NA-LUBE - King Industries, Inc.

King Industries, Inc.Lubricant Additives DivisionSpecialty Additives and Synthetic Base Oilsfor Industrial & Automotive Lubricants, Greases,Metalworking Fluids and Rust PreventivesNA-LUBE ® KR SeriesAlkylated NaphthaleneSynthetic BasestocksNA-LUBE ® ADTCAshless DialkyldithiocarbamateNA-LUBE ® AO SeriesAntioxidantsNA-LUBE ® AW SeriesAntiwear AdditivesNA-LUBE ® EP SeriesExtreme Pressure AdditivesK-CORR ® G SeriesSpecialty Additives for GreaseNA-SUL ®Rust & Corrosion InhibitorsK-CORR ®Rust & Corrosion InhibitorsNA-LUBE ® BL SeriesAdditive Blends & PackagesPerformance Products Backed ByUnsurpassed Technical Service

King Industries, Inc.Lubricant Additives DivisionKing Industries offers a broad range of products for use in formulating high performanceindustrial and automotive lubricants, greases, metalworking fluids, and rust preventives.King’s product lines include:Synthetic Base Oils & Base Oil ModifiersNA-LUBE ® KR Series - Alkylated Naphthalene Base Oils and Base Oil Modifiers:The NA-LUBE KR Series represents the industry’s broadest range of alkylated naphthalenesynthetic basestocks. With decades of experience in alkylation, King offers a diverse range ofproducts with viscosities from 22 cSt to 190 cSt (40°C).Specialty AdditivesNA-LUBE ® EP 5000 Series - Extreme Pressure Additives:A series of light-colored, low odor sulfurized fatty acid esters/triglycerides, and sulfurized olefins/triglycerides for industrial and automotive lubricants, greases, and metalworking fluids. When usedin combination with ash-containing or ashless phosphorus-type antiwear and lubricity additives,these additives are outstanding alternatives to chlorinated paraffins in metalworking fluids.NA-LUBE ® AW 6000 Series - Antiwear Additives:These additives are based on amine salts of phosphoric acid and dithiophosphoric acid derivatives.Some of these additives are formulated with other components, offering synergistic antiwear,extreme pressure, and rust and corrosion protection.NA-LUBE ® ADTC - Ashless Dialkyldithiocarbamate:A multifunctional additive offering extreme pressure, antioxidant, and antiwear properties when usedin industrial and automotive lubricants and greases.NA-LUBE ® AO - Primary Antioxidants:Phenolic and aminic antioxidants that are effective stabilizers for a broad range of industrial andautomotive lubricants and greases. All products are ashless and non-corrosive, and offer excellentsolubility in petroleum and synthetic base oils.NA-SUL ® - Rust and Corrosion Inhibitors:A broad range of high performance rust and corrosion inhibitors based on dinonylnaphthalenesulfonic acid. They are supplied as metal or ashless salts in a variety of liquid and solid diluents.Applications include industrial and automotive lubricants, greases, metalworking fluids, and rustpreventives.K-CORR ® - Rust and Corrosion Inhibitors:Non-sulfonate rust and corrosion inhibitors that are effective in a broad range of industrial andautomotive lubricants, greases, and rust preventives. K-CORR inhibitors have demonstratedsynergistic performance with select antiwear/extreme pressure additives.K-CORR ® G Series - Rust Inhibitor Systems for Grease:The K-CORR G Series was specifically designed for greases subjected to severe conditions andoffers excellent rust protection and enhanced AW/EP properties.NA-LUBE ® BL - Blends - Multifunctional Additive Packages:Several specialized additive blends offering an alternative to individual component formulations.A complete overview of product offerings including new developmental products as well as technicaland application brochures can be found at King’s website:www.kingindustries.com

Table of ContentsIntroduction/King Industries Page 2NA-LUBE KR Series - Alkylated Naphthalenes Page 3NA-LUBE AW Series - Antiwear Additives Page 7NA-LUBE AO Series - Primary Antioxidants Page 12NA-LUBE ADTC - Ashless Dialkyldithiocarbamate Page 14NA-LUBE EP Series - Extreme Pressure Additives Page 15NA-SUL Rust & Corrosion Inhibitors Page 19King Product and Application ChartCenterfoldK-CORR Rust & Corrosion Inhibitors Page 32K-CORR G Series - Rust Inhibitor Systems for Grease Page 35HX-1 Registered Products Page 38NA-LUBE Blends Page 41Technical Support Page 49KING FACILITIESUSAWorld HeadquartersKing Industries, Inc.Science RoadNorwalk, CT 06852Phone: 203-866-5551Fax: 203-866-0425E-mail:lad@kingindustries.comEUROPETechnical Sales OfficeKing IndustriesInternational, Inc.Noordkade 642741 EZ WaddinxveenThe NetherlandsPhone: +31 182-631360Fax: +31 182-621002E-mail:dgartz@kingindustries.comASIA/PACIFICTechnical Service LabDr. Zhiqiang HeSynlico Tech(Zhongshan) Co., Ltd.106 Chuangye Building,Kang Le Ave.Torch DevelopmentZone,Zhongshan, ChinaPhone: +760-88229866Fax: +760-88229896E-mail:alex.he@kingindustries.comKing Industries“Our passion has always been to provide innovative additive technology andvalue-added customized solutions to our customers worldwide.”- Richard S. King, PresidentFor close to eight decades, King Industries has been owned and operated by the King family inNorwalk, Connecticut. In the 1940’s, R. Gardner King and associate George Thielcke pioneeredthe development of a unique chemical, dinonlynaphthalenesulfonic acid, the salts of whichexhibited excellent rust inhibiting properties. Since then, NA-SUL sulfonate technology has beenunsurpassed with respect to rust and corrosion inhibition and demulsification properties inhigh-tech lubricants and greases.In the mid-1990’s, King Industries expanded its product offerings with the development ofK-CORR non-sulfonate rust and corrosion inhibitor technology and an extensive NA-LUBEproduct portfolio consisting of extreme pressure, antiwear, and antioxidant additives, as well asalkylated naphthalene base oils and multifunctional/synergistic blends.By offering comprehensive solutions to lubricant problems and a growing portfolio of the mostadvanced additive technologies, King Industries strives to provide its worldwide customers withthe ability to formulate the most cost-effective premium products in the marketplace.King Industries, Inc is proud to be:ISO 9001, 14001 and 18001 Certified

NA-LUBE ® KR Series - Alkylated NaphthalenesSynthetic Base Oils and Base Oil ModifiersNA-LUBE ® KR-Series - Alkylated NaphthalenesFor over 50 years, King has been a leader in the alkylation of naphthalenes, and today King is theproducer of the world’s broadest line of alkylated naphthalene synthetic fluids. Designated theNA-LUBE KR Series, these products are the ideal choice for use as base stocks to meet theindustry’s highest performance standards where high temperatures degrade petroleum basedproducts or as modifiers for non-polar base stocks, such as Group II oils, Group III oils, and PAO’s.Whether working to develop an innovative new product or to improve an existing product, theNA-LUBE KR Series can help formulators meet today’s ever-increasing demands placed onlubricants. This includes three new NSF HX-1 registered products that meet the requirements forincidental food contact as prescribed by FDA 21 CFR 178.3570 - NA-LUBE KR-006FG, KR-015FGand KR-029FG.NA-LUBE KR alkylated naphthalenes provide superior thermo-oxidative stability, excellent hydrolyticstability, and greater film thickness compared to alternative base fluids (see comparison tablebelow). In addition, the non-polar nature of the NA-LUBE KR products makes them superior to othersynthetic fluids in that there is no surface competition with additives.PROPERTYNA-LUBEKR SeriesPAOEstersMineral Oils(Group II & III)Thermo-Oxidative Stability Excellent Good Good to Excellent GoodThermal Stability Excellent Excellent Excellent ExcellentHydrolytic Stability Excellent Excellent Good ExcellentSeal Swell Good to Excellent Poor Excellent PoorViscosity Index Good Excellent Excellent Good to ExcellentAdditive Solubility Good to Excellent Poor Excellent PoorFilm Thickness Excellent Good Good FairNA-LUBE ® KR Series Products - Typical PropertiesNA-LUBEViscosity@ 40°CASTM D 445Viscosity@ 100°CASTM D 445ViscosityIndexCalculatedAnilinePointASTM D 611NoackVolatilityCEC L40PourPointASTM D 97FlashPointASTM D 92KR-007A 21.8 cSt 3.8 cSt 22 40°C 39%

Applications and Product CustomizationAs can be seen from the Typical Properties Chart, King Industries offers a range of products withdiverse viscosity and polarity (aniline point) that leads to their use in a multitude of applications.Ranging from low viscosity for automotive lubricants to high viscosity for industrial lubricants andgreases - all NA-LUBE KR Series products offer exceptional performance in thermal and oxidativestability, hydrolytic stability, low volatility, good solvency and seal swell capability.MonoestersDiestersPolyol EstersNA-LUBEKR-007ARelative Aniline Points of Various Base OilsNA-LUBEKR-008NA-LUBEKR-015NA-LUBEKR-019PAOGroup II and IIIMineral Oils-7 to 5°C 40°C 42°C 94°C 103°C 115 to 135°CAUTOMOTIVE LUBRICANTSNA-LUBE KR-007A KR-008 KR-015 KR-019Transmission Fluids • •Crankcase OilsApplicationsAutomotive Lubricants•Gear Oils • • •INDUSTRIAL LUBRICANTSApplicationsIndustrial LubricantsGreasesNA-LUBE KR-007A KR-008 KR-015 KR-019 KR-023Chain Oils • • •Compressor Oils • •Gear Oils • •NA-LUBE ® KR-Series - Alkylated NaphthalenesGreases • • •Heat Transfer Oils • •H-1 Fluids KR-006FG, KR-015FG & KR-029FGHydraulic FluidsLow Temperature Applications••Paper Machine Oils • • •Pages 3-4Turbine OilsVacuum Oils••

NA-LUBE KR-Series Performance as a Base OilNA-LUBE ® KR-Series - Alkylated NaphthalenesThe performance characteristic that sets the NA-LUBE KR-Series apart from other base oils is theirsuperior thermal-oxidative stability. Thermal-oxidative stability results from both the CEC-L-48-A-95Modified Bulk Oxidation Test and ASTM D 6186 Pressure Differential Scanning Calorimetry (PDSC)are shown to illustrate this point. Thermal-Oxidative Stability - Modified CEC-L-48-A-95 Bulk Oxidation TestNA-LUBE KR-015 and a variety of other base fluids were subjected to heat and oxygen in thepresence of metal catalysts. Increases in acid number and viscosity were monitored over time. Anincrease in acid number is indicative of oxidation and degradation of the base oil. As shown in thegraph below on the left, NA-LUBE KR-015 was the most stable of the six base oils tested. Likewise,it maintained its original viscosity better than all the other fluids tested including a 7 cSt Group IIIbase oil containing an antioxidant (graph on the right).Acid # (mg KOH/g)706050403020100Increase in Acid ValueColor Key to Base Oils:NA-LUBE KR-0150 20 40 60 80Time (hour) Thermal-Oxidative Stability - PDSC - (ASTM D 6168)PDSC - Induction Time With O 2Modified Bulk Oxidation Test ConditionsBase Oil PAO Group I Group II Group III500 grams @ 160°C for 72 hours with solubleFe and Cu catalysts and air purge at 15L/hr10009008007006005004003002001000% Increase in Viscosity0 20 40 60 80Time (hour)NA-LUBE KR-015 and KR-019 (neat) when tested at 200°C and 210°C using 500 psig O 2 resulted inthe following performance compared to other base stocks:NA-LUBEKR-015NA-LUBEKR-019Minutes @ 200°C

NA-LUBE KR-Series Performance as a Base Oil ModifierWhen used as base oil modifiers, the NA-LUBE KR Series can:Offer dramatic improvements in thermal-oxidative stability when used alone or in conjunctionwith antioxidantsBoost RPVOT performance of formulations containing highly refined mineral oilsImprove thermal stabilityThe first graph below compares the thermal-oxidative stability performance of NA-LUBE KR-015and a variety of other synthetic base oil modifiers when used at a 20% level in a 7 cSt Group III oil.RPVOT Rotating Pressurized Vessel Oxidation Test (ASTM D 2272) data follow showing theinfluence of modification levels and the addition of some common antioxidants. Thermal-Oxidative Stability - PDSC - (ASTM D 6186)PDSC Oxidation Induction Times(Isothermal at 160°C with 150 psi air pressure)2520151050No Modifier KR-015 Diester Polyol Ester PAO Thermal-Oxidative Stability - RPVOT - (ASTM D 2272)Induction TimeBlends of 20% Synthetic Base Oils in 7 cSt Group III OilRPVOT of NA-LUBE KR-015in a 7 cSt Group III Oil90807060504030201000 25% 50% 75% 100%% NA-LUBE KR-015Induction Time600500400300200100The chart to the left shows oxidativeinduction times for blends containing20% of various synthetic base oils andNA-LUBE KR-015 in a 7 cSt Group IIIoil as measured by PDSC - PressureDifferential Scanning Calorimetry.As can be seen, NA-LUBE KR-015significantly outperforms the other fluidstested - PAO, diester and polyol esterbase oils.0Effect of 0.2% Antioxidant AdditionNoneDTBPNA-LUBEAO-210ZnDTPDPANA-LUBEAO-1427 cSt Group III NA-LUBE KR-015NA-LUBE ® KR-Series - Alkylated NaphthalenesAs shown above, NA-LUBE KR-015 was testedat various concentrations in a 7 cSt Group IIIbase oil to track its influence on RPVOTperformance.NA-LUBE KR-015 can impart dramaticimprovements in thermo-oxidative stability whenused as a base oil modifier. Testing was donewithout the addition of additives or stabilizers.Both NA-LUBE KR-015 and a 7 cSt Group III oilwere tested to determine the effect of adding0.2% of various antioxidants to the base oils.As shown in the graph above, significantimprovements to the thermal-oxidative stability(induction time) were obtained using theNA-LUBE KR-015.Pages 5-6

NA-LUBE ® AW 6000 Series - Ashless Antiwear AdditivesNA-LUBE ® AW 6000 SeriesAshless Multifunctional Antiwear AdditivesThe NA-LUBE AW 6000 Series consists of light-colored, 100% active antiwear additives basedon various phosphorous, nitrogen and sulfur chemistries. With the exception of AW-6010, all aremultifunctional in terms of providing excellent antiwear properties in combination with other propertyenhancing functions as shown in the chart that follows. Performance details are shown on pages9-11.Product % P % N % S Description FunctionsNA-LUBEAW-6010NA-LUBEAW-6110NA-LUBEAW-6110PNA-LUBEAW-6220NA-LUBEAW-6310NA-LUBEAW-6330NA-LUBEAW-6360NA-LUBEAW-6400FG5.3 4.8 -8.2 1.8 -5.3 3.7 -4.5 5.7 -4.2 3.0 9.14.5 - 10.05.0 2.6 10.88.3 2.4 -Amine phosphate with excellent antiwear properties atvery low treat levels.Amine phosphate with excellent antiwear properties andexcellent rust protection. Imparts outstanding FZGperformance (higher than 12 load stages) at low treatlevels (0.10 – 0.15%).Amine phosphate with excellent antiwear properties andexcellent rust protection. Can be used with NA-LUBEEP-5216 as an alternative to chlorinated paraffins.Complex composition of amine phosphate chemistrieswith excellent antiwear properties, excellent rustprotection and yellow metal deactivating functionality.Outstanding FZG performance at low treat levels.Multifunctional composition with excellent extremepressure/antiwear properties, excellent rust protection,yellow metal deactivating functionality and demulsificationproperties. Imparts outstanding FZG performance(higher than 12 load stages) at low treat levels(0.15 – 0.20%).Multifunctional additive with excellent extreme pressure/antiwear and antioxidation properties. Can be used asan ashless alternative to zinc dialkyldithiophosphates inindustrial lubricants, greases, and metalworking fluids.Multifunctional additive with excellent extreme pressure/antiwear and outstanding steel corrosion inhibitingproperties.NSF HX-1 approved multifunctional additive - please seepage 40 for details.AWAW, CIAW, CIAW, CI, YMDAW, CI, YMDEP/AW, AO, CIEP/AW, CIEP/AW, CINA-LUBE AW technology offers excellent antiwear and FZGperformance coupled with rust and corrosion inhibition.Photos:Far Left: Base Oil without any additivesImmediate Left: Base Oil with NA-LUBE AW technologyThe NA-LUBE AW 6000 product line of unique ashless chemistries exhibits the following properties: Excellent antiwear and extreme pressure (FZG) performance Good rust and corrosion inhibition Protection of non-ferrous metals Good to excellent demulsification Solubility in a wide range of base oils, including silicone fluids Synergy with other additives(e.g., King Industries’ NA-LUBE EP and K-CORR Series) Good hydrolytic stability

Because of their multifunctionality, the NA-LUBE AW 6000 Products are used in:SolubilityScrew Compressor Oils NA-LUBE AW-6310 is strongly recommended for high performance screwcompressor oils.Rust and Oxidation OilsAutomotive Gear OilsIndustrial Gear Oils NA-LUBE AW-6110 in combination with well selected sulfur carriers (SIBtechnology/sulfurized esters) has proven to be an excellent antiwear additivefor formulating industrial gear oils requiring excellent performance in theFAG-FE8 test. NA-LUBE AW-6310 is strongly recommended for industrial gear oils.Automatic and Manual Transmission FluidsSlide Way OilsHydraulic Fluids NA-LUBE AW-6310 is strongly recommended for ashless HF-2 typehydraulic fluids.GreasesApplications for theNA-LUBE AW 6000 SeriesFood Grade Lubricants NA-LUBE AW-6400FG is NSF HX-1 registered and complies withFDA 21 CFR 178.3750.“Neat Oil” Metalworking Fluids The NA-LUBE AW 6000 Series can also be used in combination with theNA-LUBE EP 5000 Series for formulating heavy-duty chlorine-free “neatoil” metalworking fluids. NA-LUBE AW-6010 and AW-6220 are specifically designed for “neat oil”metalworking fluids, such as high-speed grinding fluids based on mineraloil or synthetic esters.Multifunctional Fluids (Hydraulic/Metalworking Fluids) NA-LUBE AW-6310 in combination with inactive sulfurized products andaminic/phenolic antioxidants can be used to formulate multifunctional fluids(hydraulic fluid/metalworking fluid) based on Group I-V base oils, includingcanola and sunflower oils.The NA-LUBE AW 6000 Series exhibits excellent solubility in a wide range of base oils, includingnaphthenic oils, solvent refined Group I base oils, hydrotreated Group II base oils, Group III baseoils, polyalphaolefins, synthetic diesters, and silicone fluids (i.e., Dow Corning 200, 510, and 550).NA-LUBE ® AW 6000 Series - Ashless Antiwear AdditivesPages 7-8

NA-LUBE ® AW 6000 Series - Ashless Antiwear Additives Performance in a Paraffinic ISO VG 46 Base OilThe following table shows the performance of NA-LUBE AW-6010, AW-6110, and AW-6220 whenadded to a paraffinic ISO VG 46 base oil.TestsBase Oil0.25%AW-60100.10%AW-6110ISO VG 46 (Group II)0.10%AW-6220Steel Corrosion (ASTM D 665, DIN 51 585) A & B Not Applicable Pass PassDemulsibility (ASTM D 1401, DIN 51 599)Oil-Water-EmulsionSeparation Time (Minutes)Copper Corrosion (ASTM D 130, DIN 51 759)3 hours, 100°C24 hours, 100°C3 hours, 135°C42-38-0101a1b1b41-39-0101a1b1b41-39-05FZG A/8.3/90 (ASTM D 5182, DIN 51 354 Part 2)Damage Load Stage >12 >12 12Four Ball Wear (ASTM D 4172)1 hour, 75°C, 1200 rpm, 30 kgf, Scar Diameter (mm)1 hour, 75°C, 1200 rpm, 40 kgf, Scar Diameter (mm)Performance of theNA-LUBE AW 6000 Series0.460.640.320.50 Performance of NA-LUBE AW-6220 as a Yellow Metal DeactivatorNA-LUBE AW-6220 also acts as a yellow metal deactivator. The table below compares theperformance of NA-LUBE AW-6220 to the performance of two common yellow metal deactivators.As the data show, at a treat level of 0.10%, NA-LUBE AW-6220 provides excellent yellow metalprotection while also providing steel corrosion protection with good antiwear properties.Tests --Base OilISO VG 46 * +100 ppm Sulfur**0.10% DMTD***DerivativeISO VG 46 +100 ppm Sulfur0.10%TolytriazoleISO VG 46 +100 ppm Sulfur1a1b1b0.400.430.10%NA-LUBE AW-6220ISO VG 46 +100 ppm SulfurSteel Corrosion(ASTM D 665, DIN 51 585) A & B Fail Fail Fail PassCopper Corrosion(ASTM D 130, DIN 51 759)3 hours, 100°C3 hours, 120ºC24 hours, 120ºC3 hours, 135ºC24 hours, 135°C4a4b4b4b4bFour Ball Wear(ASTM D 4172)Scar Diameter (mm)1 hour, 75°C, 1200 rpm, 40 kgf 0.75 0.66 0.71 0.50Four Ball Weld Load(ASTM D 2783)10 second, 25ºC, 1800 rpmOK Load (kgf)Weld Load (kgf)1001201b1b3a1b3b1401601b1b3a1b3a1401601b1b3a1b3a140160* Hydrotreated paraffinic oil (Group II) with less than 0.03% natural sulfur ** Elemental sulfur soluble in Group II oil***Dimercaptothiadiazole

Enhancing the Antiwear Performance of Extreme Pressure AgentsNA-LUBE AW-6010 in Combination with NA-LUBE EP-5218Sulfurized EP agents typically provide very good extreme pressure properties and moderateantiwear properties when used alone. One of the unique performance characteristics of an aminephosphate, such as NA-LUBE AW-6010, is the ability to improve the antiwear performance of wellselected sulfurized extreme pressure agents. As depicted below, the addition of 2.0% NA-LUBEAW-6010, reduces the scar diameter from 0.81 mm to 0.51 mm. However, additional NA-LUBEAW-6010 to approximately 6% is required to return the weld load back to the starting level of>300 kgf.Different Levels of NA-LUBE AW-6010 in Group II Oil containing 10% NA-LUBE EP-5218Four Ball Wear Test (ASTM D 4172) - 1 hour, 75ºC, 40 kgf, 1200 rpm, - Four Ball Weld (ASTM D 2783) - 10 seconds, 25°C, 1800 rpmWeld Load (kgf)3503002502001501005000% 1% 2% 3% 4% 5% 6% 7% 8% 9% 10%% NA-LUBE AW-6010 NA-LUBE AW-6330 as an Ashless Alternative to Zinc DialkyldithiophosphatesNA-LUBE AW-6330 Comparison to ZnDTPAs shown below, NA-LUBE AW-6330 is an excellent ashless alternative to zinc dialkyldithiophosphates. Itoffers outstanding performance in Group I, II and synthetic base stocks.TestsBase Oil1.0%AW-63301.0%ZnDTP*WeldWear1.0% AW-63300.35% Blend**Steel Corrosion (ASTM D 665, DIN 51 585) A & B Pass Pass PassDemulsibility (ASTM D 1401, DIN 51 599)Oil-Water-EmulsionSeparation Time (Minutes)Copper Corrosion (ASTM D 130, DIN 51 759)3 hours, 100°C3 hours, 135°C42-38-052a2a41-39-0102a2aISO VG 46 (Group I)42-38-051b1b0.90.80.70.60.50.40.30.20.10Average ScarDiameter (mm)1.0% ZnDTP0.35% Blend**Pass43-35-2301a-NA-LUBE ® AW 6000 Series - Ashless Antiwear AdditivesFZG A/8.3/90 (ASTM D 5182, DIN 51 354 Part 2)Damage Load Stage 12 12 1212Four Ball Wear (ASTM D 4172)1 hour, 75°C, 1500 rpm, 30 kgf, Scar Diameter (mm)1 hour, 75°C, 1800 rpm, 40 kgf, Scar Diameter (mm)0.42-0.37--0.54-0.45Pages 9-10* ZnDTP based on 2-ethylhexanol (stabilized) ** 0.35% Blend of yellow metal deactivator, aminic and phenolic antioxidants

NA-LUBE ® AW 6000 Series - Ashless Antiwear Additives Performance of the Unique NA-LUBE AW-6310NA-LUBE AW-6310 is an innovative extension of the other NA-LUBE AW products. It is aproprietary composition containing unique sulfur/phosphorus/nitrogen chemistries.NA-LUBE AW-6310 exhibits the following properties:Superior FZG performanceOutstanding rust inhibitionExcellent demulsificationGood hydrolytic stabilityGood thermal stabilityOutstanding synergy with the NA-LUBE AO SeriesExcellent solubility in a wide range of base oils, including some silicon fluidsNA-LUBE AW-6310 is used in screw compressor oils, railroad type non-mineral oil (Group V)greases, industrial gear oils, and automotive gear oils. It can also be used for formulating extremelyeffective ashless HF-2 type hydraulic fluids as shown below:TestsBase OilDemulsibility (ASTM D 1401, DIN 51 599)Oil-Water-EmulsionSeparation Time (Minutes)Steel Corrosion (ASTM D 665, DIN 51 585) A & B0.15% NA-LUBE AW-63100.20% NA-LUBE AO-2100.10% NA-LUBE AO-1300.03% K-CORR NF-20040-40-010PassAFNOR Wet Filtration (E 68691)Filterability Index 1.17Copper Corrosion (ASTM D 130, DIN 51 759)3 hours, 100°C3 hours, 135°CFZG A/8.3/90 (ASTM D 5182, DIN 51 354 Part 2)Damage Load Stage >12CM Thermal Stability (ASTM D 2070)CM Color Class: CopperSteelViscosity Change, %Acid Number Change (mg KOH/g)Total Sludge (mg/100 ml)Hydrolytic Stability (ASTM D 2619)Copper Loss (mg/cm²)Total Acidity of Water Layer (mg KOH)Copper Appearance (ASTM D 130)ISO VG 46 (Group II)1b1b530.510.0314.80NA-LUBE AW-6310 also exhibits very good performance in greases. The table below depicts theperformance of NA-LUBE AW-6310 in a synthetic lithium complex grease.Tests Without Additive NA-LUBE AW-63100.003.473bTreat Level, % — 2.0Base GreaseSynthetic Lithium ComplexTest Water5% Synthetic Sea WaterEMCOR Rust Test (ASTM D 6138, IP 220) 2,2 0,0Four Ball Wear (ASTM D 2266)1 hour, 75˚C, 40 kgf, 1200 rpmScar Diameter (mm) 0.73 0.48

R1H׀NR2NA-LUBE ® AO SeriesPrimary AntioxidantsNA-LUBE AO-130& NA-LUBE AO-142t-ButylProductNA-LUBEAO-130NA-LUBEAO-142NA-LUBEAO-210NA-LUBEAO-242OHHt-ButylNA-LUBE AO-210t-ButylHOt-ButylOC 3OR3NA-LUBE AO-242For R 1, R 2, and R 3, seechemical descriptions below.ChemicalDescriptionFormNitrogenApprox.(%)Flash Point,COC(ASTM D 92)Approx.(°C)Dinonyldiphenylamine Liquid 3.5 165Octyl/butyldiphenylamine2,6 Ditertbutylphenol2,6 DitertbutylphenolDerivativeThe NA-LUBE AO product line is a series of phenolic and aminicantioxidants that is used in a broad range of industrial lubricants, engineoils, and greases. These products retard the oxidation of lubricants thusreducing sludge formation and viscosity increase, providing economicand ecological benefits. The NA-LUBE antioxidants exhibit the followingphysical and performance properties:Liquid 4.5 185Solid at< 36° CAshlessNon-corrosiveExcellent solubility in a wide range of base fluidsEnhanced thermal and oxidative stabilityBoth solid and liquid NA-LUBE AO products are available to offermaximum formulating flexibility.NA-LUBE ADTC is a unique multifunctional additive that not onlyprovides outstanding antioxidant properties but also extreme pressureand antiwear properties.— >100Liquid — 148DescriptionExcellent antioxidant with outstandingproduct stability at low temperatures.Excellent antioxidant that is in compliancewith the Food and Drug AdministrationRegulation 21 CFR 178.3570 (lubricantswith incidental food contact) up to a treatlevel of 0.5% by weight. HX-1 registered# 140584.General purpose antioxidant with verylow volatility compared to BHT.High temperature antioxidant with lowvolatility and low viscosity. Providesreduced sludge formation.NA-LUBE ® AO Series - Primary AntioxidantsProductChemicalDescriptionSulfurApprox.(%)NitrogenApprox.(%)Flash Point,COC(ASTM D 92)Approx.(°C)DescriptionNA-LUBEADTCMethylene-bisdibutyldithiocarbamate30.0 6.5 180NA-LUBE ADTC is a unique ashlessdithiocarbamate offering extremepressure, antiwear and antioxidantproperties.Pages 11-12

Synergistic Effects of Aminic and Phenolic AO CombinationsNA-LUBE ® AO Series - Primary AntioxidantsAminic and phenolic antioxidants impart excellent oxidation stability to formulated functional fluids.Each type provides excellent protection as the sole antioxidant, or they can be used in combinationto take advantage of their synergistic strength to provide outstanding long-term protection. Below isan example of the synergistic effect.Synergy of NA-LUBE AO-142 and NA-LUBE AO-2425004003002001000Rotating Pressure Vessel Oxidation Test(ASTM D 2272)RPVOT (minutes)5004003002001000Base Oil: ISO VG 46 Group II0.20% AO-242 0.20% AO-142 0.10% AO-2420.10% AO-1420.10% AO-2420.10% AO-1420.05% K-CORR NF-200 NA-LUBE AO-142 Performance in Various HX-1 Base OilsFORMULATIONSBase OilTestViscosity@40°CBase Oil WithoutNA-LUBE AO-142Turbine Oil Oxidation Test(ASTM D 943)TOST (hours to TAN > 2 mg KOH/g)Base Oil With0.2% NA-LUBE AO-1425004003002001000.10% AO-2420.10% AO-1420.05% K-CORR NF-2000.05% K-CORR 1031RPVOT - Rotating Pressure Vessel Oxidation Test(ASTM D 2272) Lifetime - MinutesBase Oil With0.5% NA-LUBE AO-142PAO 10 66 cSt 55 266 1095White Oil 110 cSt 31 141 762PAG (Water Soluble) 120 cSt 15 40 344NA-LUBE KR-015FG 114 cSt 92 443 930NA-LUBE KR-029FG 177 cSt 76 905 1400Ester 220 cSt 115 470 2650

NA-LUBE ® ADTCMultifunctional Ashless DialkyldithiocarbamateNA-LUBE ADTC is a unique, ashless dialkyldithiocarbamate additive that offers excellent extremepressure, antiwear, and antioxidant properties. NA-LUBE ADTC has well-defined chemistry withsulfur and nitrogen present in the same molecule. Performance of NA-LUBE ADTC - Ashless Hydraulic Fluid PackageThe table below shows the performance capabilities of NA-LUBE ADTC in an ashless hydraulic fluidpackage containing K-CORR 1031, an amino acid derived rust inhibitor.TestsProductNA-LUBE ADTCCompositionMethylene-bisdibutyldithiocarbamateNA-LUBE ADTC exhibits the followingproperties:Excellent extreme pressure andantiwearExcellent oxidation inhibitionOutstanding demulsificationGood thermal stabilityExcellent solubility in highlyparaffinic base stocksASHLESS PACKAGE: NA-LUBE ADTC, NA-LUBE AO-130,NA-LUBE AW-6220, K-CORR 1031Treat Level of Additive Package, % 0.5 1.0Base Oil ISO VG 32 (Group I)Demulsibility (ASTM D 1401, DIN 51 599)Oil-Water-EmulsionSeparation Time (Minutes)SulfurApprox.(%)C 4 H 9 SN CC 4 H 9 S CH 242-38-010NitrogenApprox.(%)41-38-110Steel Corrosion (ASTM D 665B, DIN 51 585) Pass PassCopper Corrosion (ASTM D 130, DIN 51 759)3 hours, 135°C 1a 1aRPVOT* (ASTM D 2272) Lifetime (Minutes) 495 1260Four Ball Wear (ASTM D 4172)1 hour, 75°C, 40 kgf, 1200 rpm, Scar Diameter (mm) 0.50 0.47AFNOR Wet Filtration (E 68691)Filterability Index 1.25 1.10FZG A/8.3/90 (ASTM D 5182, DIN 51 354 Part 2)Damage Load Stage Not Determined >12Viscosity @ 100°C(ASTM D 445)Approx. mm 2 /s (cSt)30 6.5 15SCSDue to its multifunctionality, NA-LUBE ADTC isused in:NNA-LUBE ADTCPROPERTIES & USESC 4 H 9C 4 H 9Heavy Metal-free GreasesRust and Oxidation OilsAutomotive and Industrial Gear OilsExtreme Pressure Turbine OilsHydraulic OilsEngine OilsMetalworking FluidsNA-LUBE ® ADTC - Ashless DialkydithiocarbamatePages 13-14* Rotating Pressure Vessel Oxidation Test

NA-LUBE ® EP 5000 Series - Extreme Pressure AdditivesNA-LUBE ® EP 5000 SeriesExtreme Pressure / Antiwear AdditivesThe NA-LUBE EP 5000 Series consists of low odor, light-colored fatty acid esters, sulfurized fattyacid esters/triglycerides, and sulfurized α-olefins/triglycerides.Light-colored, low odor sulfur-containing additives are primarily produced by using hydrogen sulfideand elemental sulfur. The reaction is usually performed under high pressure and high temperatureconditions. Light-colored, low odor sulfur-containing additives have improved properties over thewell-known “black” sulfur-containing additives, including significantly improved oxidative stability andbetter solubility in highly paraffinic base oils.Sulfur-containing additives are commonly known in the lubricant and grease industry as “sulfurcarriers”. The different raw materials used for the production of these additives have a significantimpact on the properties and performance of the different sulfur carriers. Products based on shortchainolefins, such as isobutylene, can be called “dry” sulfur carriers because they only provideEP/AW properties; while those based on esters and triglycerides (fatty oils) can be called “wet”sulfur carriers because they also improve boundary lubrication.One of the most important characteristics of sulfur carriers is sulfur activity as measured inaccordance with the ASTM D 1662 test. The active sulfur content primarily depends on thepolysulfide chain length in the molecule. Sulfur-containing additives with a very low active sulfurcontent (6%) primarilyprovide extreme pressure properties.The NA-LUBE EP 5000 Series is manufactured from carefully selected raw materials to optimizeproduct quality and performance. Precisely controlled manufacturing processes result in productsthat are of light color and low odor.ProductNA-LUBEEP-5210NA-LUBEEP-5216NA-LUBEEP-5218NA-LUBEEP-5310NA-LUBEEP-5316NA-LUBEEP-5415% TotalSulfur% ActiveSulfurViscosity@ 40ºC(cSt)10

The NA-LUBE EP 5000 Series consists of a variety of novel sulfur-containing additives with totalsulfur content ranging from approximately 10% to 65% and the active sulfur content ranging from

NA-LUBE ® EP 5000 Series - Extreme Pressure AdditivesPerformance of theNA-LUBE EP 5000 Series Series Performance in a ISO VG 32 Group I Base OilThe following table highlights the performance of the products in various bench tests for lubricationproperties.TestsNA-LUBEEP-5210NA-LUBEEP-5216NA-LUBEEP-5218Base Oil ISO VG 32 (Group I)Treat Level, % 5.0Four Ball Weld (ASTM D 2783)10 seconds, 25°C, 1800 rpmOK Load (kgf)Weld Load (kgf)160200200240200240NA-LUBEEP-5316200240NA-LUBEEP-5415Four Ball Wear (ASTM D 4172)1 hour, 75°C, 40 kgf, 1200 rpmScar Diameter (mm) 0.54 0.58 0.81 0.68 0.60Copper Corrosion(ASTM D 130, DIN 51 759)3 hours, 100ºC24 hours, 100ºC NA-LUBE EP-5210 - Concentration Effect On Properties1a2aAs shown below, with increasing concentrations of NA-LUBE EP-5210, the wear and extremepressure properties improve with no negative effects on demulsibility or copper corrosion protection.Tests2.0% NA-LUBEEP-52103a4a7.5% NA-LUBEEP-52103a4a10.0% NA-LUBEEP-5210Base Oil ISO VG 32 (Group I)Four Ball Weld (ASTM D 2783)10 seconds, 25°C, 1800 rpmOK Load (kgf)Weld Load (kgf)1201601602001602001b3b2202401b3b10.0% NA-LUBE EP-52106.0% NA-LUBE AW-6010Four Ball Wear (ASTM D 4172)1 hour, 75°C, 40 kgf, 1200 rpmScar Diameter (mm) 0.72 0.59 0.60 0.50Falex PIN & VEE (ASTM D 3233)Lbs. 890 1050 1060 950Copper Corrosion(ASTM D130, DIN 51 759)3 hours, 100ºC24 hours, 100ºCDemulsibility(ASTM D 1401,DIN 51 599Oil-Water-EmulsionTime (Minutes)1a3a39-39-2101a2a41-39-0101a2a41-39-0102002401b2a40-40-010

NA-LUBE EP-5415 Metalworking Performance DataNA-LUBE EP-5415 imparts good extreme pressure performance for metalworking fluids and can beused to replace chlorinated paraffins as shown in the chart below.TestsAs shown below, tapping torque tests were conducted to compare the performance of NA-LUBEEP-5415 versus the performance of a commonly used chlorinated paraffin. The tests wereconducted using 4340 alloy steel under varying machining speeds.4340 Alloy SteelBase Oil: Paraffinic ISO VG 3210% Chlorinated ParaffinAverage Peak Torque(inch - pounds)10% NA-LUBE EP-5415Average Peak Torque(inch - pounds)% Efficiency40 sfm* (407rpm) 68.8 70.79 97.248 sfm (488rpm) 69.2 71.32 97.058 sfm (586rpm) 71.0 69.88 101.669 sfm (703rpm) 71.7 72.05 99.583 sfm (844rpm) 69.1 70.95 97.4*sfm = surface feet per minuteAdditionally, NA-LUBE EP-5415 can be used to formulate premium quality machine tool slide waylubricants. Various treat levels of NA-LUBE EP-5415 in combination with 0.5% tackifier in an ISOVG 68 oil meet the requirements of the Cincinnati Lamb P-47 Heavy-Medium Way Oil specification.Tests1.5% NA-LUBE EP-54150.5% Tackifier5.0% NA-LUBE EP-54150.5% TackifierCincinnati LambP-47 SpecificationBase Oil ISO VG 68 ISO VG 68 cSt @ 40ºC:61.6-74.8SUS @ 100ºF:317-389Flash Point (ASTM D 92)COC (ºF) >380 >380 330 MinimumFire Point (ASTM D 92)COC (ºF) >380 >380 360 MinimumAcid Number (ASTM D 974)(mg KOH/g) 0.07 0.10 1.7 MaximumCincinnati Lamb Stick-Slip(μs/μK)* 0.0710 / 0.0982 = 0.72 0.0783 / 0.1009 = 0.78 0.80 MaximumThermal Stability TestProcedure B: 24 hours, 101ºCCM Color ClassRod Weight of Deposit (mg)Rod Metal Loss (mg)Acid Number Change (mg KOH/g)PrecipitateSteel Copper1 30.30 1.00.2 0.40.07None10% Mid-chain ChlorinatedParaffin (C 14-17 >50% Cl)Base Oil ISO VG 32 (Group I)Four Ball Weld (ASTM D 2783)10 seconds, 25°C, 1800 rpmOK Load (kgf)Weld Load (kgf)160180Steel Copper1 30.35 1.20.3 0.40.07None10% NA-LUBEEP-5415Four Ball Wear (ASTM D 4172)1 hour, 75°C, 40 kgf, 1200 rpm 0.80 0.75Copper Corrosion (ASTM D 130, DIN 51 759)3 hours, 100ºC 1a 1b320340Maximum LimitsSteel Copper1 53.5 --1.0 5.05--NA-LUBE ® EP 5000 Series - Extreme Pressure AdditivesPages 17-18* Ratio of static to kinetic friction

NA-SUL ®Rust & Corrosion InhibitorsSince the introduction of the first products in 1952, the NA-SUL trade name has been synonymouswith high quality, cost-effective rust protection. After 50 years of continuous improvement andinnovation, these unique synthetic sulfonates continue to be recognized as the premium rust andcorrosion inhibitors for industrial and automotive lubricants, greases, metalworking fluids, and rustpreventives.NA-SUL ® Rust & Corrosion InhibitorsThe NA-SUL line is based upon salts of dinonylnaphthalenesulfonic acid. Controlled alkylation ofnaphthalene with nonene produces dinonylnaphthalene. This is then sulfonated to produce thebuilding block sulfonic acid that becomes a NA-SUL when neutralized to form various salts. NA-SULproducts use a wide variety of neutralizing metals and amines resulting in the world’s broadest lineof sulfonates.The NA-SUL line provides excellent rust and corrosion protection in addition to other uniqueperformance properties. King’s process of direct neutralization produces sulfonates with no chlorine,resulting in enhanced rust protection and resistance to staining.PerformanceRust & Corrosion ProtectionThe NA-SUL line consistently outperforms other synthetic orpetroleum sulfonates, thus offering:Better performance at equal or lower concentrationsHigher maximum performanceFerrous and non-ferrous metal protectionSynergy with other anti-rust additivesUnsurpassed DemulsibilityNA-SUL Inhibitors OfferSuperior PerformanceASTM D 665 B0.025% 0.05% 0.05% 0.05%NA-SUL COMP. COMP. COMP.729 A B CPerformance BeyondRust & Corrosion ProtectionIn addition to superior rust and corrosioninhibition, NA-SUL inhibitors impart otherdesirable performance properties to industriallubricants and rust preventive applications,including:Unsurpassed demulsibilityEnhanced oxidation stabilityExcellent filterabilityExcellent additive compatibilityExcellent solubilityCalciumDinonylnaphthaleneSulfonateNA-SUL 729CalciumPetroleumSulfonateSyntheticCalciumSulfonate ASyntheticCalciumSulfonate B

Acid # (mg KOH/g)2.50.5Enhanced Oxidation Stability of NA-SUL 72921.510Increase in Acid Value vs. TimeFORMULATION0.25% NA-SUL 7290.25% Phenolic Antioxidant99.5% Paraffinic Oil0 20 40 50 60 80 100 120 140Hours in ASTM D 4636 @ 150ºCNA- SUL 729 Didodecylbenzene Sulfonate Oil + AO w/o SulfonateImproved FilterabilityAFNOR Filtration (Wet) - ISO VG 46 Group II OilTreat LevelFORMULATIONHF-0 Type Package*Without NA-SUL 7290.8% of Additive Package*Package: ZnDTP (Primary C8), Yellow Metal Deactivator and AntioxidantsEnhanced OxidativeStabilityIn addition to unsurpassedrust and corrosion protectionand demulsibility, NA-SULsulfonates can enhance oxidativestability performanceas shown in the graph to theleft.NA-SUL Sulfonates can also improve filterability. The table below compares the Wet AFNORFiltration when NA-SUL 729 was incorporated into a Denison HF-0 type package at 9.0% replacingoil so that the concentration of all other additives was held constant. This package was then addedto the oil at a treat level of 0.8%, resulting in a final NA-SUL 729 concentration in the oil of 720ppm. The package without NA-SUL 729 plugged the filter, while the package with the NA-SUL 729passed the AFNOR Filtration. A good AFNOR Filterability Index is

NA-SUL Rust & Corrosion Inhibitors - TypesNA-SUL TYPE PRIMARY USES PAGE NA-SUL TYPE PRIMARY USES PAGENeutral Metal Salts Ind. Lubes/RP’s 21 Specialty Grades Ind. Lubes/RP’s 22Amine Salts Ind. Lubes/Fuel/RP’s 21 RP Concentrates RP’s 27NA-SUL ® Rust & Corrosion InhibitorsBasic Metal Salts Lubricants/RP’s 22 Aqueous RP’s/Cleaners 31RSO 3Neutral dinonylnaphthalenesulfonates are used in almost all applications where premium rust andcorrosion inhibitors are required. The divalent metal salts also exhibit excellent demulsibility.Several of the neutral metal sulfonates are available in a variety of diluents.ProductNA-SUL 707NA-SUL 729NA-SUL BSNNA-SUL MGNA-SUL SSNA-SUL ZSRMM M = Ca, = Ca, Ba, Ba, Mg, Mg and or ZnRSO 32Metal DNNS Salt*(Metal Approx. %)R. R'NH 32Lithium(0.76)Calcium(2.1)Barium(6.6)Magnesium(1.3)Sodium(2.4)Zinc(2.8)NA-SUL Neutral Metal SaltsDescriptionLow ash rust inhibitor with good high temperature stability in industrial oilsand greases. Retards bleeding in lithium soap greases.Premium rust inhibitor for petroleum and synthetic lubricants, hydraulic fluidsand circulating oils. Outstanding water resistance properties, includingdemulsibility, wet filterability, and hydrolytic stability.Premium rust inhibitor for industrial lubricants, greases, rust preventivefluids, and metalworking specialties. Excellent water resistance properties.Non-staining to metal surfaces. Widely used in gear oils and greases.Lowest ash premium rust inhibitor. Particularly effective in rust preventiveapplications exposed to water, such as ballast tank coatings.High molecular weight sodium sulfonate. Not an emulsifier, but excellentadditive to enhance rust preventive properties of emulsions.Premium rust inhibitor for industrial oils, greases, and hydraulic fluids,particularly when used in combination with zinc dithiophosphates.NA-SUL Amine Salts (Ashless)RSO 3. MM=Lior NaRNeutralization with amines, instead of metals, produces ashless sulfonates. The base strength andvolatility of the amine chosen influences the properties and applications.ProductNA-SUL ASNA-SUL DTANA-SUL EDSAmine DNNS Salt*(Nitrogen Approx. %)Ammonia(1.5)Diethylenetriamine(0.5)Ethylenediamine(0.7)DescriptionAshless rust inhibitor used in a wide range of petroleum fluids, includingdistillate fuels. May be used as a supplemental additive withother rust inhibitors.Stable ashless rust inhibitor with good demulsibility in petroleum andsynthetic lubricants.Ashless rust inhibitor for lubricants, distillate fuels, and mild-duty rustpreventives. Diluent is 70°C flash aliphatic solvent.* Diluent is light Mineral Oil with the exception of NA-SUL EDS.

NA-SUL Basic Metal SaltsRRCa·CaCO3SO 32Basic sulfonates find application as rust inhibitors in lubricants, greases and metalworking specialtieswhere alkalinity is desirable to neutralize mild acid contamination, thus improving oxidationstability. They are also used in rust preventives to improve performance when applied overcontaminated substrates.ProductNA-SUL 611NA-SUL BSBNA-SUL CA-50Several specialty NA-SUL grades have evolved for applications with different requirements than thesulfonates alone can provide. Various complexes take advantage of synergisms to enhanceproperties.ProductNA-SUL 729-NFNA-SUL CA-770FGNA-SUL BSN-HTNA-SUL CA-1089Metal DNNS Salt*(Metal Approx. %)Barium(11.7)Barium(12.0)Calcium(3.2)DNNS Salt Derivative*(Metal Approx. %)Calcium with YMD**(1.9)Calcium(1.7)Barium Complex(8.7)Calcium Complex(2.2)DescriptionApproximate TBN is 45 mg KOH/g as barium carbonate. Particularlyeffective in polyglycol/ester based compressor fluids.Approximate TBN is 45 mg KOH/g as barium hydroxide. Versatile rustinhibitor additive for rust preventives, greases and lubricants containingacidic components.Approximate TBN is 50 mg KOH/g as calcium carbonate. Excellentresistance to salt water environments, particularly in greases and rustpreventive fluids. Also used in high performance military hydraulic fluids.NA-SUL Grades for Specialty LubricantsDescriptionComplexes andHX-1 RegisteredSynergistsPremium ferrous rust inhibitor plus yellow metal deactivatorfor non-ferrous corrosion protection.Calcium based sulfonate in PAO specifically designed for usein food grade applications. NSF HX-1 Registration # 143718.Synergistic rust inhibitor with excellent thermal stability.Particularly suited for high temperature applications.Exceptional additive providing excellent rust protection,demulsibility, filterability (dry and wet), and thermal stability.Makes excellent RP fluids and dewatering fluids because ofits superior water resistance.NA-SUL ® Rust & Corrosion InhibitorsNA-SUL CA-HT3Calcium Complex(2.5)Excellent rust inhibitor with thermal stability and gooddemulsibility required for applications such as paper machineoils and high temperature circulating fluids.NA-SUL MG-HTMagnesium Complex(1.7)Synergistic rust inhibitor with good thermal stability.Particularly effective at neutralizing the corrosivity andstaining of chlorinated paraffins.NA-SUL ZS-HTZinc Complex(3.8)Excellent rust inhibitor, particularly in systems with other zinccontaining additives. Exhibits antioxidation synergism withprimary antioxidants in petroleum and PAO base fluids.Pages 21-22* Diluent is light Mineral Oil with the exception of NA-SUL CA-770 FG, ** YMD = Yellow metal deactivator

NA-SUL CA-1089Hydraulic Fluid Performance DataNA-SUL ® Rust & Corrosion InhibitorsNA-SUL CA-1089 is a calcium sulfonate/carboxylate complex that imparts outstanding steelcorrosion protection, demulsibility and filtration performance to formulated functional fluids. Hydraulicfluids meeting the Denison HF-0 specification can be developed using NA-SUL CA-1089 as thecorrosion inhibitor/demulsifier portion of the formulation. NA-SUL CA-1089 Performance in a Denison HF-0 Type Hydraulic Fluid PackageHF-0 Type Package w/o NA-SUL w/ 2.0% NA-SULTestsCA-1089 CA-1089Treat Level of Additive Package, % 0.8Base OilISO VG 46 (Group II)w/ 4.5% NA-SULCA-1089Additive Package Color Light Amber Light Amber Light AmberSteel Corrosion (ASTM D 665, DIN 51 585)A & B Fail Pass PassDemulsibility (ASTM D 1401, DIN 51 599)Oil-Water-EmulsionTime (Minutes)41-34-53040-39-11039-39-210Four Ball Wear (ASTM D 4172)1 hour, 75°C, 40 kgf, 1200 rpmScar Diameter (mm) 0.42 0.41 0.40Copper Corrosion (ASTM D 130, DIN 51 759)3 hours, 100°C3 hours, 135°C3 hours, 160°CCincinnati Milacron Thermal Stability (ASTM D 2070)CM Color Class: CopperSteelViscosity Change, %Acid Number Change (mg KOH/g)Rod Weight of Deposit, Steel / Copper (mg/200ml)Rod Metal Loss, Steel / Copper (mg/200ml)Total Sludge (mg/100 ml)Whatman Precipitate (mg/100 ml)Millipore Precipitate (mg/100 ml)Hydrolytic Stability (ASTM D 2619)Copper Loss (mg/cm 2 )Total Acidity of Water Layer (mg KOH)Copper Appearance (ASTM D 130)1b1b1b1.51.51.80.230.1 / 0.10.2 / 0.65.52.72.80.290.912a1b1b1b1.01.52.10.360.2 / 0.70.0 / 0.13.60.72.80.050.701b1b1b1b1.01.51.30.300.2 / 0.30.0 / 0.21.70.41.20.301.101bAFNOR Wet Filtration (E 68691)Filterability Index Plugged 1.34 1.27FZG A/8.3/90 (ASTM D 5182, DIN 51 354 Part 2)Damage Load Stage 12 12 12This table compares the performance of a Denison HF-0 type package for hydraulic fluids with andwithout NA-SUL CA-1089. NA-SUL CA-1089 was incorporated into the package at 2.0% and 4.5%replacing the oil. The concentrations of all other additives were held constant. Testing wasconducted at a package treat level of 0.8% in an ISO VG 46 Group II oil resulting in final NA-SULCA-1089 concentrations of 0.036% and 0.016% in the oil. The package without NA-SUL CA-1089failed the steel corrosion, demulsibility, and AFNOR filtration tests and resulted in notable copper lossin the hydrolytic stability test. Inclusion of NA-SUL CA-1089 in the formulation imparted excellentsteel corrosion protection, demulsibility, and AFNOR filtration performance and greatly reduced theamount of copper loss in the hydrolytic stability test when tested at the lower concentration. Theimproved AFNOR filtration performance is attributed to the excellent dispersancy characteristics ofNA-SUL CA-1089. NA-SUL CA-1089 also exhibited no adverse effects on other performance tests,including four ball wear, copper corrosion, Cincinnati Milacron thermal stability and FZG.

NA-SUL CA-1089Performance In Rust PreventivesNA-SUL CA-1089 is not only an excellent rust inhibitor for industrial lubricants, as shownpreviously in the hydraulic fluid example, but is also highly effective in a broad range ofrust preventive applications where it offers:Remarkable non-staining performance in stacked stain testing in all oils tested, makingit an outstanding barium sulfonate replacement. Highly recommended for protection ofcoiled steel and closely stacked steel parts.Exceptional performance in both cyclic and constant humidity testing, making it anexcellent choice for most parts storage applications.Outstanding water displacement and demulsibility performance, including acidic andbasic aqueous fluids. A perfect choice for difficult dewatering fluids.Excellent solubility in paraffinic oils, PAO, esters and vegetable oils. A versatileadditive that can be used in a variety of products using different base stocks. NA-SUL CA-1089 Performance in a Paraffinic ISO VG 32 Base OilTests2.0% CA-108998.0% Oil #15.0% CA-108995.0% Oil #110.0% CA-108990.0% Oil #1Average Film ThicknessMeasured by Weight (m) 2.8 2.8 3.0Salt Fog (ASTM B 117)Average Hours to Failure 3-5 5-10 12-15Humidity Cabinet (ASTM D 1748)Average Hours to Failure 100-125 300-350 450-500 NA-SUL CA-1089 Performance in a Solvent/Oil Based System*Tests3.0% CA-108920.0% Oil #177.0% Solvent5.0% CA-108920.0% Oil #175.0% Solvent10.0% CA-108920.0% Oil #170.0% SolventAverage Film ThicknessMeasured by Weight (m) 1.8 2.0 2.4Salt Fog (ASTM B 117)Average Hours to Failure 5-10 5-10 16-20Humidity Cabinet (ASTM D 1748)Average Hours to Failure 230-300 400-500 500-600* Solvent: 40°C Mineral Spirits, Oil: Paraffinic ISO VG 32 (150 SUS)“Hours to failure” is defined as rust more than 1.5 cm from the top panel edge or more than 0.5 cm from either side edge.NA-SUL ® Rust & Corrosion Inhibitors NA-SUL CA-1089 Performance - Accelerated Stacked Stain Test10.0% CA-108990.0% Oil #15.0% CA-108995.0% Oil #2Stack Stain7-Day Accelerated Pass PassOil #1 - Paraffinic Group I - ISO VG 32 (150 SUS)Oil #2 - Paraffinic Group II - ISO VG 46 (220 SUS)5% NA-SUL CA-108995% Group II ParaffinicISO VG 46 (220 SUS)5% Commercial RP95% Group II ParaffinicISO VG 46 (220 SUS)Pages 23-24

King Industries, Inc. - Lubricant Additives DivisionPRODUCTS & APPLICATIONS CHART*CHART KEY:ApplicationsColored Box = RecommendedTR= Technical Report AvailableCirculatingOilsCompressorOilsGearOilsGreaseHydraulicFluidsPowerTransferTurbineOilsGearOilsEngineOilsSolubleOilsCuttingOilsOil/SolventBasedAqueousEmulsionAqueousSolutionNA-LUBE EP ExtremePressure AdditivesNA-LUBE EP-5210NA-LUBE EP-5216NA-LUBE EP-5218NA-LUBE EP-5310NA-LUBE EP-5316NA-LUBE EP-5415NA-LUBE EP-5425NA-LUBE EP-5665NA-LUBE ADTC NA-LUBE ADTC TR TRNA-LUBE AW-6010NA-LUBE AWAntiwear AdditivesNA-LUBE AW-6110NA-LUBE AW-6110PNA-LUBE AW-6220 TR TRNA-LUBE AW-6310 TR TRNA-LUBE AW-6330NA-LUBE AW-6360 TR TRNA-LUBE AW-6400FGIndustrial Lubricants Automotive Metalworking Rust Preventive SystemsTRTRTRTRTRTRTRTRTRNA-LUBE AOAntioxidantsNA-SULNeutral Metal SaltsNA-SULBasic Metal SaltsNA-SULAshless / Amine SaltsNA-SULConcentratesfor Oil & Oil/SolventRust Preventive SystemsNA-SULAdditives forAqueous SystemsNA-SULAdditives forSpecialty LubricantsK-CORRNA-LUBE AO-130NA-LUBE AO-142NA-LUBE AO-210NA-LUBE AO-242NA-SUL 707TRNA-SUL 729 TR TR TR TRNA-SUL BSN TR TRNA-SUL MGTRNA-SUL SS TR TRNA-SUL ZSNA-SUL 611NA-SUL BSBNA-SUL CA-50NA-SUL ASNA-SUL DTANA-SUL EDSNA-SUL CA-1082TRNA-SUL CA-1089 TR TRNA-SUL CA-1183NA-SUL CA-1259NA-SUL CA/W1146NA-SUL CA/W1177NA-SUL CA/W1213NA-SUL TEA/LBNA-SUL 1019ANA-SUL 437NA-SUL 420KX450NA-SUL BSN-HTNA-SUL CA-770FGTRNA-SUL CA-1089 TR TRNA-SUL CA-HT3 TR TR TRNA-SUL MG-HT TR TRNA-SUL ZS-HT TR TRNA-SUL 729-NF TR TRK-CORR 100 TR TRK-CORR 100A2K-CORR 1031K-CORR G-1086AK-CORR G-1107K-CORR G-1270K-CORR ZN-510K-CORR NF-200 TR TRK-CORR NF-410TRTRTRTRK-CORR SA-300 TR TR TRTRTRTRTRTRTRTRTR* See inside back cover for information regarding recommendations and product uses.

Technical Assistance: (203) 866-5551 lad@kingindustries.comApplicationsCharacteristicsHotMeltWaxThickFilmPostTensioningGreaseDemulsibilityDispersancyOxidativeStabilityThermalStabilityWaterDisplacementAcidAtmosphere Anti-StainWaterSolubleWaterEmulsifiableNonferrousAshlessProtectionSulfurCarrier,ActiveSulfurCarrier,InactivePhosphorusPhenolicAOAminicAORust Preventive SystemsTRTRTRTR TR TRTRTRTRTRTRTRTRTRTRTRTR

NA-SUL Rust and CorrosionPreventive AdditivesNA-SUL ® Rust & Corrosion InhibitorsKing Industries’ rust preventive additives are generally based on salts of dinonylnaphthalenesulfonatewith additional polar compounds chosen to provide rust preventive synergy. This results inextremely hydrophobic rust preventive coatings that effectively exclude water and air from reachingthe metal surface. The resulting performance advantage provides levels of metal protection thatcompetitive additives cannot achieve and/or reductions in additive use levels that result in significantformulation savings.NA-SUL Rust Preventive Concentrates for Oil and Oil/Solvent SystemsProductNA-SUL CA-1089NA-SUL CA-1183Formerly KX1183NA-SUL CA-1259Formerly KX1259NA-SUL CA/W1146NA-SUL CA/W1177Formerly KX1177NA-SUL CA/W1213Formerly KX1213NA-SUL CA-HT3Form(% Calcium)Liquid(2.2%)ViscousLiquid(2.6%)Liquid(1.6%)Very ViscousLiquid(2.0%)ViscousLiquid(1.4%)ViscousLiquid(1.4%)Liquid(2.5%)DescriptionExcellent general purpose rust preventive additive. Good dewateringproperties. Good performance after water contamination. Recommendedfor medium to long term indoor storage.Provides excellent corrosion protection for steel, galvanized steel andaluminum with good water separation characteristics. Designed for usewhere water contact is likely, such as dewatering fluids.High performance rust and corrosion inhibitor for rust preventives anddewatering fluids. Excellent solubility (should be verified) in a wide rangeof mineral oils, esters, and vegetable oils. Particularly recommendedwhere water displacement is important.Recommended for heavy duty applications, such as sheltered outdoorstorage and marine environments. Best in naphthenic oils. Effective inacid atmospheres. Not recommended if water contamination will occurbefore application on metals.Specifically designed for use where water contact is likely, such asdewatering fluids. It combines excellent corrosion protection with goodwater separation characteristics.Specifically designed for formulating rust preventive fluids for use inharsh environments, such as salt fog exposure. Also recommended forhigh humidity and normal indoor storage.Excellent solubility in a wide range of diluents. Effective in salt andhumidity tests at low treat levels. Not recommended if watercontamination will occur before application on metals.NA-SUL CA-1082Liquid(1.4%)Excellent for long term warehouse storage. Best in Group I paraffinic ornaphthenic oils. Good water separation character. Avoid contaminationwith strong alkaline materials.Film CharacteristicsThese additives should be used with 10% to 30% mineral oil in oil/solvent formulations forbest corrosion protection. This results in thin, slightly oily coatings. If oil is not used withsolvent, these additives may produce a slightly tacky coating particularly at higher additivelevels. ,NA-SUL CA/W1213, CA/W1177, and CA/W1146 will be almost dry at low treatlevels.

Selection Guide - NA-SUL Additives forOil/Solvent Based Rust PreventivesThere are many rust preventive additives available from King Industries that are used for formulatingoil or oil/solvent based rust preventives. The following selection guide is designed to help chosefrom among them based on specific performance requirements. Multiple requirements can bedetermined using the respective scales (0 to 4) to optimize formulations.RequirementSolubility (Oil)Tolerance of fluidto water exposure(Dewatering)Ease of useIndoor storageOutdoor shelteredstorageMarineenvironment0NotRecommendedCA/W11461 2 3 4HighlyRecommendedCA-HT3CA-1089Acid atmosphere CA-1089 CA-HT3CA/W1146CA/W1177CA/W1213CA/W1146CA/W1177CA/W1213CA-HT3CA-HT3CA-1082CA/W1177CA-1183CA-1082CA/W1213CA-1183CA/W1146CA/W1213CA-HT3CA/W1146CA-1089CA-1082CA-1082CA/W1177CA-1259CA-1259CA-1082CA-1089CA-HT3CA-1183CA-1089CA/W1177CA-1183CA-1259CA-1089CA-1082CA-HT3CA-1259CA-1089CA-1082CA/W1177CA-1183CA-1259CA-1259CA-1183CA/W1177CA/W1146CA/W1213CA/W1146CA/W1213NA-SUL ® Rust & Corrosion InhibitorsTolerance tostrongly basicmaterialsCA/W1146CA-1082CA-HT3CA/W1213CA-1259CA-1089CA-1183Let King’s rust preventivelaboratory assist you indeveloping highperformance RP products.Call 203-866-5551or emaillad@kingindustries.comPages 27-28

Performance - NA-SUL CA-1259in Rust PreventivesNA-SUL ® Rust & Corrosion InhibitorsNA-SUL CA-1259 is a high performance liquid rust and corrosion inhibitor specifically designed forrust preventives and dewatering fluids. It offers excellent solubility in a wide range of mineral oils,esters, solvents, and vegetable oils with excellent rust protection as shown below. However, it isrecommended to verify the solubility in the base oils/fluids used and compatibility with otheradditives.NA-SUL CA-1259 contains a minimal amount of wax giving good barrier properties. It is less viscousthan many other additives of its type and often can be cold blended into oils.It has an exceptional ability to help separate water from oil and oil/solvent solutions making it verysuitable for dewatering fluid applications. In addition to its water displacement characteristics,NA-SUL CA-1259 resists gelling in the presence of bulk water making it ideal for high moistureapplications, such as rust preventives associated with wet parts. NA-SUL CA-1259 Salt Fog Performance in Oil Based Formulations on SteelSalt Fog(ASTM B 117)Average Hrs to Failure5.0% CA-125995.0% Group IISO VG 32 Oil28 (Polished)18 (Matte)10.0% CA-125990.0% Group IISO VG 32 Oil30 (Polished)50 (Matte)10.0% CA-125990.0% Group IIISO VG 22 Oil40 (Polished)32 (Matte)10.0% CA-125990.0% NaphthenicISO VG 46 Oil72 (Polished)60 (Matte) NA-SUL CA-1259 Salt Fog Performance in Oil/Solvent Formulations on SteelSalt Fog(ASTM B 117)Average Hrs to Failure5.0% CA-125920.0% Group IISO VG 32 Oil75.0% MS*85 (Polished)80 (Matte)5.0% CA-125920.0% Group IISO VG 32 Oil75.0% ISOPAR ® H**90 (Polished)110 (Matte)20.0% CA-125930.0% Group IISO VG 32 Oil50.0% ISOPAR ® H**105 (Polished)240 (Matte)10.0% CA-125920.0% Group IISO VG 32 Oil70.0% Exxsol ® D-40**90 (Polished)95 (Matte) NA-SUL CA-1259 Performance in Vegetable Oil Based Formulations on Steel2.0% CA-125998.0% Soy BaseFluid4.0% CA-125996.0% Soy BaseFluid10.0% CA-125990.0% Canola Oil15.0% CA-125930.0% Canola Oil55.0% MethylSoyateSalt Fog(ASTM B 117)Average Hrs to Failure10 (Polished)8 (Matte)14 (Polished)10 (Matte)20 (Polished)14 (Matte)22 (Polished)18 (Matte)*MS - Mineral Spirits, **ISOPAR ® H and Exxsol ® D-40 are registered trademarks of ExxonMobil.“Hrs to failure” is defined as rust more than 1.5 cm from the top panel edge or more than 0.5 cm from either side edge.

NA-SUL Additives PerformanceIn Oil Based Rust PreventivesThe following data show the relative performance of three widely used rust preventive additives fromKing Industries. NA-SUL CA-1089 is not as effective at preventing rust in salt environments asCA/W1177 or especially CA-1259. CA-1089 does have exceptional anti-staining properties, as shownon page 24. The data below show that the addition of a minor quantity of CA/W1177 significantlyboosts salt fog performance. This combination even approaches the performance of CA-1259 onsome surfaces while maintaining the outstanding anti-staining properties of CA-1089. NA-SUL RP Additives In Oil Based SystemsTestsTests5% CA-108995% Naph Oil*10% CA-108990% Naph Oil5% CA/W117795% Naph Oil10% CA/W117790% Naph Oil4% CA-10891% CA/W117795% Naph Oil8% CA-10892% CA/W117790% Naph Oil5% CA-125995% Naph OilAverage Film ThicknessMeasured by Weight (μm) 2.0 2.1 2.6 1.5Salt Fog (ASTM B 117)Average Hours to Failure(P) (M) (SB)8 6 20Photo 1 - 50 Hours Salt Fog Exposure10% NA-SUL CA-1259, 90% Naphthenic Oil(P) Polished (M) Matte (SB) Sand Blasted(P) (M) (SB)32 20 16(P) (M) (SB)14 10 36(P) (M) (SB)30 30 72Photo 2 - 50 Hours Salt Fog Exposure10% NA-SUL CA/W1177, 90% Naphthenic Oil(P) Polished (M) Matte (SB) Sand Blasted10% CA-125990% Naph OilNA-SUL ® Rust & Corrosion InhibitorsAverage Film ThicknessMeasured by Weight (μm) 2.6 2.8 3.3 1.9Salt Fog (ASTM B 117)Average Hours to Failure(P) (M) (SB)14 8 28(P) (M) (SB)44 30 50(P) (M) (SB)24 16 72(P) (M) (SB)72 48 80* 200 SUS Naphthenic Oil(P) = polished surface (M) = matte surface (SB) = sand blasted surface“Hours to failure” is defined as rust more than 1.5 cm from the top panel edge or more than 0.5 cm from either side edge.Pages 29-30

NA-SUL AqueousRust & Corrosion InhibitorsNA-SUL ® Rust & Corrosion InhibitorsNA-SUL rust inhibitors for aqueous applications contain ingredients that allow the hydrophobicdinonylnaphthalenesulfonate molecule to be used in water systems. Depending on the additivechosen, the result is either a clear solution or an emulsion. These formulations can often achieveresults similar to oil or solvent based systems.ProductAmine/Metal DNNSSaltAppearanceNA-SUL TEA/LB Triethanolamine Stable dispersionNA-SUL 437NA-SUL 1019ATriethanolamine/diethylethanolamineTriethanolamine/diethylethanolamineClear solutionClear solutionNA-SUL 420 Sodium EmulsionKX450 Calcium Dark Brown LiquidRequirementWater SolubleSystemsWaterEmulsifiable0NotRecommended420KX450DescriptionGood coupling agent. Short to medium termindoor storage. Building block for waterbased corrosion inhibitors. Easy to use.Short to long term indoor storage. Aerosolcan protection. Easy to use. Hard watertolerant.Improved iron chip test results. Short to longterm indoor storage. Hard water tolerant.General purpose aqueous rust preventive.Easy to use. Medium to long term indoorstorage. Short term outdoor shelteredstorage.Liquid rust preventive concentrate that easilyforms stable emulsions when added to waterwith moderate stirring. Excellent rust protectionfor steel parts during storage and transportation.Selection Guide - Aqueous Corrosion Inhibitors1 2 3 4HighlyRecommended4371019A4371019A420KX450Ease of Use420, 4371019AKX450Indoor Storage4371019AKX450420MarineEnvironment4371019A420KX450Aerosol CansProtection420KX4504371019AStacking WetParts420437KX4501019A

K-CORR ® NF SeriesYellow Metal DeactivatorsK-CORR NF-200 is a premium ashless liquid yellow metal deactivator for industrial and automotive lubricants,greases, and rust preventive fluids. It complies with FDA 21 CFR 178.3570 standards and is NSF HX-1registered.K-CORR NF-410 is a multifunctional additive that provides extreme pressure properties in addition to yellowmetal protection. It can be used with K-CORR NF-200 to achieve higher levels of non-ferrous metal protection.TestProduct Composition DescriptionK-CORR NF-200K-CORR NF-410ADVANTAGES:Base OilProprietary HeterocyclicDerivativeSulfur & NitrogenChemistryExcellent thermal and hydrolytic stabilityGood demulsificationOutstanding solubility in mineral oil and syntheticbase stocksGood compatibility with other additivesLow viscosityEnhanced oxidation stabilityK-CORR NF-200 is used in all types of lubricants and greases wherecopper and copper-alloy machine parts need to be protected fromcorrosion.The table below shows the ability of K-CORR NF-200 to protect copperagainst the corrosive effects of active sulfur. The incorporation of activesulfur into an ISO VG 32 oil results in severe corrosion of the copperstrips in the ASTM D 130 test. Addition of a low treat level of K-CORRNF-200 offsets the detrimental effects of the active sulfur.No AdditiveISO VG 32*+ 50 ppm Sulfur**Premium ashless liquid yellow metal deactivator forindustrial and automotive lubricants, greases, and rustpreventive fluids. HX-1 registered - # 141124.Premium ashless liquid multifunctional additive providingextreme pressure and yellow metal protecting properties byscavenging active sulfur.0.05%K-CORR NF-200ISO VG 32+ 50 ppm SulfurNo AdditiveISO VG 32+ 100 ppm Sulfur1a4aASTM D 130Copper0.05%K-CORR NF-200ISO VG 32+ 100 ppm SulfurK-CORR ® NF Series - Yellow Metal DeactivatorsCopper Corrosion(ASTM D 130, DIN 51 759)3 hours, 100°C3 hours, 135°C3a4a1a1b4a4c1b1b* Solvent refined paraffinic Group I oil, ** Elemental sulfurAdditional formulations containing K-CORR NF-200 and K-CORR NF-410 can be found on pages11, 13, 34, 35, 36, 37, 40 and 50 of this product guide.Pages 31-32

O OHO R NOOR''OR''K-CORR ® 100 SeriesAshless Rust InhibitorsR'OK-CORR ® Ashless Rust & Corrosion InhibitorsThe K-CORR 100 Series is based on a unique amino acid derivative and is effective in a broadrange of industrial lubricants and functional fluids. In addition to excellent rust protection at lowadditive levels, the K-CORR 100 inhibitors offer a variety of performance advantages in specificsystems, including:Neutral behavior in FZG testingExcellent thermal stabilityGood hydrolytic stabilityGood demulsibility and water separationAntiwear synergism with selected EP/AW additivesEnhanced oxidation stabilityProductChemical BasisAcid Value(mg KOH/g)DescriptionK-CORR 100 Amino Acid Derivative ~105 Ashless rust inhibitor and intermediateK-CORR 100A2K-CORR 1031Amino Acid Derivativewith AmineAmino Acid Derivativewith Amine~80Ashless rust inhibitor with improvedsolubility~95 Premium ashless rust inhibitorImproving Antiwear Performanceof Extreme Pressure Agents with K-CORR 100 Series ProductsAntiwear agents and rust inhibitors compete for sites on the substrate and typically are antagonistictowards each other. The K-CORR 100 Series rust inhibitors are unique because they aresynergistic with a variety of EP/AW agents including phosphate esters, sulfurized olefins, triphenylphosphorothionate (TPPT), and ashless dialkyldithiocarbamates.Scar Diameter: Four Ball Wear (ASTM D 4172) 1 hour, 75ºC, 40 kgf, 1200 rpm0.90.80.70.60.50.40.30.2WithoutK-CORR 1031With 0.25%K-CORR 10310.10Paraffinic Base OilISO VG 320.75% TPPT 1.00% PhosphateEster1.00% SulfurizedOlefin

K-CORR 1031 andNA-LUBE ADTC SynergyC 4 H 9 SN CC 4 H 9 S CH 2SCSNA-LUBE ADTCNC 4 H 9C 4 H 9At various additive treat levels in an ISO VG 32paraffinic oil, K-CORR 1031 improves the lowload antiwear performance of an additive normallychosen for high load extreme pressure effectiveness.The graph to the right shows an example of theantiwear synergism of K-CORR 1031 with theextreme pressure agent NA-LUBE ADTC (anashless dialkyldithiocarbamate).K-CORR 1031 Industrial Lubricant PerformanceTestsBase Oil0.35% K-CORR NF-410 0.35% K-CORR NF-4100.06% K-CORR 1031ParaffinicISO VG 32ParaffinicISO VG 320.35% K-CORR NF-4100.25% K-CORR 1031ParaffinicISO VG 32Steel Corrosion(ASTM D 665, DIN 51 585) A & B Fail Pass PassDemulsibility(ASTM D 1401, DIN 51 599)Oil-Water-EmulsionSeparation Time (minutes)Copper Corrosion(ASTM D 130, DIN 51 759)3 hours, 100°C24 hours, 100°C3 hours, 135°C42-38-0101a1a1aASTM D 4172 Four Ball Wear Test1 hour, 75°C, 40 kgf, 1200 rpm43-37-015FZG A/8.3/90 (DIN 51 354 Part 2)Damage Load Stage 9 9 91b1b1b41-39-015Four Ball Wear (ASTM D 4172)1 hour, 75°C, 40 kgf, 1200 rpmScar Diameter (mm) 0.75 0.76 0.610.80.60.40.20Without K-CORRWith 0.25% K-CORR 10310.0 0.5 1.0 1.5 2.0Weight % NA- LUBE ADTCK-CORR 1031 imparts outstanding steel corrosion protection and demulsibility to formulated fluids.The table below shows the typical performance of K-CORR 1031 in an oil containing a dimercaptothiadiazolederivative.Average Scar Diameter1a1a1aK-CORR ® Ashless Rust & Corrosion InhibitorsK-CORR 1031 at 0.06% in this base oil passes the standard steel corrosion tests without detractingfrom other test requirements. At an increased level of 0.25% K-CORR 1031, improvement in theFour Ball Wear performance, similar to that shown on the previous page, is demonstrated.Additive CompatibilityA concern exists regarding the compatibility of ashless and metal-containing (primarily zinc)lubricants and functional fluids. Formulations containing K-CORR 100 Series rust inhibitors,particularly K-CORR 1031, are tolerant of contamination with zinc dithiophosphate-based fluids.Studies showing this behavior are available.Pages 33-34

K-CORR ® G SeriesRust Inhibitors for GreasesK-CORR ® G Series - Rust Inhibitors for GreaseThe K-CORR G Series was specifically designed for greases subjected to severe conditions.K-CORR G-1086A and K-CORR G-1270 are zinc-based. K-CORR G-1107 is ashless. All areformulated to enhance EP/AW properties and to minimize adverse effects on other greaseproperties, including water washout, water spray-off, penetration, and dropping point.PRODUCT Metal Content AttributesK-CORR G-1086A Zinc (9%) Antiwear synergist with first intention EP/AW additivesK-CORR G-1107 None - Ashless Metal free rust preventive with excellent antiwear propertiesK-CORR G-1270 Zinc (16.8%) Especially suitable to fulfill severe rust requirements K-CORR G-1086A PerformanceTestsWithoutAdditive1%G-1086AWithoutAdditive3%G-1086AWithoutAdditiveBase Grease Lithium 12-hydroxystearate (NLGI Number 2)Test Water 5% Synthetic Sea Water 100% Synthetic Sea WaterStatic Rust Test(ASTM D 5969) Fail Pass Fail Pass Fail3%G-1086A3% NaCI SolutionBorderlineFail4%G-1086AEMCOR Rust Test(ASTM D 6138, IP 220) 3,3 0,0 4,4 0,0 4,5 1,2 0,0 K-CORR G-1086A Performance - Three Week EMCORK-CORR G-1086A is also able to meet new and aggressive industry targets for grease performance.One such target requires a grease to provide “1” maximum EMCOR ratings (almost rust-free races)after a three-week EMCOR test. K-CORR G-1086A can provide rust-free results using the threeweek EMCOR test and 100% synthetic sea water.Tests4% K-CORR G-1086A4% K-CORR G-1086A2% NA-LUBE EP-52104% NA-LUBE ADTC0.05% K-CORR NF-200Base Grease Lithium 12-hydroxystearate (NLGI Number 2)Test Water100% Synthetic Sea WaterThree Week EMCOR Rust Test(ASTM D 6138, IP 220 - Modified) 0 0 K-CORR G-1107 PerformancePassTestsWithoutAdditive1%G-1107WithoutAdditive3%G-11075%G-1107Base Grease Lithium 12-hydroxystearate (NLGI Number 2)Test Water 5% Synthetic Sea Water 100% Synthetic Sea WaterStatic Rust Test(ASTM D 5969) Fail Pass Fail PassEMCOR Rust Test(ASTM D 6138, IP 220) 3,3 0,0 4,4 2,2Pass0,0

K-CORR ® G SeriesAntiwear Performance K-CORR G-1107 Performance ContinuedSince greases have performance requirements other than just rust protection, it is important toconsider the effects of rust inhibitors on different types of additives and on other grease properties.In addition to imparting excellent rust protection, K-CORR G-1107 also imparts excellent antiwearperformance.TestsBase Grease3.0%K-CORR G-11071.0% NA-LUBE ADTC3.0% Zinc Phosphate0.05% K-CORR NF-2001.0% NA-LUBE ADTC3.0% Zinc Phosphate0.05% K-CORR NF-2003.0% K-CORR G-1107EMCOR Rust Test(ASTM D 6138, IP 220)5% Synthetic Sea Water 0,0 2,2 0,0Four Ball Wear(ASTM D 2266)1 hour, 75ºC, 40 kgf, 1200 rpmScar Diameter (mm) 0.42 0.52 0.40Four Ball Weld Load(ASTM D 2596)10 seconds, 25ºC, 1800 rpmOK Load (kgf)Weld Load (kgf)140160Lithium 12-hydroxystearate (NLGI Number 2) K-CORR G-1270 Performance In 5% & 100% Synthetic Sea WaterTestsWithoutAdditive1%G-1270140160WithoutAdditiveBase Grease Lithium 12-hydroxystearate (NLGI Number 2)1401603%G-1270Test Water 5% Synthetic Sea Water 100% Synthetic Sea WaterStatic Rust Test(ASTM D 5969) Fail Pass Fail PassEMCOR Rust Test(ASTM D 6138, IP 220) 3,3 0,0 4,4 2,2K-CORR ® ZN-510K-CORR ® G Series - Rust Inhibitors for GreaseK-CORR ZN-510 is a zinc naphthenate rust inhibitor for industrial and automotive greases. Effectiveat low treat levels, K-CORR ZN-510 has excellent solubility in mineral oils, synthetic oils andgreases.PRODUCT Metal Content AttributesK-CORR ZN-510 Zinc (10%) Highly effective rust inhibitor for grease.Pages 35-36

K-CORR ® SA-300Ashless Rust InhibitorK-CORR ® SA-300 - Ashless Rust InhibitorK-CORR SA-300 is an ashless rust inhibitor based upon organic acid/ester chemistry. The additiveis highly efficient and may be used at treat levels as low as 0.03% to pass the ASTM D 665B test inR&O circulating oils and HF-2 hydraulic oils. In addition, it is recommended for formulating highperformance ashless steam turbine oils, paper machine oils, industrial and automotive gear oils,greases, and rust preventive fluids.Advantages:AshlessOutstanding rust and corrosion protectionExcellent demulsificationGood thermal and hydrolytic stabilitySoluble in highly paraffinic and synthetic base oilsEffective at very low treat levelsExcellent compatibility with all types of conventional functional additivesThe following table shows that the addition of a low treat level of K-CORR SA-300 imparts excellentsteel corrosion protection to an oil already containing antioxidants. In addition, K-CORR SA-300exhibits no adverse effects on other performance tests including copper corrosion, demulsibility, androtating pressure vessel oxidation. Further addition of a low treat level of an ashless yellow metaldeactivator to the formulation significantly increases the oxidation resistance of the oil as indicatedby rotating pressure vessel oxidation testing.Tests0.125% NA-LUBE AO-1300.125% NA-LUBE AO-2420.125% NA-LUBE AO-1300.125% NA-LUBE AO-2420.070% K-CORR SA-300Base Oil ISO VG 46 (Group II ) *0.125% NA-LUBE AO-1300.125% NA-LUBE AO-2420.070% K-CORR SA-3000.050% K-CORR NF-200Steel Corrosion(ASTM D 665, DIN 51 585)A & B Fail Pass PassCopper Corrosion(ASTM D 130, DIN 51 759)3 hours, 100°C3 hours, 135°C1b1b1b1b1b1bDemulsibility(ASTM D 1401, DIN 51 599)Oil-Water-EmulsionSeparation Time (Minutes)40-40-0540-40-0540-40-05RPVOT(ASTM D 2272)Lifetime (Minutes) 218 222 463* Compared to solvent refined HVI oils, Group II oils are more difficult to inhibit because the natural antioxidants (sulfur, nitrogen,and oxygen-containing compounds) have been removed by the refining process. The current industry trend is towardsGroup II and Group III base oils.

King IndustriesNSF HX-1 Registered ProductsKing Industries now offers a number of high performance additives and base oils/base oil modifiersthat are NSF HX-1 registered for use in lubricants with incidental food contact. Complying with FDACFR 178.3570, these specialty products include:NA-LUBE ® KR-006FG, KR-015FG, and KR-029FG are unique alkylated aromatic base oils withgood solubility and exceptional hydrolytic and thermo-oxidative stability.NA-LUBE ® AW-6400FG is a high performance, multi-functional additive that offersanticorrosion, antiwear and extreme pressure properties.NA-LUBE ® AO-142 is a liquid, easy to handle, diphenylamine antioxidant.K-CORR ® NF-200 is an ashless, yellow metal deactivator/corrosion inhibitor.NA-SUL ® CA-770FG is a premium rust inhibitor that provides excellent demulsibility andfilterability and is compatible with a wide range of additives and base stocks.PRODUCTChemicalCompositionViscosity @ 40°CASTM D 445DIN 51 550SYNTHETIC BASE OILS & BASE OIL MODIFIERSNA-LUBEKR-006FGNA-LUBEKR-015FGNA-LUBEKR-029FGProprietaryAlkylatedAromaticProprietaryAlkylatedAromaticProprietaryAlkylatedAromaticHIGH PERFORMANCE ADDITIVESLiquid Rust Preventive/DemulsifierNA-SULCA-770FGNeutral CalciumSulfonate in PAO36 mm 2 /s (cSt)124 mm 2 /s (cSt)174 mm 2 /s (cSt)214 mm 2 /s (cSt)Density @ 25°CASTM D 40520.90 g/ml7.5 lbs/gal0.884 g/ml7.40 lbs/gal0.875 g/ml7.29 lbs/gal0.91 g/ml7.6 lbs/galLiquid Multifunctional Additive (Anticorrosion, Antiwear & Extreme Pressure)Misc.Pour PointASTM D 97-33ºCPour PointASTM D 97-47 °CPour PointASTM D 97-26°CFlash Point,COCASTM D 92DIN 51376165ºCMaximumAllowableTreat LevelNSF HX-1Registration #100%* 143717100%* 140436100%* 14122010% byweight143718NSF HX-1 Registered ProductsNA-LUBEAW-6400FGAmine Salts ofAliphatic PhosphoricAcid Esters1400 mm 2 /s (cSt)0.97 g/ml8.06 lbs/galContentNitrogen2.4%Phosphorus8.3%0.5% byweight141635Liquid Diphenylamine AntioxidantNA-LUBEAO-142Butylated,OctylatedDiphenylamine280 mm 2 /s (cSt)0.98 g/ml8.20 lbs/galContentNitrogen4.5%0.5% byweight140584Liquid Yellow Metal Deactivator/Corrosion InhibitorK-CORRNF-200ProprietaryHeterocyclicDerivative78 mm 2 /s (cSt)0.95 g/ml7.90 lbs/galFlash Point,COCASTM D 92DIN 51376170°C0.1% byweight141124Pages 37-38* Not to exceed minimum amount required to achieve desired technical effect

PerformanceKing HX-1 Registered ProductsSynthetic Base Oils - NA-LUBE ® KR-006FG, KR-015FG & KR-029FGNSF HX-1 Registered ProductsThese unique synthetic base oils are used to formulate high performance lubricants and greases.They offer outstanding solubility and excellent hydrolytic and thermo-oxidative stability. The threecharts below demonstrate NA-LUBE KR-015FG’s superior thermo-oxidative stability over othercommonly used NSF HX-1 oils when tested in RPVOT, PDSC and Cincinnati Milacron ThermalOxidative Stability Tests at equivalent viscosities.Though not shown below, NA-LUBE KR-006FG and KR-029FG offer similar performance andadvantages over the other NSF HX-1 oils tested.Thermo-Oxidative Stability Comparison (NA-LUBE KR-015FG to Other NSF HX-1 Oils)The oils tested below were chosen for having equal viscosities to NA-LUBE KR-015FG and are asfollows.Base Oil PAO PAG White Oil KR-015FGViscosity @ 40°C 124 cSt 120 cSt 124 cSt 122 cStRPVOT - ASTM D 2272Rotating Pressurized Vessel Oxidation TestBASE FLUID PAO* PAGWhite Oil KR-015FGInduction Time(Minutes) Neat 55 1531 92Induction Time(Minutes) with 0.2% NA-LUBE AO-142 266 40141 443PDSC - ASTM D 3895Pressure Differential Scanning CalorimetryBASE FLUID PAO PAG White Oil KR-015FGInduction Time(Minutes) @ 200˚C3.6 2.1 3.7 20.0Heat Flow(W/g) Peak 62 390 155 1.5MODIFIED CINCINNATI MILACRON TESTCincinnati Milacron Thermal Stability Test Modified to higher temperatures (200°C, 225°C)Conditions Neat Fluid @ 200°CNeat Fluid @ 225°CBASE FLUIDTotal Sludge(mg/100ml)% ViscosityIncreaseTotal Sludge(mg/100ml)% ViscosityIncreaseNA-LUBE KR-015FG 2.85 8.36 19.98 20.32PAO(PAO viscosity of 124 cSt @ 40°C) 2.15 100.67 13.65 332.75

PerformanceKing HX-1 Registered Products NA-LUBE AW-6400FG PerformanceNA-LUBE AW-6400FG is an ashless, HX-1 approved, multi-functional additive that offers anticorrosion,antiwear and EP properties. As shown, NA-LUBE AW-6400FG is effective in a variety of H-1approved base oils.TestsHX-1 Approved Base Oil0.50%AW-6400FGPAO 100.50%AW-6400FGWhite Oil0.50%AW-6400FGNA-LUBEKR-029FG0.50%AW-6400FGViscosity @ 40°C 96 cSt 110 cSt 177 cSt 220 cStSteel Corrosion (ASTM D 665, DIN 51 585) A & B Pass Pass Pass PassDemulsibility (ASTM D 1401, DIN 51 599)Oil-Water-EmulsionSeparation Time (Minutes)Copper Corrosion (ASTM D 130, DIN 51 759)3 hours, 100°C24 hours, 100°CFour Ball Wear (ASTM D 4172)1 hour, 75°C, 1200 rpm, 30 kgf, Scar Diameter (mm)1 hour, 75°C, 1200 rpm, 40 kgf, Scar Diameter (mm)Four Ball Weld (ASTM D 2783)10 seconds, 25°C, 1800 rpmOK Load (kgf)Weld Load (kgf)Ashless Additives - NA-LUBE ®41-39-0101a1b0.380.4816018043-37-0151a1b0.370.51140160AO-142 & K-CORR NF-20039-41-0341a1b0.380.40140160Ester14-12-6430K-CORR NF-200 is a HX-1 food grade approved yellow metal deactivator that protects copper andcopper alloys against corrosion initiated by active sulfur. K-CORR NF-200 also enhances theoxidation stability of food grade lubricants and greases when used in combination with HX-1 foodgrade approved NA-LUBE ® AO-142 and an ashless dithiocarbamate.1a1b0.400.41140160NSF HX-1 Registered ProductsK-CORR NF-200 is recommended for formulating high performance food grade circulating andsteam turbine oils, hydraulic oils, vacuum oils, and industrial gear oils, as well as greases.TestsBase OilFORMULATIONCopper Corrosion(ASTM D 130, DIN 51 579)3 hours, 100° C24 hours, 100° CDemulsibility(ASTM D 1401, DIN 51 599)Oil-Water-EmulsionTime (Minutes)0.20%NA-LUBE AO-1421a2a40-40-0150.20% NA-LUBE AO-1420.50% Ashless DithiocarbamateISO VG 110 - White Oil1b3b40-36-4300.20% NA-LUBE AO-1420.50% Ashless Dithiocarbamate0.05% K-CORR NF-2001a1b40-40-015RPVOT(ASTM D 2272)Lifetime (Minutes) 141 2670 3735Pages 39-40

Additive Packagesfor Industrial Oils and GreasesMany of the NA-SUL ® , NA-LUBE ® and K-CORR ® additives are multifunctional. Ongoing additivetechnical service and the continued study of interactions, both positive and negative, lead to thedevelopment of packages that incorporates the desirable features into one blend. The packagesbelow are the results of projects targeted at specialty requirements and are generally available inlieu of additive component formulating.Additive Packages - BlendsPRODUCTNA-LUBEBL-1208NA-LUBEBL-1232 EL(Eco-Label)NA-LUBEAW-6310DESCRIPTIONAshless AW R&O package for industrial oils withoutstanding antioxidant performance in RPVOT(ASTM D 2272) and TOST (ASTM D 943) at lessthan 1.0% treat level. Test results are available inGroup I, II, III, IV (PAO) and canola oils.Environmentally friendly multifunctional ashlesshydraulic oil package specifically designed forester based functional fluids. The focus ofNA-LUBE BL-1232 EL is DIN ISO 15360:2004-05.Typical use is 1.8%. The incorporation of BL-1232EL into the formulation does not require any additionalregulatory labeling and holds the distinctionas the first additive package in compliance with theEuropean Ecolabel criteria for lubricants.Multifunctional package for AW and rust protection.Adding 0.1% AW-6310 to 0.7% BL-1208 willimprove FZG performance from ~9 to >12 damageload stages. The addition of 0.3% AW-6310 to0.7% BL-1208 will produce a mild EP industrialgear oil in the appropriate base fluid.Typical Properties - NA-LUBE BL SeriesTECHNICALREPORTSBL-12081. In Ashless IndustrialR&O Oils2. In Canola Oil3. In Group III Oils(Modified with NA-LUBE ® KR)BL-1232 EL1. In Saturated Esters2. Extended SealCompatibility3. Saturated vs.Unsaturated EstersPlease request ourNA-LUBE BL-1232 ELflyer for details of its use.NA-LUBE AW-6310Multifunctional AshlessLubricant AdditiveSee page 11 forperformance detailsTYPICAL PROPERTIESAppearanceNA-LUBE BL-1208Clear amber,moderately viscous liquidSulfur Content 7.0%Nitrogen Content 3.5%Phosphorus Content 0.2%Viscosity @ 40°C132 mm 2 /s (cSt)ASTM D 445, DIN 51 550Viscosity @ 100° C9 mm 2 /s (cSt)ASTM D 445, DIN 51 550Density @ 25°C0.976 g/mlASTM D 4052Weight per Gallon @ 25°C 8.1 lbs.Flash Point, COC140°CASTM D 92, DIN 51376NOTE: The above data are not specifications.NA-LUBE BL-1232 ELClear amber,Slightly viscous liquid8.2%2.7%0.9%180 mm 2/ /s (cSt)11 mm 2/ /s (cSt)0.990 g/ml8.2 lbs.170°C

NA-LUBE BL-1208 Performance - Group I, II, III & IV OilsThe table on this page and the following page demonstrate the performance of NA-LUBEBL-1208 at 0.7 % in typical Group I, II, III and IV base oils. Most of the test results aresimilar across the four oils except oxidation stability, which increases with the degree ofrefinement of the base oils.Base Oil ISO VG 46 ISO VG 46 ISO VG 46 PAO 6 cSt Most SevereTestsGroup I Group II Group III Group IV SpecificationTreat Level of NA-LUBE BL-1208, % 0.70 0.70 0.70 0.70Steel Corrosion (ASTM D 665)Siemens TLVProcedure B Pass Pass Pass Pass PassCopper Corrosion (ASTM D 130)GEK ISO/DP3 hours, 100°C 1b 1b 1b 1b 1b max.24 hours, 100°C 3a 3a 2a 3aDemulsibility (ASTM D 1401) @ 54ºCSiemens TLVOil-Water-Emulsion, ml 42-38-0 41-39-0 41-39-0 41-39-0 40-40-0 min.Time, minutes 20 15 25 15 20 max.FZG A/8.3/90(ASTM D 5182, DIN 51 354 Part 2)*Damage Load Stage n/d 9 n/d n/dFour Ball Wear (ASTM D 4172)40 kgf, Ambient, 1 hour, 1,200 rpmScar Diameter (mm) 0.50 0.40 0.50 0.50Hydrolytic Stability (ASTM D 2619)Alstom HTGD9 min.Industry DesiredCopper Loss (mg/cm2) 0.00 0.00 0.01 0.02 0.2 max. (HF-0)TAN of Water Layer (mg KOH) 3.81 3.53 3.09 3.93 4 max. (HF-0)Copper Appearance (ASTM D 130) 2a 2b 2e 3a 3 max.Filtration, WetAFNOR E 68691, FI 1.14 1.35 1.10 1.03DIN ISO 13357-1, F I 86.7 90.5 85.4 82.6Air Release (ASTM D 3427)Brown BovenDIN BS 489Additive Packages - BlendsMinutes 4 4 4 4 5 max.CM Thermal Stability (ASTM D 2070)Cincinnati LambViscosity Change (%) 4.66 3.53 2.59 -2.11 5 max.Acid Number Change (mg KOH/g) 0.11 0.03 0.07 0.01 50 max.Condition of Steel/Copper Rod: Color 1.5/5 1.5/4 1.5/3 1.5/4Steel Rod Deposit / Metal Loss (mg) 0.9/0.0 1.0/0.1 0.7/0.5 0.4/0.0Copper Rod Deposit / Metal Loss (mg) 2.4/0.9 0.6/0.0 0.6/0.1 0.7/0.0Total Sludge (mg/100 ml) 32.25 22.30 23.55 28.5 25 max.Whatman Precipitate (mg/100 ml) 19.05 6.80 3.56 4.15Millipore Precipitate (mg/100 ml) 12.00 15.20 19.60 24.00RPVOT (ASTM D 2272) DIN 51515-2Lifetime, minutes 598 1536 1740 2207 800 min.* The FZG Gear Test performance was determined for the Group II oil. Experience suggests that the result will be similar for the other three oilsof the same viscosity. If increasing performance in the FZG Test is desired, addition of 0.1% of NA-LUBE ® AW-6310 is expected to increase thedamage load stage to >12.Pages 41-42Continued Next Page

NA-LUBE BL-1208 Performance - Group I, II, III & IV Oils ContinuedTestsBase OilISO VG 46Group IISO VG 46Group IIISO VG46Group IIIPAO 6 cStGroup IVMost SevereSpecificationRPVOT Modified (GEK-32568 A)GEKLifetime, minutes 587 1551 1704 2146Decrease compared to unmodified test, % -1.8 -2.2 -2.1 -2.8 -20 max.Turbine Oil Sludge (ASTM D 4310)Brown Bowen1000-hour sludge (g) 0.12 0.03 0.02 0.02 0.1 max.Additive Packages - BlendsCu in Oil / Water layers (ppm, X-ray) 0/0 0/0 0/0 0/0TOST (ASTM D 943)95ºC, O 2 , Fe and Cu Catalysts DIN 51515-2Hours to TAN 2 (mg KOH/g) 3600 >10000 >12000 >12000 300 min.Oxidation Stability (IP-280)Volatile Acid (mg KOH/g) 0.07 0.06 0.05 0.05Soluble Acid (mg KOH/g) 0.20 0.17 0.13 0.11Sludge (%) 0.098 0.044 0.050 0.037Total Oxidation Products (%) 0.19 0.118 0.11 0.09Formulating Industrial Gear Oils With NA-LUBE BL-1208The performance data that follow demonstrate how 0.3% NA-LUBE BL-1208 used with 1.1%of King’s KX1236, an ashless EP/AW booster, can be used to meet the requirements of theAGMA 9005-E02 Industrial Gear Oil Specification in both conventional and synthetic basestocks. (Note that the new AGMA specification requires a FZG result >12 load stages butdoes not include Timken, Four Ball Wear and Four Ball Weld performance, as previouslyrequired in the US Steel No. 224 specification that is shown for reference.)The data also show that 0.3% NA-LUBE AW-6310 can be added to an R&O oil containing0.7% NA-LUBE BL-1208 to meet the AGMA 9005-E02 Industrial Gear Oil Specification,however, this blend does not show as good EP performance as the NA-LUBE BL-1208/KX1236 blend, as noted using the Four Ball Weld test. NA-LUBE BL-1208 Performance In Industrial Gear OilsTESTSADDITIVESISO VG 2200.30% BL-12081.10% KX1236Mineral Oil0.30% BL-12081.10% KX123680% PAO 40 cSt10% PAO 8 cSt10% DIDA*0.70% BL-12080.30% AW-6310Mineral OilAGMA 9005-E02Industrial Gear Oil EPSpecificationMineral OilFour Ball Wear (ASTM D 4172)40 kgf, 1200 rpm, 75ºC, 1 hour (mm)40 kgf, 1800 rpm, 75ºC, 1 hour (mm)30 kgf, 1800 rpm, 75ºC, 1 hour (mm)20 kgf, 1800 rpm, 75ºC, 1 hour (mm)0.580.570.490.440.530.510.430.290.42------US Steel No. 2240.35 maxFour Ball Weld (ASTM D 2783)10 seconds, 1800 rpm, 25ºCOK Load (kgf)Weld Load (kgf)240260280300160180US Steel No. 224250 kgf min

TESTSADDITIVESISO VG 2200.30% BL-12081.10% KX1236Mineral Oil0.30% BL-12081.10% KX123680% PAO 40 cSt10% PAO 8 cSt10% DIDA*0.70% BL-12080.30% AW-6310Mineral OilAGMA 9005-E02Industrial Gear OilEP SpecificationMineral OilTimken (ASTM D 2782)OK Load (lbs)Total Weight Loss (ring+block, mg)607.5706.8----US Steel No. 22460 lbs minFZG (ASTM D 5182)A/8.3/90 >12 >12 >12 >12Copper Corrosion (ASTM D 130)3 hours, 100ºC24 hours, 100ºC1b1b1b2a1bDark 3a1b maxSteel Corrosion (ASTM D 665) B Pass, Pass Pass Pass, Pass PassDemulsibility (ASTM D 1401)180ºF Oil-Water-Emulsion (ml)Time (minutes)Demulsibility (ASTM D 2711)Amount of free water (ml)% water in oilAmount of emulsion (ml)40-37-320Proc. A Proc. B38 860.10 0.400.1 0.341-39-020Proc. B860.200.141-37-225Proc. A Proc. B38 870.50 0.400.6

NA-LUBE ® BL-1208 Performance In Canola OilNA-LUBE BL-1208 can be used to formulate general purpose turbine and circulating oilswhere an environmentally friendly fluid based on triglycerides (HETG) is desired. A treatlevel of 2.2% NA-LUBE BL-1208 can impart excellent Rust Protection, RPVOT OxidationStability, and improved Four Ball Wear performance to canola oil while imparting no orminimal effects to other performance tests. NA-LUBE BL-1208 Performance - Canola OilAdditive Packages - BlendsTestsCanola OilAloneWith2.2% NA-LUBE BL-1208Treat Level, % -- 2.2Base FluidSteel Corrosion (ASTM D 665)Agri-Pure ® 60 Canola OilProcedure B Fail PassRPVOT (ASTM D 2272)Lifetime, minutes 14 102Copper Corrosion (ASTM D 130)VDMA 24558 HETGRequirements3 hours, 100°C 1b 1b 2 max.24 hours, 100°C 1b 1bDemulsibility (ASTM D 1401) @ 54ºCOil-Water-Emulsion, ml 41-37-2 40-40-0Time, minutes 10 30FZG A/8.3/90 (ASTM D 5182, DIN 51 354 Part 2)Damage Load Stage -- >12Not required but good result is100 min.Not required but good resultsare40-40-0 min.30 max.Four Ball Wear (ASTM D 4172), 1200 rpm40 kgf, 75°C, 1hour, Scar Diameter (mm) 0.78 0.5230 kgf, 75°C, 1hour, Scar Diameter (mm) 0.70 0.44Hydrolytic Stability (ASTM D 2619)Copper Loss (mg/cm2) 0.055 0.014TAN of Water Layer (mg KOH) 3.1 4.9Copper Appearance (ASTM D 130) 1b 1bFoam Test (ASTM D 892)Sequence I, 25ºC 0-0 10-0 150-0 max.Sequence II, 93ºC 0-0 0-0 75-0 max.Sequence III, 25ºC 0-0 10-0 150-0 max.

NA-LUBE ® BL-1208 Performance In Soybean OilTesting was also conducted using a soybean oil. At a treat level of 1.8%, NA-LUBEBL-1208 again imparts excellent Rust Protection, RPVOT Oxidation Stability, and improvedFour Ball Wear performance while imparting no or minimal effects to other performancetests. NA-LUBE BL-1208 Performance - Soybean OilTestsSoybean OilAloneWith1.8% NA-LUBE BL-1208Treat Level, % -- 1.8Base FluidSteel Corrosion (ASTM D 665)Agri-Pure ® 82 Soybean OilProcedure B Fail PassRPVOT (ASTM D 2272)VDMA 24558 HETGRequirementsNot required but good result isLifetime, minutes 17 268 100 min.Copper Corrosion (ASTM D 130)3 hours, 100°C 1a 1a 2 max.24 hours, 100°C 1a 1bDemulsibility (ASTM D 1401) @ 54ºCOil-Water-Emulsion, ml 40-38-2 40-40-0Time, minutes 10 25Four Ball Wear (ASTM D 4172), 1200 rpm30 kgf, 75°C, 1 hour, Scar Diameter (mm) 0.58 0.4440 kgf, 75°C, 1 hour, Scar Diameter (mm) 0.62 0.50CM Thermal Stability (ASTM D 2070)Not required but good resultsare40-40-0 min.30 max.Additive Packages - BlendsViscosity Change (%) 8.5 5.5Acid Number Change (mg KOH/g) 0.35 0.54Condition of Steel Rod: Color 1 1Steel Rod Deposit/Metal Loss (mg) 0.9/0.9 1.0/0.8Condition of Copper Rod: Color 2 4Copper Rod Deposit/Metal Loss (mg) 0.6/0.4 1.3/1.6Total Sludge (mg/100ml) 6.5 7.6Whatman Precipitate (mg/100 ml) 0.8 1.7Millipore Precipitate (mg/100 ml) 5.2 4.8Foam Test (ASTM D 892)Sequence I, 25ºC 10ml-Trace Trace-0 150-0 max.Pages 45-46Sequence II, 93ºC 0-0 Trace-0 75-0 max.Sequence III, 25ºC Trace-0 Trace-0 150-0 max.

NEW NA-LUBE ® BL-1232 ELEnvironmentally Driven...Performance ProvenThroughout the world, environmentally friendly lubricants are beingdeveloped to replace older technologies that are non-renewable and arecontaminates when released into soil or water. Almost universally, thechallenge formulators face when developing these new, replacementproducts is maintaining or surpassing the performance characteristics ofthe original.Additive Packages - BlendsA particular area of focus for new greener lubricants has been hydraulicfluids, given their propensity to leak and the ensuing ground and watercontamination. Here too, the challenge has been finding additives andadditive packages that are eco-friendly and deliver the performanceneeded. In that regard King Industries is proud to introduce NA-LUBEBL-1232 EL, an ashless, multifunctional additive package specificallydesigned for use in ester based systems including hydraulic fluids.Additive Package NA-LUBE BL-1232 EL has been evaluated against thelatest European Ecolabel criteria for lubricants. Based on that evaluation,NA-LUBE BL-1232 EL, when used as a single additive, qualifies for usein a final product eligible for the European Eco-Label in a concentrationup to 1.8% by weight. NA-LUBE BL-1232 EL Performance With Saturated EstersBase Fluid Priolube 1973Saturated EsterTreat Level, % Neat With 1.8%BL-1232 ELSteel Corrosion(ASTM D 665)Procedure A (distilled H 2O)Procedure B (synthetic sea water)Demulsibility(ASTM D 1401) @ (54°C)Oil-Water-EmulsionTime (minutes)FailFail43-37-015PassPass40-40-015Radialube ® 7588Saturated EsterNeat With 1.8%BL-1232 ELFailFail43-37-025PassPassSpecificationDIN ISO 15380PassPass41-38-025 30FZG A/8.3/90(ASTM D 5182, DIN 51 354 Part 2)Damage Load Stage n/d >12 n/d 12 10 min.Four Ball Wear (ASTM D 4172)1 hour, 22°C, 15 kgf, 1500 rpm (mm)1 hour, 22°C, 30 kgf, 1500 rpm (mm)1 hour, 75°C, 40 kgf, 1500 rpm (mm)n/d0.490.570.48n/d0.540.590.40120 max.30 max.V 104C Vane Pump(DIN EN ISO 20 763)Reported Wear Loss Ring (mg)Wear Loss Vanes (mg)n/d 4.67.5n/dn/dCopper Corrosion (ASTM D 130)3 hours, 100°C 1b 1a 1b 1a 2 max.AFNOR FiltrationDry (E 68690) FI 1.05 1.04 1.09 1.08Wet (E 68691) FI 1.28 1.08 1.33 1.12Filterability Dry (DIN ISO 13357-2)F IF II99.598.995.487.799.196.396.984.880 min.60 min.Filterability Wet (DIN ISO 13357-2)F lF ll92.583.693.885.995.082.091.779.170 min.50 min.

Base Fluid Priolube 1973Saturated EsterTreat Level, % Neat With 1.8%BL-1232 ELHydrolytic Stability (ASTM D 2619)Copper Loss (mg/cm 2 )TAN of Water Layer (mg/KOH)Copper Appearance (ASTM D 130)0.051.21b0.012.93a0.051.51bRadialube ® 7588Saturated EsterNeat With 1.8%BL-1232 EL-0.032.92cSpecificationDIN ISO 15380RPVOT (ASTM D 2272)150°C, H 2O, O 2, Cu CatalystLifetime (minutes)

Over Seven Decades of Manufacturing ExperienceCoupled with a Commitment to Superior Technical ServiceKing Industries, Inc., a pioneer in the development of synthetic sulfonates, maintains state of the artmanufacturing facilities for a broad range of specialty chemical products. King is ISO 9001,ISO 14001 and ISO 18001 certified and controls all aspects of production, from raw materialsto custom finished products.Technical Service & Contact InfoIncorporating integrated manufacturing capabilities, from alkylation to sulfonation, neutralization topurification, we (King) have unique technologies and processes to work with you on your additiverequirements.Technical Service CapabilitiesTo develop today’s high performance industrial lubricants, greases, and rust preventives, extensivetesting and practical experience are required. We maintain a broad range of ASTM, DIN and IP testingcapabilities and equipment coupled with committed, experienced personnel to assist you in yourformulating endeavors. Our performance testing capabilities in our Technical Service Laboratoriesinclude:Rust ProtectionYellow Metal Corrosion ProtectionWear/Weld PerformanceOxidative StabilityThermal StabilityHydrolytic StabilityDemulsibilityFilterabilityCoefficient of Friction - (SRV)The technical service that we offer to existing and potential customers are an important part of ourbusiness. As an experienced lubricant additive supplier, our goal is to help customers fulfill theirneeds by designing specific technical solutions targeted towards their applications. By using thisapproach, we can help position our customers’ products in the current and future marketplaces.

King Global NetworkKing Industries is headquartered in Norwalk, CT, USA and maintains technical sales offices inWaddinxveen, The Netherlands and Zhongshan, China. A network of technical sales representativesand distributors serve King customers in virtually every industrialized country of the world.In addition to lubricant additives, King manufacturers and markets specialty products for the paintand coatings industry, electronics industry, rubber industry, inks, sealants and adhesives. Foradditional information on King products or our global network of technical sales representatives,please contact our primary offices as shown below.WORLD HEADQUARTERSKing Industries, Inc.1 Science Rd.Norwalk, CT 06852Phone: 203-866-5551Fax: 203-866-1268Email: LAD@kingindustries.comAdditional InformationASIA-PACIFIC OFFICESynlico Tech (Zhongshan) Co., Ltd.106 Chuangye Building, Kang Le Ave.Torch Development Zone,Zhongshan, ChinaPhone: 86 760 88229866Fax: 86 760 88229896Email: alex.he@kingindustries.comVisit us at: www.kingindustries.comEUROPEAN OFFICEKing Industries, InternationalNoordkade 642741 EZ WaddinxveenThe NetherlandsPhone: 31 182 631360Fax: 31 182 621002Email: dgartz@kingindustries.comDetailed product data sheets for each product and performance reports are available bycontacting the King offices as shown above or emailing; LAD@kingindustries.com.Technical Service & Contact InfoWarranty of InformationNA-SUL ® , NA-LUBE ® , and K-CORR ® are registered trademarks of King Industries, Inc.The results shown in this brochure reflect data generated by King Industries’ Technical Service Laboratories.Actual results may vary depending on the additive package, base oil, thickener system, and test equipmentdesign.The conditions of your use and application of our products, technical assistance and information (whether verbal, written or by way of productevaluations), including any suggested formulations and recommendations, are beyond our control. Therefore, it is imperative that you test ourproducts, technical assistance and information to determine to your own satisfaction whether they are suitable for your intended uses andapplications. Such testing has not necessarily been done by King Industries, Inc. (“King”). The facts, recommendations and suggestions hereinstated are believed to be reliable; however, no guaranty or warranty of their accuracy is made. EXCEPT AS STATED, THERE ARE NOWARRANTIES, EXPRESS OR IMPLIED, OF MERCHANTABILITY, FITNESS OR OTHERWISE. KING SHALL NOT BE HELD LIABLE FORSPECIAL, INCIDENTAL, CONSEQUENTIAL OR EXEMPLARY DAMAGES. Any statement inconsistent herewith is not authorized and shall notbind King. Nothing herein shall be construed as a recommendation to use any product(s) in conflict with patents covering any material or itsuse. No license is implied or granted under the claims of any patent. Sales or use of all products are pursuant to Standard Terms andConditions stated in King sales documents.Pages 49-50

King Industries, Inc.1 Science Rd.Norwalk, CT 06852Phone: 203-866-5551Fax: 203-866-1268Email: LAD@kingindustries.comLGB-32012