use of metal templates for microcavity formation in alumina
use of metal templates for microcavity formation in alumina
use of metal templates for microcavity formation in alumina
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Densification Rate (1/ o C)<br />
0,009<br />
0,007<br />
0,005<br />
0,003<br />
0,001<br />
800 900 1000 1100 1200 1300 1400 1500 1600<br />
-0,001<br />
-0,003<br />
Figure 4.7. Densification rate curve <strong>for</strong> powder compact (UP 150MPa) <strong>of</strong> alum<strong>in</strong>a<br />
CR6 dur<strong>in</strong>g s<strong>in</strong>ter<strong>in</strong>g at a heat<strong>in</strong>g rate <strong>of</strong> 5 o C/m<strong>in</strong> at 1500 o C.<br />
4.2. BET Analyses <strong>of</strong> the Powders<br />
Temperature ( o C)<br />
The surface area <strong>of</strong> alum<strong>in</strong>a powders were measured by BET analysis. Table 4.1<br />
shows the report <strong>of</strong> the surface area <strong>of</strong> alum<strong>in</strong>a CR6, CR15 and CR30F. Accord<strong>in</strong>g to<br />
this report, it is clear that the particles <strong>of</strong> alum<strong>in</strong>a CR6 have less surface area, pore<br />
volume and pore size than the others, and it is understood that it is not easy <strong>for</strong> CR6 to<br />
create a reaction to the diffusion with the <strong>metal</strong> <strong>templates</strong>. All measurements done <strong>in</strong><br />
this study were lower than those published by the producers.<br />
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