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Quattro 2 User's Guide, issue 2. 6666533 - Waters

Quattro 2 User's Guide, issue 2. 6666533 - Waters

Quattro 2 User's Guide, issue 2. 6666533 - Waters

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<strong>Quattro</strong> II<br />

<strong>User's</strong> <strong>Guide</strong><br />

Fault Finding<br />

Introduction 205<br />

The API Source 205<br />

No Beam 205<br />

Unsteady Beam 205<br />

Low Intensity Solvent Ions 206<br />

High Back Pressure 206<br />

Low Pressure 207<br />

The EI/CI Ion Source 207<br />

No Source Current 208<br />

High Source Current 208<br />

Incorrect Emission (Trap) Current 209<br />

Dynamic-FAB 210<br />

The Gas Chromatograph 211<br />

Low Sensitivity 211<br />

Poor Resolution and Peak Shape 211<br />

Vacuum System 212<br />

Poor Vacuum 212<br />

Vacuum Leaks 213<br />

Electronics 214<br />

Ripple 214<br />

Loss of Sensitivity 215<br />

High Noise Levels 216<br />

Fault Finding Check List 217<br />

General Loss of Performance 217<br />

No Beam 217<br />

Unsteady or Low Intensity Beam 218<br />

Reference Information<br />

Positive Ion API 221<br />

Horse Heart Myoglobin 222<br />

Polyethylene Glycol 222<br />

Sodium Iodide and Caesium Iodide Mixture 223<br />

Negative Ion API 224<br />

Horse Heart Myoglobin 224<br />

Mixture of Sugars 224<br />

EI/CI 225<br />

Air 225<br />

Heptacosa (perfluorotributylamine) (FC43) 226<br />

Ultramark 227<br />

Fast Atom Bombardment 228<br />

Caesium Iodide and Rubidium Iodide Mixture 228<br />

Table of Contents

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