SON(rcHEMICAI, SYNIIIISIS AIID CIIARACTERIZATION OF PR.ECT ...

ABSTRACT
A sinlle &!d & efici€ sonochenical D.thod ha b€ln usd for ihc ay.rh6es of
Eiety of rcDon€d m.&l 9dildoMLs lil. M{@), (l-r), Mltld)" (tG[), bis
riph.nylpbGphin zinc (II) cblo.i.le zn (PPhr ) cL O7), N,N-dineliiyleamjd€ z.
(dma, (r8) sd new hct€rcI€plic adduci liLe [Cu(dre)(oAc)(H:o)lz (14).
ICuttErOH)' N- (oAc)l:l (23), Izn(!E\(au (t5) (wkE s = ctheolmmq
&3c = edyr@rooatc) IztrG@),(dmeH)l 06) (wh@ dlreH = NN-
dinethyldido.th6ol), t(znp,(dDa),(oAoel @0) (wher dna= N.N
dincthylaet$ide), [dr@)zdl. (21) tzd!@cxH,o]lcl (19), tNilGEA)rt,(oAc),1
(22), (qh* TEA= LidheddiE' &d OAc = &er.t ),. All th* @mpl*€s hav.
ben chdabnz.d by n,p,, CHNS-O, AAAS. FTI& NMR ud Singlc Cry$als Xdy
aralysis techniqu.s. 'ftmal behavioa ldn€ics, dd €volved gs padem of th€
ptFte6 und.r onaollcd 6vim@1 Bfr sndied by Tca/sDTA .nd TGA,FIIR
lehriqu€s. Bed on thmal dd €volvcd gs srudiB d a, m€cheism of rhemal
d€@nposition he ba wo*ed out. IFs ndly synthelied coDpt€x€s havc been usd
lor th€ falicllion of !u zio, Zlo troped witb s , Ztq &d mcr.Iic @ppq rhi!
fiLtrs @Dprilin8 of @oprnict* of si* tu8q Aon 20 to too M bt indiS@uty
d.v.loped ultasoDic a.resol aslisl.d ch€nical vapou d€penion CJAACVD) r€chnjqe.
Thc moryhology ad conposilion of thj! fitm w@ .mined by SEM. EDx ed
pow