Differential Scanning Calorimetry (DSC)
Differential Scanning Calorimetry (DSC)
Differential Scanning Calorimetry (DSC)
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<strong>DSC</strong>: Available Method Segments<br />
JUMP ABORT NEXT SEG*<br />
EQUILIBRATE SAMPLING INTERVAL<br />
INITIAL TEMPERATURE SELECT GAS<br />
RAMP EXTERNAL EVENT<br />
ISOTHERMAL DATA STORAGE<br />
ISO-TRACK AIR COOL*<br />
STEP LNCA CONTROL*<br />
INCREMENT MARK END OF CYCLE*<br />
REPEAT SEGMENT x FOR y TIMES MODULATE#<br />
REPEAT SEGMENT x TILL y °C<br />
* Available on <strong>DSC</strong> 29XX only<br />
# Available on M<strong>DSC</strong> 29XX only<br />
<strong>DSC</strong>: Method Design Rules<br />
�Start Temperature<br />
�Generally, the baseline should have three (3)<br />
minutes to completely stabilize prior to the<br />
transition of interest. Therefore, at 10°C/min.,<br />
start at least 30°C below the transition onset<br />
temperature<br />
�End Temperature<br />
�Allow a three (3) minute baseline after the<br />
transition of interest in order to correctly select<br />
integration or analysis limits
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