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ekS - Instytut Agrofizyki im. Bohdana Dobrzańskiego PAN w Lublinie ...

ekS - Instytut Agrofizyki im. Bohdana Dobrzańskiego PAN w Lublinie ...

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l<strong>im</strong>ited. This l<strong>im</strong>itation comes from the fact that in case of materials of high<br />

dielectric permittivity and at high frequencies, the changes of the dielectric<br />

permittivity of the material causes very small changes of the phase shift of the<br />

reflection coefficient. This drastically decreases the accuracy of measurement and<br />

the need to apply calibration media of small value of dielectric permittivity.<br />

9.3. Materials and methods<br />

Dielectric permittivity of three soils was compared. Table 16 presents the<br />

basic physical parameters of the tested soils.<br />

Table 16. Localization and selected physical parameters of tested soil samples<br />

No.<br />

611 Olempin<br />

606<br />

Localization<br />

Wólka<br />

Kątna<br />

Soil type<br />

Gleba<br />

brunatna<br />

Gleba<br />

murszowa<br />

Density<br />

[gcm -3 ]<br />

Soil texture ISSS<br />

sand silt clay<br />

2-0,02 mm<br />

0,02-0,002 < 0,002<br />

mm mm<br />

Specific<br />

surface<br />

[cm 2·g -1 ]<br />

1.59 94 5 1 9<br />

1.42 97 2 1 23<br />

619 Sahryń Czarnoziem 1.16 87 12 1 69<br />

Dry soils were mixed with appropriate amount of distilled water to achieve<br />

four samples for each analysed soil with different water content values and taking<br />

care to get the homogeneous distribution of water in the soil samples. Twelve<br />

containers with soil samples covered with plastic foil (to min<strong>im</strong>ize evaporation)<br />

were left for 24 hours in room temperature for water distribution in the samples in<br />

natural way. The grav<strong>im</strong>etric water content, θ, and bulk density, ρ, were<br />

determined according to ISO standard 16586 [44] for each soil sample directly<br />

after the dielectric permittivity measurements were completed. The values of ρ in<br />

Table 1 are the mean for all applied water contents for each tested soil. Soil<br />

texture was determined by standard Bouyoucos method (Turski [93]). The values<br />

of soil specific surface, S, was determined with water vapour adsorption method<br />

(Ościk [73]).<br />

T<strong>im</strong>e Domain Reflectometry (TDR) and Open-Ended Coax Probe methods of<br />

determination of the complex dielectric permittivity of porous materials were<br />

applied.<br />

TDR measurements were performed using the oscilloscope frame HP54120<br />

with the TDR unit HP54121T, featured by 20 ps rise-t<strong>im</strong>e step pulse. The TDR<br />

probe was based on the standard coaxial connector (type N jack) with three<br />

90

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