use of metal templates for microcavity formation in alumina
use of metal templates for microcavity formation in alumina
use of metal templates for microcavity formation in alumina
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(a) (b)<br />
A B A<br />
B<br />
(c) (d)<br />
A<br />
(e)<br />
Figure 4.15. SEM micrographs <strong>of</strong> alum<strong>in</strong>a that <strong>use</strong>d Ti wire (a) alum<strong>in</strong>a CR6<br />
(b) alum<strong>in</strong>a CR15 (c) alum<strong>in</strong>a CR30F (d) alum<strong>in</strong>a AKP50 (e) alum<strong>in</strong>a<br />
CT3000SG.<br />
Accord<strong>in</strong>g to Figure 4.15, some <strong>of</strong> the samples had cracks and porosity <strong>in</strong><br />
alum<strong>in</strong>a. This is most likely beca<strong>use</strong> the s<strong>in</strong>ter<strong>in</strong>g temperature <strong>use</strong>d here is <strong>in</strong>sufficient<br />
to <strong>for</strong>m a dense ceramic from unmilled and undoped powder (Goodshaw et al., 2009).<br />
Secondly, the Ti wire seems to be still present <strong>in</strong> the alum<strong>in</strong>a. There<strong>for</strong>e, the diffusion<br />
region <strong>in</strong> Figure 4.15 shows consequential contrast, and EDS analysis <strong>of</strong> zones with<strong>in</strong><br />
the diffusion region display that either Al or Ti is present.<br />
B<br />
A B<br />
A B<br />
40