Synthesis, Characterization, and Gas Permeation Properties

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To Mom and Daddy, for their profound love and care. To Filza, Faiza and Awais, for their unflinching support and encouragement. To Irfan, for being there whenever I needed him, always.
Table of Contents General Introduction……………….…………………………………………............1 Chapter 1 Synthesis, Characterization, and Gas Permeation Properties of Silylated Derivatives of Ethyl Cellulose…………………………...31 Chapter 2 Synthesis, Characterization, and Gas Permeation Properties of Perfluoroacylated Ethyl Cellulose….………………………………51 Chapter 3 Synthesis and Properties of Amidoimide Dendrons and Dendronized Cellulose derivatives……………………………………………….75 Chapter 4 Synthesis, Characterization, and Gas Permeation Properties of t-Butylcarbamates of Cellulose Derivatives………………………111 Chapter 5 Synthesis and Properties of Amino Acid Esters of Hydroxypropyl Cellulose…………………………………………………………..135 List of Publications………………………….……………………………………...153 Acknowledgements…………………………………………………………………157
Page 1: Synthesis, Characterization, and Ga
Page 5 and 6: General Introduction cellulose deri
Page 7 and 8: General Introduction biogenetically
Page 9 and 10: General Introduction chemistry offe
Page 11 and 12: General Introduction solution-diffu
Page 13 and 14: General Introduction A simplified t
Page 15 and 16: General Introduction been observed
Page 17 and 18: polymers. 41,46 General Introductio
Page 19 and 20: General Introduction Keeping in vie
Page 21 and 22: General Introduction the derivatize
Page 23 and 24: General Introduction strategy (G1-a
Page 25 and 26: General Introduction In conclusion,
Page 27 and 28: General Introduction 5. (a) Kobayas
Page 29 and 30: General Introduction 15. (a) Goetma
Page 31 and 32: General Introduction American Chemi
Page 33 and 34: General Introduction Macromolecules
Page 35 and 36: Silylation of Ethyl Cellulose Intro
Page 37 and 38: Silylation of Ethyl Cellulose milli
Page 39 and 40: Silylation of Ethyl Cellulose chlor
Page 41 and 42: Silylation of Ethyl Cellulose Resul
Page 43 and 44: Silylation of Ethyl Cellulose Solub
Page 45 and 46: Silylation of Ethyl Cellulose 1.034
Page 47 and 48: Silylation of Ethyl Cellulose poly(
Page 49 and 50: Silylation of Ethyl Cellulose the r
Page 51 and 52: Silylation of Ethyl Cellulose D.; Y
Page 53 and 54:
Chapter 2 51 Chapter 2 Synthesis, C
Page 55 and 56:
53 Chapter 2 are few and far betwee
Page 57 and 58:
55 Chapter 2 constant volume/variab
Page 59 and 60:
57 Chapter 2 Membrane Density. Memb
Page 61 and 62:
59 Chapter 2 IR spectrum of 1 (Figu
Page 63 and 64:
61 Chapter 2 1,3-bis(trifluoromethy
Page 65 and 66:
63 Chapter 2 The increase in the po
Page 67 and 68:
65 Chapter 2 other fluorinated poly
Page 69 and 70:
67 Chapter 2 of the gas permeabilit
Page 71 and 72:
69 Chapter 2 Gas Diffusivity and So
Page 73 and 74:
71 Chapter 2 mobility of the perflu
Page 75 and 76:
73 Chapter 2 1325-1329. (b) Hamza,
Page 77 and 78:
Chapter 3 75 Chapter 3 Synthesis an
Page 79 and 80:
77 Chapter 3 cost, and above all ap
Page 81 and 82:
79 Chapter 3 molecular weights (Mn
Page 83 and 84:
81 Chapter 3 1.99-2.07 (m, 2H, (CH3
Page 85 and 86:
83 Chapter 3 25 °C, ppm): 11.9, 13
Page 87 and 88:
85 Chapter 3 38.1, 44.7, 46.8, 47.9
Page 89 and 90:
87 Chapter 3 CH2CH2C(=O)O), 2.50-4.
Page 91 and 92:
89 Chapter 3 1091, 1053, 853, 806,
Page 93 and 94:
91 Chapter 3 dendrons (G1-a-ІІ-G1
Page 95 and 96:
93 Chapter 3 (DMAP) as a base, as s
Page 97 and 98:
Figure 3. FTIR spectra of 1, 2c, an
Page 99 and 100:
97 Chapter 3 (partly soluble) and 3
Page 101 and 102:
99 Chapter 3 increased polarity of
Page 103 and 104:
101 Chapter 3 that of 1, and approx
Page 105 and 106:
103 Chapter 3 derivatization per th
Page 107 and 108:
105 Chapter 3 (2a-c) were in the or
Page 109 and 110:
107 Chapter 3 2709-2719. (b) Schenn
Page 111 and 112:
109 Chapter 3 17. van Krevelen, D.
Page 113 and 114:
Chapter 4 111 Chapter 4 Synthesis,
Page 115 and 116:
113 Chapter 4 Since, no significant
Page 117 and 118:
115 Chapter 4 Materials. Ethyl cell
Page 119 and 120:
DStotal = DSEt + DSCarb (for 1a and
Page 121 and 122:
119 Chapter 4 Figure 2. 1 H NMR spe
Page 123 and 124:
121 Chapter 4 ruling out the possib
Page 125 and 126:
123 Chapter 4 t-butyl moiety. A str
Page 127 and 128:
125 Chapter 4 reported to lead to t
Page 129 and 130:
127 Chapter 4 Table 4. Gas Permeabi
Page 131 and 132:
129 Chapter 4 augmentation in eithe
Page 133 and 134:
131 Chapter 4 indicate the signific
Page 135 and 136:
133 Chapter 4 M.-R. J. Appl. Polym.
Page 137 and 138:
Chapter 5 135 Chapter5 Synthesis an
Page 139 and 140:
137 Chapter5 acid- and peptide-cont
Page 141 and 142:
139 Chapter5 Specific rotations ([
Page 143 and 144:
141 Chapter5 1.66 (brs, 1.1H, NHCH(
Page 145 and 146:
143 Chapter5 as shown in Scheme 1,
Page 147 and 148:
145 Chapter5 in Table 1. The molecu
Page 149 and 150:
147 Chapter5 almost same pattern of
Page 151 and 152:
Conclusions Table 3. Thermal Proper
Page 153 and 154:
151 Chapter5 W.; Jing, X. J. Polym.
Page 155 and 156:
Chapter 5 Synthesis and Properties
Page 157 and 158:
Acknowledgments While submitting th
Page 159:
Synthesis, Characterization, and Ga
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Synthesis, Characterization, and Gas Permeation Properties

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