Differential Scanning Calorimetry (DSC)
Differential Scanning Calorimetry (DSC)
Differential Scanning Calorimetry (DSC)
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<strong>DSC</strong>: Heating/Cooling Method<br />
Heating Method<br />
(NOTE: No equilibrate segment necessary if<br />
starting at or near ambient temperature.)<br />
1) Ramp 10°C/min. to 300°C<br />
Cooling Method<br />
1) Equilibrate at 300°C<br />
2) Ramp 10°C/min. to 25°C<br />
<strong>DSC</strong>: Heat-Cool-Reheat Method<br />
Heat-Cool-Reheat Method<br />
1) LNCA control: High<br />
2) Ramp 10°C/min. to 300°C<br />
3) Mark cycle end 0<br />
4) Ramp 10°C/min. to 25°C<br />
5) Mark cycle end 0<br />
6) Ramp 10°C/min. to 300°C<br />
7) Mark cycle end 0<br />
The first segment in this method allows for rapid cooling
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