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34<br />
some of the zircons suffered Pb loss after crystallisation, what explains why data points<br />
plot below the concordia and the obtained minimum age of 216 ± 2.0 Ma. To evaluate<br />
the complexity of this sample, SHRIMP analyses were performed on 12 single zircon<br />
grains. Cathodoluminescence images show spectacular, multiple growth and<br />
resorption facets; inner grain portions are sometimes metamict (Appendix B, plate B2).<br />
No cores have been detected. At several grains core and rim portions were probed but<br />
yielded identical ages within error. One grain gave an imprecise Devonian age (~ 400<br />
Ma); the weighted mean of 14 spot ages, excluding the youngest grain (~ 189 Ma), is<br />
227 ± 4.1 Ma (Fig. 3.7c).<br />
P22: Two zircon fractions were analysed from this granite. Cathodoluminescence<br />
images (Appendix B, plates B1, B2) of zircons from this sample show grains with a fine<br />
magmatic zonation and often large cores, which show also magmatic zonation.<br />
Fraction 1 is long prismatic (150-250 �m), colourless and clear. The other fraction (F2) is<br />
prismatic and shorter (80-200 �m), also clear but more brownish. In the concordia<br />
diagram (Fig. 3.7b) one fraction (F2) lies above the concordia, whereas F1 has a<br />
concordant age of about 215 ± 1.5 Ma. Samples P22 and P26 were measured in two<br />
different laboratories but show both the phenomena of data points plotting above the<br />
concordia. The real reason is unclear, but it is most likely to result in similar Pb<br />
diffusion behavior. As all fractions plot on or near the concordia between 200-225 Ma,<br />
this age range is interpreted as minimum crystallisation time span for these batholiths.<br />
Central Pamirs/Muzkol dome<br />
P17: Two fractions were available for analyses from this granite (Fig. 3.7d). One<br />
fraction (D2) has very small (63-80 �m) zircon grains, the other fraction (DE2) has grains<br />
in the range of 80-125 �m. Assuming a simple crystallisation and recent partial Pb loss<br />
model for these two fractions the age interpretation is at 531 � 30 Ma. A better MSWDvalue<br />
can be obtained assuming a Pb loss around 41 Ma � 22 Ma with an upper<br />
interception age at 539 � 5 Ma. SHRIMP analyses of 14 grains aimed to probe possible<br />
Tertiary rims. The zircons are exceedingly complex internally and inclusion rich<br />
(Appendix B, plate B2). Spot ages range from 561 to 424 Ma; no younger rims have been<br />
detected. The weighted mean of 14 spot ages, excluding the youngest spot (~ 424 Ma),<br />
is 536 � 18 Ma (Fig. 3.7e).<br />
96M9a: Four fractions were extracted from this sample with big (around 200 �m),<br />
euhedral zircons. F1 comprises elongated, brownish-pink zircons, F2 consists of smaller<br />
clear and pinkish zircons, F4 has also pinkish medium sized zircons and F5 contains<br />
the largest yellow-brownish to pinkish and short prismatic zircons. Many of the zircons<br />
show optically dark inclusions. The cathodoluminescence images (Appendix B, plate<br />
B2) reveal mainly long prismatic grains with large, well rounded cores. The cores show<br />
oscillatory zoning and have embayments likely caused by resorption of inclusions in<br />
the igneous melt. Most of the zircons illustrate sector zoning along the prismatic long<br />
axis. Many of the grains are fractured but not broken. The four measured fractions are<br />
all discordant (Fig. 3.7f). Since F2 has a too low 206 Pb/ 204 Pb ratio (< 100), the fraction<br />
was excluded from the discordia calculation. The fractions F1, F3 and F5 show a linear