Annual Report 2009/2010 - JUWEL - Forschungszentrum Jülich

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Magnusson, D.; Chritiansen, B.; Foreman, M.R.S.; Geist, A.; Glatz, J.-P.; Malmbeck, R.; Modolo, G.; Serrano-Purroy, D.; Sorel, C.: Demonstration of a SANEX Process in Centrifugal Contactors using the CyMe4-BTBP Molecule on a Genuine Fuel Solution, Solvent Extraction and Ion Exchange, 27 (2009) 2, 97 – 106 Mincher, B.J.; Modolo, G.; Mezyk, St.P.: The Effects of Radiation Chemistry on Solvent Extraction 3: A Review of Actinide and Lanthanide Extraction, Solvent Extraction and Ion Exchange, 27 (2009) 5/6, 579 – 606 Mincher, B.J.; Modolo, G.; Mezyk, St.P.: Review Article: The Effects of Radiation Chemistry on Solvent Extraction: 1. Conditions in Acidic Solution and a Review of TBP Radiolysis, Solvent Extraction and Ion Exchange, 27 (2009) 1, 1 – 25 Mincher, B.J.; Modolo, G.; Mezyk, St.P.: Review Article: The Effects of Radiation Chemistry on Solvent Extraction: 2. A Review of Fission-Product Extraction, Solvent Extraction and Ion Exchange, 27 (2009) 3, 331 – 353 Rezniczek, A.; Richter, B.: Assessment of the Performance of Containment and Surveillance Equipment, Part I: Methodology, ESARDA-Bulletin, 41 (2009) June, 46 – 50 Rezniczek, A.; Richter, B.; Jussofie, A.: Assessment of the Performance of Containment and Surveillance Equipment, Part II: Trial Application, ESARDA-Bulletin, 41 (2009) June, 51 – 61 Richter, B.: The ESARDA Working Group on Containment and Surveillance, Activities in 2008 - Chairman’s Report, ESARDA Bulletin, 41 (2009), 41-44 11.2.2 Proceedings/Books Proceedings Benay, G.; Modolo, G.; Robisson, A.C.; Grandjean, S.: Microspheres prepared by Internal Gelation for Actinide Co-Conversion - Influence of Organic Precursors in Initial Solution on Structure during Thermal Treatment, International Conference ATALANTE 2008 Nuclear Fuel Cycles for a Sustainable Future May 19-23 2008 Montpellier, France Carrot, M.; Fox, D.; Maher, C.; Modolo, G.; McLachlan, F.; Sarsfield, M.; Taylor, R.; Woodhead,D.: Extraction and stripping of actinides in TBP and TODGA/TBP systems for advanced fuels processing, Proceedings of Global 2009, Paper 9033, Paris, France. - 6.- 11.09.2009 Janssens, W.A.M.; Autrusson, B.; Boella, M.; Bril, L.-V.; Goncalves, J.G.M.; Janssens- Maenhout, G.G.A.; Martikka, E.; Mayer, K.; Peerani, P.; Rezniczek, A.; Richard, M.; Richter, B.; Sevini, F.; Stanley, W.T.; Stein, G.; Weh, R.: A Selection of Recent Achievements and Future Challenges in Safeguards R&D as Identified by the European Safeguards Research and Development Association, Proceedings of the INMM 50th Annual Meeting, Tuscon, 12.-16 Juli 2009, erschienen auf CD-ROM Modolo, G.; Kluxen, P.; Geist, A.: Selective separation of americium(III) from curium(III), californium(III), and lanthanides(III) by the LUCA process, Proceedings of Global 2009, Paper 9193, Paris, France, 6-11.10.2009 225
Rezniczek, A.; Richter, B.; Jussofie, A.: Assessment of the Performance of Containment and Surveillance Equipment - Trial Application, Proceedings of the 31st ESARDA Annual Meeting, Vilnius, 26.-28.Mai 2009. - Erschienen auf CD-ROM Stein, M.; Lange, S.; Möslinger, M.; Neumann, G.; Queirolo, A.; Richter, B.: Papier des ESARDA-Board and der WG-Chairs, Proceedings of the INMM 50th Annual Meeting, Tuscon, 12.-16. Juli 2009. - Erschienen auf CD-ROM Stein, M.; Lange, S.; Möslinger, M.; Neumann, G.; Queirolo, A.; Richter, B.: The IAEA's Next Generation Surveillance System, System Testing - Phase IV Report, Prod. INMM 50th Annual Meeting, Tucson, 12.-16. Juli 2009. - Erschienen auf CD-ROM Stein, M.; Richter, B.; Möslinger, M.; Queirolo, A.; Heppleston, M.; Neumann, G.; Lange, S.: The Next Generation Surveillance System - Development Project Overview, Proceedings of the 31st ESARDA Annual Meeting, Vilnius, 26.-28. Mai 2009. - Erschienen auf CD-ROM Books Jasani, B.; Niemeyer, I.; Nussbaum, S.; Richter, B.; Stein, G. (Hrsg.): International Safeguards and Satellite Imagery, Key Features of the Nuclear Fuel Cycle and Computer- Based Analysis, Springer, 2009, 9783540791317 11.2.3 Internal reports Kreutz, F.: Bericht über die Prüfung der Daten und Unterlagen zu den COGEMA HAW- Glaskokillen der Beladung für den Transport VGO92, PKS-WAA-VG091 / 2009, Version: 1.0 vom 30.01.2009 Prüfberichte AREVA, Version: 1.0 vom 30.01.2009 Prüfberichte AREVA, Jülich, FZJ, Institut für Energieforschung-6, 2009 Kreutz, F.: Bericht über die Prüfung der Daten und Unterlagen zu den COGEMA HAW- Glaskokillen der Beladung für den Transport VGO92, PKS-WAA-VG092 / 2009, Version: 1.0 vom 05.11.2009 Prüfberichte AREVA, Version: 1.0 vom 05.11.2009, Jülich, FZJ, Institut für Energieforschung-6, 2009 Kreutz, F.: Bericht über die Prüfung der Daten und Unterlagen zu den COGEMA HAW- Glaskokillen der Beladung für den Transport VGO93, PKS-WAA-VG093 / 2009, Version: 1.0 vom 21.04.2009 Prüfberichte AREVA, Version: 1.0 vom 21.04.2009, Jülich, FZJ, Institut für Energieforschung-6, 2009 Kreutz, F.: Bericht über die Prüfung der Daten und Unterlagen zu den COGEMA HAW- Glaskokillen der Beladung für den Transport VGO94, PKS-WAA-VG094 / 2009, Version: 1.0 vom 05.11.2009 Prüfberichte AREVA, Version: 1.0 vom 05.11.2009, Jülich, FZJ, Institut für Energieforschung-6, 2009 Kreutz, F.: Bericht über die Prüfung der Daten und Unterlagen zu den COGEMA HAW- Glaskokillen der Beladung für den Transport VGO95, PKS-WAA-VG095 / 2009, Version: 1.0 vom 15.10.2009 Prüfberichte AREVA, Version: 1.0 vom 15.10.2009, Jülich, FZJ, Institut für Energieforschung-6, 2009 Kreutz, F.: Bericht über die Prüfung der Daten und Unterlagen zu den COGEMA HAW- Glaskokillen der Beladung für den Transport VGO96, PKS-WAA-VG096 / 2009, Version: 1.0 vom 31.08.2009 Prüfberichte AREVA, Version: 1.0 vom 31.08.2009, Jülich, FZJ, Institut für Energieforschung-6, 2009 226
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Mitglied Mitglied der der Helmholtz
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Forschungszentrum Jülich GmbH Inst
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TABLE OF CONTENTS 1 Preface .......
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6.2.2 Doctoral Thesis .............
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state of NRW. The collaborative pro
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2 Institute’s Profile Due to the
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2.2. Organization chart Reactor Saf
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3 Key Research Topics 3.1. Long Ter
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actinide co-conversion into polyact
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Fig. 7: Non-destructive analytical
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Fig. 9: Thermal treatment of an AVR
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3.8. Product Quality Control of Rad
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3.8.2 Product Quality Control of Lo
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The advantage of working at low vac
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NdPO 4 powder sample, directly rece
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4.5. Non-destructive assay testing
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5 Scientific and Technical Reports
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Results and Discussion The irradiat
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work will focus on the identificati
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Different solvents (iso-propanol an
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e & j) Aggregates of aluminium oxid
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Experimental details The corrosion
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Intensity [CPS] 500 400 300 200 100
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Fig. 24: Left: High resolution TEM
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a) MD model [10] b) Derived Lesukit
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5.4. Minor actinide(III) recovery f
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Extensive extraction studies were p
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of the extraction properties of the
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Cm(III) together with the lanthanid
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using a mixture of CyMe4BTBP and TO
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A more challenging route studied wi
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These preliminary results show that
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The 1-cycle SANEX process is intend
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Continuous counter-current tests us
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Conclusion In this work, it was sho
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shaken by a vortex mixer for 15 min
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100 100 Distribution ratio 10 1 0.1
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Tab. 15: The distribution ratios of
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5.7. Synthesis and thermal treatmen
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Acid-Deficient Uranyl-Nitrate via d
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Optical investigation showed a noti
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TG /% 100 98 96 94 92 90 88 86 84 8
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Radiolysis in the aqueous solutions
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is about 4% while the one of the rh
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Fig. 59: Compressibility curve for
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Conclusion and outlook Monazite-typ
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Fig. 63: Description of the unit ce
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agents for the synthesis of neodymi
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100 TG 785°C Exo DSC 0,2 0,0 90 -0
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After synthesis the product was cen
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process of monazite and additional
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Tab. 18: Lattice parameters determi
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Conclusions For Sm 1-x Ce x PO 4 mo
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5.11. Raman Spectra of Synthetic Ra
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The numerical values of all measure
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knowledge, these special relationsh
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Fig. 80: Raman spectra of LaPO 4 ir
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5.12. MC simulation of thermal neut
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content was replaced by hydrogen. C
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constant for hydrogen concentration
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with a 0 1 -183.88 ± 8.55 and a 2
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5.13. An Improved Method for the no
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2 2 2 d0 R ds d0 dw la( )
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The relative uncertainty for the ac
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In the drum, 4 ‘hot spots’ for
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activity of Cs-137 is much more und
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gamma-ray detector approximated by
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shown in Fig. 96. In both cases the
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econstruction than the old calculat
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Neutron capture cross sections and
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Outlook The evaluated data will be
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from carbon-based HTR fuel elements
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Fig. 102: 3D volume reconstructions
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dislocate the 14 C atom from its pr
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It can be seen that nearly all trit
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Acknowledgement The authors like to
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development by investigations of ga
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Fig. 109: The left picture shows th
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[2] A European Roadmap for Developi
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from airborne SWIR Full Spectrum Im
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Fig. 113: Visualization of the vege
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number of training samples up to 19
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Acknowledgements The work presented
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three approaches has severe drawbac
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neighbours from the list of merge c
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it gives a difference in segmentati
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[6] I. Niemeyer, F. Bachmann, A. Jo
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Monitoring 3 cooperated intensively
Page 179 and 180: facilities and other treaty related
Page 181 and 182: parameters of the SAR system, such
Page 183 and 184: The MGD products used in the study
Page 185 and 186: Fig. 134 contains the result for th
Page 187 and 188: [2] H. Maître (ed.), Processing of
Page 189 and 190: Preparatory Committee to allocate t
Page 191 and 192: unconditional security assurances f
Page 193 and 194: safeguards was also requested. Deci
Page 195 and 196: [16] United Nations Security Counci
Page 197 and 198: 5.24. Development and Application o
Page 199 and 200: Hardware layer The hardware layer i
Page 201 and 202: So in most applications the scale u
Page 203 and 204: The ENDF-B/V and ENDF-B/VI librarie
Page 205 and 206: 5.26. Product control of waste prod
Page 207 and 208: Polysiloxane which has been investi
Page 209 and 210: acceptance requirements [3]. In the
Page 211 and 212: Fig. 145: List of description and d
Page 213 and 214: 6.1. Courses taught at universities
Page 215 and 216: Umwelt / Energy & Environment 2010;
Page 217 and 218: 6.5. Institute Seminar The IEK-6 or
Page 219 and 220: 6.5.3 Invited talks 2009 30.04.2009
Page 221 and 222: 21.09.2010 Dr. N. Evans: The Chemis
Page 223 and 224: 8 Selected R&D projects 8.1. EU pro
Page 225 and 226: K. Aymanns: Nominated as deputy re
Page 227 and 228: Bukaemskiy A.A., Barrier D., Modolo
Page 229: 11.2. Publications 2009 11.2.1 Jour
Page 233 and 234: Daniels, H.: Co-conversion of actin
Page 235 and 236: 11.3. Publications 2010 11.3.1 Jour
Page 237 and 238: Sypula, M.; Wilden, A.; Schreinemac
Page 239 and 240: (Partitioning) - Stabilitätsunters
Page 241 and 242: Modolo, G.; Bosbach, D.; Geist, A.;
Page 243 and 244: 12 How to reach us Postal Address F
Page 245 and 246: By train: Take the train from Aache
Page 247 and 248: Schriften des Forschungszentrums J
Page 259: Schriften des Forschungszentrums J
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Annual Report 2009/2010 - JUWEL - Forschungszentrum Jülich

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