Waters 2414 Refractive Index Detector

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HPLC system, with the detector under Empower software control via theIEEE-488 bus interfaceIEEE-488 connector600 Series pumpEmpower datasystembusLAC/E orNetwork LAC/E cardIEEE-488 cable717plusautosampler2414 RIdetectorAlliance HPLC system, with the detector under Empower software controlvia the IEEE-488 bus interfaceIEEE-488 connectorbusLAC/E orNetwork LAC/E cardIEEE-488cableEmpower datasystemAllianceSeparationsModule2414 RI detectorWhen connected to a Waters data system, the 2414 detector is automaticallyconfigured to operate in 410 (remote) mode. You use the data control softwareto create instrument methods and method sets to control the detector andother HPLC system components. See Chapter 5, “Operating the Detector” andthe data control software documentation for more information on configuringthe detector and operating in 410 (remote) mode.3-6 Connecting Signal Cables
Connecting to a Waters PowerLine system controller via theIEEE-488 bus interfaceThe Waters PowerLine system controller is an IEEE-488 configuration inwhich the Alliance Separations Module or a 600-series solvent delivery systemoperates as the system controller for the HPLC system components, includingthe 2414 detector.To connect the detector to a Waters PowerLine system controller, use theIEEE-488 interface cables as shown in the figure below.Each fluid-handling unit is configured with either of the following injectors:• Integrated manual injector (built in as part of the drawer or shelf unit)• Externally connected manual injector or autosamplerWaters PowerLine system controller IEEE-488 connectionsIEEE-488cablePowerLineController (600-series solventdelivery system orAllianceSeparationsModule)717plusAutosampler2414 RI detectorRequirements:When an Alliance Separations Module using the IEEE-488 interface controlsthe detector, these conditions apply:• The detector is configured in 410 mode (a task you perform via thekeypad’s “Config” menu).IEEE-488 signal cable connections 3-7
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Waters 2414Refractive IndexDetector
Page 4: Customer commentsWaters’ Technica
Page 7: Operating this instrumentWhen opera
Page 10 and 11: Electronics........................
Page 12 and 13: Operating in 410 (standalone) mode
Page 14 and 15: xivTable of Contents
Page 16 and 17: Use of refractive index detectorsTh
Page 18 and 19: Effect of density on RIWeight perce
Page 20 and 21: θ 2 = Angle of refractionn 1 = RI
Page 22 and 23: External angle of deflectionThe amo
Page 24 and 25: By detecting how far the image shif
Page 26 and 27: • Single channel/additional chann
Page 28 and 29: • Enable keypad - You can program
Page 30 and 31: Flow path during analysisFlow cellE
Page 32 and 33: An icon in the front panel display
Page 34 and 35: Solenoid valveDuring normal operati
Page 36 and 37: Optics bench assembly light pathMir
Page 38 and 39: PolarityThe default time constant o
Page 40 and 41: 1-26 Introduction
Page 42 and 43: DimensionsThe following figure show
Page 44 and 45: Rear panelInputs andoutputsGroundte
Page 46 and 47: Tubing connectionsInlet lineSolenoi
Page 48 and 49: 2. Connect the tubing to the white
Page 50 and 51: Component connection overviewThe fo
Page 52 and 53: Ethernet signal cable connectionsYo
Page 56 and 57: • The detector automatically chan
Page 58 and 59: Connecting to a manual injectorIf y
Page 60 and 61: Waters 2414 analog-out/event-in con
Page 62 and 63: Generating a chart mark on injectin
Page 64 and 65: Connecting to the Waters 746 Data M
Page 66 and 67: Connecting to a data control system
Page 68 and 69: Each time the detector receives a s
Page 70 and 71: Inject start connections to a manua
Page 72 and 73: 3-24 Connecting Signal Cables
Page 74 and 75: Common solvent problemsThe 2414 det
Page 76 and 77: intend to use for your analysis has
Page 78 and 79: is endothermic, the solubility incr
Page 80 and 81: 4-8 Preparing Solvents
Page 82 and 83: Powering-onInitializingBefore you p
Page 84 and 85: • Navigation to specific screens
Page 86 and 87: Keypad description (Continued)KeyUn
Page 88 and 89: Keypad description (Continued)KeyUn
Page 90 and 91: • Press the corresponding number
Page 92 and 93: Mode, function, and message screen
Page 94 and 95: Secondary functions of the RIU mode
Page 96 and 97: • Voltage offset - Adjusts the ch
Page 98 and 99: Note: When the detector is operatin
Page 100 and 101: 10. Press HOME to return to the RIU
Page 102 and 103: 2. From the Method choice list, pre
Page 104 and 105:
• If you press Enter, the followi
Page 106 and 107:
Home screen 410 mode% Full scalePol
Page 108 and 109:
• Voltage offset• Enable/disabl
Page 110 and 111:
• Voltage offset - This parameter
Page 112 and 113:
Setting the IEEE addressIEEE addres
Page 114 and 115:
• Rectangular wave (in seconds) -
Page 116 and 117:
Effects of attenuation/sensitivity
Page 118 and 119:
When the Column Heater Module Tempe
Page 120 and 121:
2. Replace the 100% water mobile ph
Page 122 and 123:
Detector maintenance involves clean
Page 124 and 125:
9. Switch the pump or solvent deliv
Page 126 and 127:
6-6 Maintenance Procedures
Page 128 and 129:
Error messagesThe detector can disp
Page 130 and 131:
ubbles before you recycle power. If
Page 132 and 133:
Error messages preventing operation
Page 134 and 135:
The user-selectable sticky diagnost
Page 136 and 137:
Specifying fixed voltage outputFrom
Page 138 and 139:
Using the Other diagnostic function
Page 140 and 141:
TroubleshootingThis section provide
Page 142 and 143:
Chromatography troubleshootingThis
Page 144 and 145:
Abnormal baseline troubleshooting (
Page 146 and 147:
Abnormal baseline troubleshooting (
Page 148 and 149:
Use the following table to troubles
Page 150 and 151:
Use the following table to troubles
Page 152 and 153:
Incorrect results troubleshooting (
Page 154 and 155:
Warning symbolsWarning symbols aler
Page 156 and 157:
Chemical hazard warningThis warning
Page 158 and 159:
Warning: Use caution when working w
Page 160 and 161:
警告 : 当有压力的情
Page 162 and 163:
Warning: To protect against fire, r
Page 164 and 165:
Handling symbolsThese handling symb
Page 166 and 167:
Operational specifications (Continu
Page 168 and 169:
B-4 Specifications
Page 170 and 171:
connections, power. See powerconnec
Page 172 and 173:
integratoroutput 5-35signal 3-18Kke
Page 174 and 175:
shift icon 5-11, 5-26signal connect
Page 176:
Index-8
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Waters 2414 Refractive Index Detector

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