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Diploma Thesis - Erich Schmid Institute

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8. Deposition of Thin Films<br />

Deposition of Thin Films<br />

8.1. Magnetron sputtering of polycrystalline Al thin films on Si(1 0 0)<br />

Magnetron sputtering of polycrystalline thin films is a widely used deposition<br />

technique. Thin layers of chromium, gold, titanium, aluminium and many other<br />

materials can be produced using the technique in a deposition chamber<br />

schematically depicted in Fig. 8.1. In the evacuated chamber, ionized gas atoms<br />

(usually argon ions) are accelerated under influence of an electrical field towards a<br />

target. The high kinetic energy enables the ions to strike out surface bound atoms<br />

which are leaving, with rather low kinetic energy (some keV), the target’s surface in<br />

all possible directions. A substrate, fixed usually on the opposited side of the<br />

chamber, is covered by a thin film of the sputtered atoms. The advantages of the<br />

magnetron sputtering process are a good control of process parameters, high purity<br />

of the films and a possibility to use low process temperatures.<br />

For the production of polycrystalline Al thin films on monocrystalline Si(1 0 0) wafers,<br />

magnetron sputtering device installed at the “<strong>Institute</strong> of Physics, Technical University<br />

Wien” was used. As a substrate for the specimen preparation, a 1 mm thick Si(1 0 0)<br />

wafer cleaned using isopropanol and acetone was used. On this native-oxidized<br />

silicon wafer, a polycrystalline aluminium thin film with a thickness of 2 µm was<br />

deposited using magnetron sputtering. The deposition was performed at 150 °C<br />

applying a pressure of 4 x 10 -3 mbar.<br />

+<br />

Figure 8.1: A schematic view of a sputtering reactor<br />

1 Vacuum chamber, 2 upper electrode, 3 plasma,<br />

4 lower electrode, 5 gas inlet, 6 vacuum pump connection<br />

7 substrate, 8 high frequency voltage, 9 target<br />

10 plasma ion, 11 target atom<br />

33

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