLATILE ANALYSIS<br />
AMOUNT<br />
-----------<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
ND<br />
730.<br />
ND<br />
ND<br />
150.<br />
ND<br />
ND<br />
ND<br />
Data File:>9822V<br />
719822<br />
Checked By
L. Water<br />
-<br />
-<br />
So1 1<br />
Reference Methods<br />
Volatile Organic Analysis<br />
1) Eisenberg. Don M.. et al, "Guidel~nes for<br />
Preparation Analysis<br />
Addressing Fuel Leaks", California Regional<br />
Water Qua1 i ty Control Board. San Francisco<br />
Bay Reg~on. Sept. 1985.<br />
- EPA 601<br />
-. EVA 602<br />
- EPA 624<br />
- EPA 5030 - EPA 8010<br />
- EPA 8015<br />
EPA 8020<br />
.* EPA 8240<br />
Project # 87-035-03-3086<br />
Date Completed 11-19-1987<br />
- Guidelines for<br />
Addressing<br />
Fuel Leaks 1
-<br />
:tiv~ty.,. ... . b Enf 0 SUIV SiIeMit o ~ermltting _a A I Tech ~<br />
O!hrr<br />
10. SAMPLING LOCATION<br />
11. SAMPLES<br />
- -<br />
12. ANALYSIS REQUESTED I. PC8<br />
Container I<br />
k. q Ext. Orp<br />
(Scroeng)<br />
e. 0 pH g. c VOA I. ~Cnlorinrtrd<br />
Pect~c~drr<br />
JM~tal<br />
Scan h. 0 PAH<br />
m. ~Organo-P<br />
PestIclde8<br />
d. a W.E.T.<br />
4<br />
I. 0 Phenols n, Cl<br />
I. ucarba-<br />
- ~ L ~ O S 0.0<br />
13. CHAIN OF CUSTODY I<br />
4. SPECIAL REMARKS j<br />
7 ANALYSIS REQUESTED<br />
.<br />
-<br />
L I<br />
A I<br />
B I<br />
, ,
ww QCliEPT<br />
. .- 02-19-** . - - -<br />
FRI 05:33:36 G 3 ** ****<br />
. .<br />
NO. 85
L<br />
-<br />
LABORATORY REPORT FOR TOTAL METAL ANALYSIS<br />
COLLECTOR'S NAHE: C DAVENPORT COLLECTOR'S SAMPLE NO. : RY-1R<br />
WlPLE LOCATION : BRY AREA DRUM H Y BITER ACTIVITY :<br />
8FO DATE RECEIVED :<br />
ANALYTICAL SAMPLES ARE DIOESTED WITH CONCENfRdTED NITRIC ACID OVER A HOT<br />
PROCEDURE : PCdTE. THE DIGEBTED BAHPLEB ARE FILTERED AND MADE TO 100 ML<br />
WITH 5% NITRIC ACID IN DISTILLED DEIONIZED WATER. RETAL ANALYSIS<br />
OF THE DIOEBT IS BY ICPREB. RESULTS ARE REPORTED R8 UOIGRRH,<br />
HUL NUUBER : Dl047 Dl048<br />
COLLECT SAHP #: RW-LA RY-10<br />
SAMPLE TYPE : LIQUID LIPUlD<br />
AG-S ILVE R<br />
WRSENIC<br />
BA-BARIUFI<br />
BE-BERYLLIUH<br />
CD-CADMIUH<br />
CO-COBALT<br />
CR-CHROUIUFl<br />
CU-COPPER<br />
flO-MOLYBDENUH<br />
N1-NICKEL<br />
Pa-LEAD<br />
SO-ANTfUONY<br />
BE-SELENIUM<br />
V -VANADIUM<br />
ZN-ZINC<br />
TL-THflLLIUH<br />
-<br />
NOTE: < BELOW DETECTION LIMIT OF INBTRUMENT (***).NOT DETERMINED BY ICP<br />
- :<br />
.. 02-19-** FRI 05:31:14 G3<br />
: hx .<br />
3%:<br />
Y* **** N0.03
STAT5 OF CAiiiD2i::i-iiEiilK ASC VIE::AEE AGENCY GEORGE DE~l~EjiiN, Gor?.nar<br />
--<br />
DEPARTMENT OF HEALTH SERVICES<br />
2151 GEiKE:F\ r' : i<br />
JAN74 198F /--a?!<br />
'CKELEY. CA PI704<br />
Tommy Lee<br />
SF Dept. of Public Works<br />
750 Phelps Street<br />
SF, CA 94124<br />
Dear Tommy,<br />
January 13, 1987<br />
As per our phone conversation yesterday, I am forwarding to you<br />
our laboratory analysis of <strong>the</strong> rainwater that has pnded inside<br />
<strong>the</strong> Bay Area Drum building. The cyanide analysis is enclosed, and<br />
<strong>the</strong> metals analyses have already been sent to you. The cyanide<br />
analysis was delayed dua to internal prioritization at <strong>the</strong><br />
laboratory.<br />
As we agreed, I have informed Kurt Ahlich of Canonie<br />
Environmental that he can take <strong>the</strong> necessary steps to transfer<br />
this water to <strong>the</strong> sewer. He will contact you to arrange a<br />
convenient time for both you and him to initiate <strong>the</strong> discharge.<br />
-<br />
Thanks again for your cooperation in assisting DHS in <strong>the</strong>ir<br />
cleanup efforts at <strong>the</strong> Site. If you have any questions, please<br />
contact me at (415) 540-3401.<br />
4<br />
cc: u ~ Ahlich, t Canonie<br />
Herome ~arcotte, DHS<br />
Cordially<br />
~lif#on W. ~avendort<br />
Associate Engineering Geologist<br />
Site Mitigation Unit
. site BOLL A\- -? c fipk? 1'.2<br />
. . c'<br />
- c. .As'dress 13 \I<br />
a. EPk ID W3.<br />
6. INDEX<br />
>\c&z . S.F (.&<br />
ii.73~: Sirecl Cily Zip . .<br />
-<br />
i... 3 Ex:. 0:g<br />
72. A~\'.~LYs:s EC:.ISTED 1. n PCB (sc;;t"g)
Cate Received<br />
lector's ::me c/;/'hm II&UP~,D"~P by Laboratory /2//// 87<br />
San?plin,- Location R&, q.-c, A!. fd =?;re<br />
J Collector's Sarcple !,Qwl(d to<br />
Reference: MNL Hg - /A oob<br />
ANALYSIS RiSULTS: . . . .<br />
. .. . . .<br />
. .. . . . .<br />
Analyst ' s Sienatures: ..<br />
7 . /I cL 22<br />
I , ..Ll!zU' date<br />
2.<br />
M CRLY.)<br />
'date<br />
California Department of Health Services - Hazardous Materials Laborntory<br />
-<br />
.
APPENDIX D<br />
Environmental
James M. Cramer<br />
VICE PRESIDENT<br />
/<br />
IILEX USA INC.<br />
:alltornla Branch PO 80x 24397 Venlura CA 93002<br />
ax 1805) 642.0777<br />
NlLEX<br />
February 13, 1958<br />
Canonie Environmental<br />
1E25 S. Grant Ave. Suite 2LO<br />
San Mateo, CA.<br />
944ii2<br />
Attention: Mike Klein<br />
RE: BAY AREA DRUM, 60 MIL HDPE CAPlGEDTETFILE<br />
NlLEX USA INC;<br />
Csllfornla Branch<br />
PO Box 24397<br />
Ventura. CA 93002<br />
Phone (805) 654-0610<br />
Fax (8051 642-0777<br />
As per your request we are providing you with <strong>the</strong> required<br />
submittals far <strong>the</strong> above project.<br />
It is our recommendation that <strong>the</strong> gectextiie not be<br />
connected to <strong>the</strong> structure as it will interfere with <strong>the</strong><br />
sealing of <strong>the</strong> membrane at <strong>the</strong> concrete interface. ; n e<br />
geotextile shall be terminated within six inches 16'! frcm<br />
<strong>the</strong> edge of <strong>the</strong> liner.<br />
All seams fc~r <strong>the</strong> geotextile shall be overlapped 2' ta<br />
ensure proper continuity a+ <strong>the</strong> fabric.<br />
4 miii certificate or certifiration that ths geotextile<br />
meets ail of <strong>the</strong> enclosed specifications shall be forwarded<br />
tn <strong>the</strong> owner as soon as possible.<br />
Tie fabric shall be shi~ped in black poiyethylene wrapping<br />
te ensure protection frnm U.V. The material shall be<br />
unloaded and handled with rare to ensure <strong>the</strong> original state<br />
of <strong>the</strong> fabric.<br />
I trust <strong>the</strong> above submittal will meet with your approval<br />
should you have any comments or questions please cali me at<br />
your convenience.<br />
Sincerely,<br />
NILEX USA INC.<br />
James M Cramer<br />
Vice President<br />
I" canada: NILEX GEOTECHNICAL PRODUCTS INC. ~dmonton, AB ana ~urnaby. BC<br />
-.
Canonie Environmental<br />
1825 S. Grant fivr. Suite P60<br />
San Wateo, CQ.<br />
94 40;'<br />
RE: HUNTERS POINT 60 MIL HDPE CAP--SUBMITT0LS<br />
NlLEX USA INC.<br />
calnmla Bmnch<br />
PO Box 24397<br />
Ventura. CA 93002<br />
Phone (805) 654-0610<br />
Fax (805) 642-0777<br />
As per your recluest we are providing you with <strong>the</strong> required<br />
submittals for thp above project.<br />
1.5 HDPE Lininq<br />
1.5.1 Item C.<br />
Schleqel Lining Technology ~ 1.11 warrant <strong>the</strong> material for a<br />
period of two (2) year5 from date of installation. Nilex<br />
US0 Inr. will warrant <strong>the</strong> installation of <strong>the</strong> material for a<br />
period of two (2) years from <strong>the</strong> date of installation.<br />
1.6. Item 0.<br />
The HDPE sheet shall be laid out as per <strong>the</strong> Nilex field<br />
representative's direction. Prior to any fipld welding<br />
commencing a test weld of 3 feet shall be performed to<br />
ensure <strong>the</strong> welder- is set to <strong>the</strong> present ambient outdoor<br />
c~nditions. These welds will be tested for tensile and peel<br />
values by <strong>the</strong> Nilex technician. Pending <strong>the</strong> Nil€*x<br />
technicians approval <strong>the</strong> welding will start. Sheet that can<br />
not be seamed will not be la~d out that day. Rs <strong>the</strong> sheet<br />
is laid out at <strong>the</strong> penetrations for <strong>the</strong> fer~ce a<br />
prefabricated boot shall be installed over <strong>the</strong> fence post<br />
and welded to <strong>the</strong> parent sheet material. A compression<br />
fitted band will be installed as per enclosed detail. Upon<br />
completion of <strong>the</strong> installation of <strong>the</strong> membrane <strong>the</strong> Nilex<br />
technician shall visually inspect <strong>the</strong> entire site and all<br />
seams for any holes or defects. Upon <strong>the</strong> approval of <strong>the</strong><br />
Nilex technician backfilling of <strong>the</strong> membrane w ~ll commence.<br />
Nilex certifies that all field seams performed in <strong>the</strong> above<br />
contract will meet <strong>the</strong> enclosed General Specifications For<br />
HDPE Lining. Any samples requiring verification by an<br />
independent laboratory will be at <strong>the</strong> owners expense.<br />
In CM.d.: HIW QEOTECHNICALPROWCTS INC. E m ,<br />
*B am BuW, sC
1.5.1 Item R<br />
It is o:Jr 1-rv:oamendat~on that <strong>the</strong> r:t.otext;le not be<br />
corinected to <strong>the</strong> structirre as it will ~nterfere WI th t.hc!<br />
seal lnq OF tl;e menhi-ane at <strong>the</strong> co~lcretr. interf-?ace. The<br />
qrwt~xtile shall be tcrmlnated within six inches (6") fr-on:<br />
<strong>the</strong> ~dqe of <strong>the</strong> 1 ~ ner<br />
.<br />
All se.tms for <strong>the</strong> geolextile %hall be overlapped 2' to<br />
ensure proprr cant~nu: ty of <strong>the</strong> fabi-IC.<br />
R m i l l certificate or certlflcatlon that <strong>the</strong> geotextlle<br />
meets all of <strong>the</strong> enclosed specif~cations shall be forwarded<br />
to <strong>the</strong> owner as soon as possibl~.<br />
Ihe fabr~c shall he shlpped in ti lack polyethylene wrappinq<br />
to ensure protection from L1.V. The material shall be<br />
unloaded and handled with care to ensure <strong>the</strong> criginal state<br />
of <strong>the</strong> fabric.<br />
I trust <strong>the</strong> above submittal will meet with your approval<br />
should you have any comments or questions please call me at<br />
your convenlencc.<br />
Sincerely,<br />
James M Cramer<br />
Vice President
a NlLEX<br />
USA INC.<br />
P 0 BOX 24397<br />
VENTURA. CA 93002<br />
PHONE (805) 654-0610<br />
N'iEX FAX. ,805) 642.0777
~ - ,-<br />
. . . ... I . ~Z3ELsALLREnSJ~E?4EXTS<br />
A. Ssgae<br />
GENERAL S1ECIIICYUONS FOR HDPE LINING<br />
The work covers <strong>the</strong> manufacture and installation of a<br />
high den'sity polyet-hylene (SCELEGEL~ sheet) liner for<br />
<strong>the</strong> lining of ear<strong>the</strong>n basins for <strong>the</strong> protection of<br />
groundwater.<br />
i<br />
The work includes furnishing all equipment and<br />
materials, providing all labor, supervision,<br />
administration and managenest; and supplying ail<br />
construction equipment, materials and services<br />
necessary to perfora <strong>the</strong> work as detailed in this<br />
specification.<br />
The lining contractor's asproved drawings for<br />
construction will specify all components and details<br />
require? to meat specifications. The responsibility<br />
of <strong>the</strong> owner or <strong>the</strong> lining contractor will be clearly<br />
indicated.
-<br />
9 d ~<br />
.~~<br />
~~ ~.<br />
.The manufacturer/installer must have at least five ( 5)<br />
years continuous ex2erience in <strong>the</strong> manufactnre and<br />
installation of SCSLEGZL~ sheet, and must have<br />
- . . . . . . -. -. manufactured and installed at least 20,000,000 square<br />
feet of <strong>the</strong> material specified for this project.<br />
The manufacturer/installer shall submit a list of ten<br />
(10) similar installations which have besn in service<br />
at least two (2) yebrs. .The list shall include <strong>the</strong><br />
owner's name, location of project, square feet of<br />
product installed, ahd <strong>the</strong> completion date.<br />
.Submittals not including this.required information<br />
will not be acce?ted.<br />
Submit for approval samples of SCELEGZL~ sheet<br />
for customer reviev 2nd testing. Testing shall<br />
include compatibility analysis by material<br />
supplier or owner.<br />
Submit for approval as soon as practical after<br />
award of <strong>the</strong> contract, six (6) sets of full and
complete shop and installation drawings showinq a<br />
minimum of:<br />
a. Layout of <strong>the</strong> liner systen.<br />
.b. .Details of jointing, liner system, liner<br />
anchorages to concrete structures, details<br />
of sealing <strong>the</strong> SCHLZGZLO sheet to concrete<br />
structures, and any o<strong>the</strong>r openings into <strong>the</strong><br />
structure.<br />
Certificates of compliance with <strong>the</strong> requirezests<br />
of standards and testing methods specified herein<br />
shall be submitred prior to delivery. .The liner<br />
material manufacturer must satisfy by affidavit<br />
to <strong>the</strong> owner and contractor, jointly, that <strong>the</strong><br />
material he offers to furnish and install will<br />
meet in every aspect <strong>the</strong> requirenents set forth<br />
in <strong>the</strong> specifications. .The contractoc shall<br />
transmit to <strong>the</strong> owner <strong>the</strong> affidavit given him by<br />
<strong>the</strong> manufacturer or supplier prior to apgroval<br />
for <strong>the</strong> furnishing and installing of any such<br />
material.
The contractor shall submit a schedule detailing<br />
<strong>the</strong> liner fabrication and installation,<br />
1. .&1i-vo=,v<br />
.Materials shall be delivered to <strong>the</strong> site after<br />
<strong>the</strong> required submittals have been ap~roved.<br />
Storage and handling of <strong>the</strong> materials shall<br />
conform to <strong>the</strong> manufacturerls recarmendations and<br />
shall be done in such a manner as to prevent<br />
dainage to any part of <strong>the</strong> work.<br />
Reference Standards shall comply with <strong>the</strong> apglicable<br />
. . . - . . .<br />
- - - - ---provisions and recommendations of <strong>the</strong> American Society<br />
for Testing Materials (AST:4), exce~t as o<strong>the</strong>rvise<br />
shown or specified.
F. Job Conddfl~ns<br />
Prior to installation of <strong>the</strong> liner, contractor shall<br />
verify conditions of existing facilities and<br />
structures to ensure an adequate subgrade for <strong>the</strong><br />
liner, as specified in Section 1II.B of this docmeat.<br />
Destructive and non-destructive testing are carried<br />
.out by trained personnel of <strong>the</strong> lining contractor.<br />
.Quality cantrol procedures are specified in Section IV<br />
of this document.<br />
Terns and conditions of <strong>the</strong> wtrranty to be agreed uFcn<br />
between <strong>the</strong> owner and <strong>the</strong> lining cont:ackor.<br />
The lining shall be a high density polyethylene<br />
(SCSLEGZL9 sheet] containing no additives, fillers or<br />
extenders. Carbon black 23 2 .51 shall be added to
___--_ ..-._L__..._.-.._.-~I_.- -- -- -- ---tke<br />
resin for ultraviolet resisk~nce. The lining sy~==~ sh211<br />
be manuftctured, furnished and installed by a single<br />
contractor. Typical physical progerties of <strong>the</strong> DPE: liner<br />
(SC~LEGZL~ sheet) are described in Table 1.<br />
Resin use? for extrusion joining shests and shest to<br />
pipe shall be WPS produced from <strong>the</strong> same resin es <strong>the</strong><br />
sheet. .Physical properties shall be <strong>the</strong> same as tkose<br />
of <strong>the</strong> resin &ed in <strong>the</strong> manufacture of <strong>the</strong> HDPE<br />
liner. The resin shall be sucolied in black.<br />
Sponge rubber sheeting shall be type SCS-41,<br />
Neoprene/EPT/SaR, Closed Cell Medium, 114 inch thick,<br />
one side adhesive.<br />
PYTHON, neoprene adhesive shall be use? for gluing<br />
sponge rubber shesting to concrete and EDPE surfac=s.<br />
Batten strips shall be No. 12 gauge steel type A-36.<br />
Width of strips shall be two inches (2") minimum.
- 7<br />
.. ~<br />
- -<br />
- -<br />
Product and manufacturez: provide alloy steel<br />
fasteners as manufactured by <strong>the</strong> following:<br />
1. -2 -Molly .Parabolts by US?{ Corporation<br />
2. Kwik-Bolt Eilti Corporation<br />
3 .Ramset, Inc.<br />
.4. Or Ap~roved Equal<br />
.Wet or dry elastic roof sealer as manufactured by<br />
Bonsey Products, Inc.<br />
The lining contractor shall be res~onsible for<br />
inspection of <strong>the</strong> sheet rolls at <strong>the</strong> job site. Should<br />
rolls show damage from transit, <strong>the</strong>y will be so<br />
identified by <strong>the</strong> lining contractor and set aside.<br />
During unrolling of <strong>the</strong> lining material, <strong>the</strong> lining<br />
contractor will carry out visual inspection of tbe
sheet surface. Any faulty areas shall be marked and rezaire; - ir.<br />
an approved mznner by <strong>the</strong> lining contractor.<br />
. B . B1f:2-S~bazzd5-E~_e2az3f i-01)<br />
The Purchaser shall be responsible for presaring <strong>the</strong><br />
earthwork as required. .No broken stones or hard<br />
objects shall be present on <strong>the</strong> surface to be lined.<br />
Stones larger than t-do inches (2") in diameter, shaq<br />
.edged stones of any size, and hard objects shall not<br />
be persitted within four inches (4") of <strong>the</strong> surface to<br />
be line?. The surface shall be compacted to a density<br />
to allow tbe movenest of vehicles and weldina<br />
equipment on it without causing rutting or o<strong>the</strong>r<br />
deleterious effects. .Typically, this is a density of<br />
.85-90 Standard Proctor.<br />
The surface of all concrete bonding surfaces shall be<br />
cleaned and smoo<strong>the</strong>d prior to anchoring <strong>the</strong> liner.<br />
The SCSLEG2L9 sheet shall be laid out and<br />
installed by manufact=reras trained technicians<br />
in ac=ordance with <strong>the</strong> applicable approved shop<br />
drawings.
-<br />
6 ~ ~ .<br />
- ' - - . - . The sheets shall be placed in <strong>the</strong> basin to persit<br />
termination at <strong>the</strong> top of <strong>the</strong> side slopes and<br />
adjacent to concrete structures and pipe conduits<br />
as shown on <strong>the</strong> drawings. The layout shall be<br />
'<br />
- - - -- - - .<br />
. - . . . . .<br />
. . . - - -<br />
.<br />
designed to minimize <strong>the</strong> number and length of <strong>the</strong><br />
field joints, consistent with proper methods of<br />
liner installation.<br />
.Field joints shall be made by overlapping<br />
adjacent sheets a minimum of eight inches<br />
- (8") and extruding a ribbon of extrusion<br />
joining resin no less than 1.5 inches (1.5")<br />
in width between <strong>the</strong> overlapped sheets or<br />
over <strong>the</strong> seam beheen <strong>the</strong> sheets where hand<br />
welds are required,<br />
Prior to extrusion welding of <strong>the</strong> seams, all<br />
.areas whicb are to become seam intezfaces<br />
shall be cleaned of dust and dirt. The<br />
slick surfaces of <strong>the</strong> HDPE sheet which are<br />
to become Sean interfaces shall be rougherbed<br />
with a wire brush or o<strong>the</strong>r acceptable means<br />
before extrudate is placed between <strong>the</strong><br />
overlapping sheets or over a lapped sean.
Exkrusion joining shall not take place<br />
unless <strong>the</strong> sheet is dry and shall not take<br />
place unless <strong>the</strong> ambient tenperature is<br />
above 20 " F and below 90" F.<br />
Joints betveen <strong>the</strong> lining sheets shall be<br />
field welded using <strong>the</strong> manufacturer's<br />
extrusion joining equipment and techniques.<br />
The joining procedure shall consist of<br />
softening <strong>the</strong> liner material by heated air.<br />
.The teqerature of <strong>the</strong> air impinging on <strong>the</strong><br />
sheet for this purpose shall range from<br />
420 .F to 680' .F. The exact tenperature<br />
used shall be determined by <strong>the</strong> installation<br />
supervisor. Directly following <strong>the</strong><br />
application of heat, a one inch (1") minims<br />
width strip of <strong>the</strong> same high density<br />
polyethylene resin from which <strong>the</strong> sheet is<br />
made shall be extruded betxeen <strong>the</strong><br />
overlapped sheets. The temperature of <strong>the</strong><br />
resin as it emerges from <strong>the</strong> extrusion die<br />
shall range from 428" F to 536' F. The<br />
overlapped sheets are <strong>the</strong>n pressed toge<strong>the</strong>r<br />
to form <strong>the</strong> extrusion joint.
Penetrations through <strong>the</strong> liner for pige<br />
flashings, patches, etc., shall be field<br />
welded using an extrusion hand welder. The<br />
joining procedure shall consist of softening<br />
...- - - - . <strong>the</strong> liner material by heated air as<br />
*<br />
described above. Directly following <strong>the</strong><br />
agplication of heat, a hot strip of <strong>the</strong> saze<br />
material from which <strong>the</strong> sheet is made will<br />
be extruded over <strong>the</strong> joint to produce <strong>the</strong><br />
extruded joint.<br />
Any required repair of mall holes in <strong>the</strong><br />
liner surface shall be made with <strong>the</strong><br />
extrusion hand welder. Liner material shall<br />
be cleaned of all dirt, dust, and o<strong>the</strong>z<br />
. foreign material, all smooth SCBLEGZLO sheet<br />
surfaces roughened, air heated to <strong>the</strong><br />
prescribed temperature, and a strip of BDPE<br />
resin extruded over <strong>the</strong> hole to produce an<br />
extrusion weld repair.<br />
- - . . . - - . - - . . - - . - . Seals around penetrations shall be made as<br />
described below.
All pipe pesetrations shall be sleeve? with<br />
DPE pipe. Each EDPE pipe sleeve shall be<br />
sealed to <strong>the</strong> liquid carrying pipe to<br />
prevent leakage. The basin liner shall be<br />
. . .- -.-anchored to a concrete collar surrounding<br />
<strong>the</strong> pefietration. A SCSLEGEL~ sheet apron<br />
shall be extrusion welded to <strong>the</strong> pipe sleeve<br />
and shall be extrusion welded to <strong>the</strong> base<br />
sheet outside of <strong>the</strong> area where <strong>the</strong> base<br />
sheet is anchored to <strong>the</strong> concrete collar.<br />
The manufacturer of <strong>the</strong> HDPE resin used in sheet<br />
production tests eacfi batch before delivery to ensure<br />
a maximum consistency of raw material quality.<br />
The following tests shall be carried out by <strong>the</strong><br />
.. . - pcoducer of <strong>the</strong> raw material on each batch and <strong>the</strong><br />
results forwarded to <strong>the</strong> sheet fabricator:<br />
The density of <strong>the</strong> material reflects <strong>the</strong> degree<br />
of czystallinity, and thus serves as an indirect
check on mechanical qualities such as hardness,<br />
stiffness and tensile strength.<br />
- .Carbon black polyethylene serves primarily as<br />
protection against <strong>the</strong>rnal aging and harmful<br />
ultraviolet radiation present in outdoor<br />
wea<strong>the</strong>zing. Thus, quality control of <strong>the</strong> carbon<br />
black content ensures t5e good wes<strong>the</strong>ring<br />
properties of polyethylene.<br />
A material's melt index is a measure of its mezn<br />
molecglar weight and rheological properties.<br />
Thus, holding <strong>the</strong> melt index of <strong>the</strong> base material<br />
within a narrow ranse is a criterion for uniforz<br />
and optimum HDPZ liner production.<br />
Bell testing is a relatively fast method of<br />
testing a material's performance under mechanical<br />
stressing in aggressive media.
Maintaining a constant moisture content in <strong>the</strong><br />
base material is necessary for processing,<br />
resulting in a pore-free, bubble-free product.<br />
.Employing only material with a moisture content<br />
in a narrow tolerance range is ano<strong>the</strong>r<br />
requirenent for consistent product quality.<br />
The data determined is evaluated by <strong>the</strong> manufacturer<br />
and, if deviating from <strong>the</strong> agreed tolerance ranges,<br />
<strong>the</strong> tested batch is not delivered. As a 'result of<br />
this testing, <strong>the</strong> manufacturer is guaranteed<br />
consistent base material quality, essential in <strong>the</strong><br />
light of <strong>the</strong> denanding conditions prevailing in <strong>the</strong><br />
various apolications of WPE liners.<br />
The incoming raw material shall be sampled and tested<br />
in <strong>the</strong> lab facilities of <strong>the</strong> sheet manufacture;.<br />
Properties relative to processing shall be deternined,<br />
specifically:<br />
- Melt Index per ASTX Designation D-1238-73<br />
- Density per ASTM Designation D-792<br />
- Moisture Content per AST:I Designation D-570-63
This testing provides fur<strong>the</strong>r verification of<br />
consistent product quality, supplementary to <strong>the</strong><br />
manufacturer's certificate.<br />
If <strong>the</strong> test results are positive, a sample of <strong>the</strong><br />
. -. - --.-.---batch is processed in manufacturing and evaluated as<br />
- - to melting behavior, forming behavior, and <strong>the</strong> product<br />
sheet's visual appearance.<br />
No batch is sent into production before positive<br />
results are obtained for <strong>the</strong> incoming base material<br />
and <strong>the</strong> tesk processing. If negative results are<br />
obtained, <strong>the</strong> batch is excluded from processing and<br />
return& to <strong>the</strong> manufacturer.<br />
All properties determined in <strong>the</strong>se tests shall be<br />
compiled in <strong>the</strong> final shest certificate.<br />
Automatic control must be included in <strong>the</strong> extrusion<br />
process and <strong>the</strong> successive processing stages.<br />
Important parameters in all stages of processing shall<br />
be controlled by automatic control systems.<br />
Three different qualities of <strong>the</strong> sheet shall be<br />
inspected continuously during production:
.- -<br />
- Forming Process<br />
- Surface Apcearanco<br />
- Sheet Thickness<br />
-- - Processing parameters such as tezperature, pressure<br />
-- - and speed shall be continuously monitored for each<br />
liner produced. A measuring device, such as a strip<br />
chart recorder, shall be furnished, if requested.<br />
.Sheet thickness shall fall within <strong>the</strong> following<br />
parameters: Ninety percent (90%) of <strong>the</strong> gross sheet<br />
area shall be ,+ ten percent (2103) of nominal<br />
specified thickness. .Ten percent (103) of <strong>the</strong> gross<br />
sheet area shall be ,+ fifteen percent (215%) of<br />
nominal specified thickness.<br />
At least three random samples shall be taken from each<br />
sheet roll and forwarded to <strong>the</strong> laboratory for<br />
.- . .extensive testing. The sample sites shall be e~enly<br />
distributed to ensure a regresentative evaluation of<br />
<strong>the</strong> overall . quality.<br />
The following tests shall be carried out for each<br />
sheet:
-<br />
-<br />
. . - . - - . . - . .. "<br />
- Tensile Testing per ASTX Designation D-638<br />
-- Impact Tensile Testing per ASTX Designation D-1822<br />
- Thickness<br />
- Stress Cracking Resistance (Bell Test) per<br />
ASTX<br />
Designation D-1693-70.<br />
The following supglenentary tests shall be carried out<br />
for sheet samples from each raw material batch:<br />
- Melt Index per ASTX Designation D-1238-72<br />
- Thermal Shrinkage per ASTM Designation D-1204<br />
- Density per ASm Designation 0-792<br />
Records of this testing shall be a permanent<br />
surveillance of <strong>the</strong> production process and constant<br />
product quality, and shall be maintained by <strong>the</strong><br />
manufacturer.<br />
... . . -- Narrow tolerance ranges ensure high quality in<br />
production. Products deviating from <strong>the</strong>se ranges<br />
shall be renoved and <strong>the</strong> cause determined.<br />
Sheet installation work shall be carried out under<br />
painstaking supervision up to, and including, project<br />
completion.
The quality control shall be carried out by <strong>the</strong><br />
on-site personnel as well as outside testing<br />
institutions.<br />
Quality control of installation shall be divided into<br />
three areas:<br />
Checking <strong>the</strong> sheets delivered to <strong>the</strong> site for<br />
transport damages; checking of sheet<br />
identification number with number on certificzte.<br />
Inspection and continuous control of all welding<br />
process parameters.<br />
Testing of <strong>the</strong> completed weld seams.<br />
.on-site welding of <strong>the</strong> SCHLEGEL' sheet shall be<br />
carried out by an e:rtrusion welding process. This<br />
.-....p rocess shall guarantee consistent weld seam quality<br />
within a wide range of ambient conditions. The<br />
.control systea of <strong>the</strong> welding machines shall be<br />
- .- e:ctensively automated .to enable monitoring of <strong>the</strong><br />
welding process by <strong>the</strong> operating personnel.<br />
The welds shall be performed in one procedure by means<br />
of an automatic welding machine, which preheats <strong>the</strong><br />
welding surfaces to <strong>the</strong> desired temperature, injects a<br />
ribbon of molten HDPE material and <strong>the</strong>n applies<br />
contact pressure to <strong>the</strong> Sean.<br />
1
The procedure for fillet welds shall be similar in<br />
.that <strong>the</strong> welding area shall be preheated and <strong>the</strong><br />
welded material shall be molten WPE. The necessary<br />
contact pressure shall come from <strong>the</strong> weight of <strong>the</strong><br />
hand welding unit itself. Fillet welds shall be used<br />
only for resair .work and special designs.<br />
.Test welds shall be run preceding all extensive<br />
welding to assure good weld quality under <strong>the</strong><br />
prevailing site conditions; <strong>the</strong>se weld samples shall<br />
be subsequently subjected to mechanical testing.<br />
The main prereqiisite for good bonding shall be<br />
continuous monitoring of <strong>the</strong> welding process<br />
parameters, such as hot air tenperature, welding<br />
speed and contact pressure. This is best carried<br />
out by specially trained personnel. Visual<br />
inspection of <strong>the</strong> welding surfaces, <strong>the</strong> welding<br />
process and <strong>the</strong> completed weld by experienced<br />
- -. . . plastic welc?ezs, allows a reliable evaluation of<br />
seam quality.
Production of a quality welding sezm starts with<br />
G - - -.- - a preliminary test weld. The machine settings,<br />
-<br />
---. - pretreatment of <strong>the</strong> weld surfaces and adjustaent<br />
to environmental effects shall be tested on a<br />
sample welding sesm. A hand operable tensile<br />
testing macbine shall be on site for confirmation<br />
of <strong>the</strong> joint's tensile strength using strip<br />
samples.<br />
.After installation, two major types of quality<br />
,control shall be available for testing <strong>the</strong> seas:<br />
- Destructive material tests of weld samples<br />
(spot cbeck)<br />
- Non-Destructive material tests of all welding<br />
seams.<br />
Txo samples shall be taken daily for<br />
Destructive tests on all weld seams;