FORENSIC TOXICOLOGY - Bio Medical Forensics

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Rajotte, James W. MSc*, Centre of Forensic Sciences, Northern Regional Laboratory, Suite 500, 70 Foster Drive, Sault Ste. Marie, Ontario P6A 6V3, Canada Ramsey, John MSc, TIC TAC Communications Ltd., St. Georges University of London, Cramner Terrace, London, SW17 0RE, UNITED KINGDOM; and Michael D. Osselton, and Eva M. Reichardt, MSc*, Bournemouth University, Talbot Campus, Fern Barrow, Poole, BH12 5BB, UNITED KINGDOM Rana, Sumandeep MS*, Wayne B. Ross, MCLS, and Victor P. Uralets, PhD, Redwood Toxicology Laboratory, 3650 Westwind Boulevard, Santa Rosa, CA 95403 Rana, Sumandeep MS, Cynthia Coulter, BS, Christine M. Moore, PhD*, Michael J. Vincent, MS, and James Soares, PhD, Immunalysis Corporation, 829 Towne Center Drive, Pomona, CA 91767 Rao, Ridhima D. BS*, Sam Houston State University, Box 2525, 1003 Bowers Boulevard, Huntsville, TX 77341, and Dan T. Anderson, MS, Los Angeles County, Department of Coroner, 1104 North Mission Road, Los Angeles, CA 90033 Raul, Jean-Sébastien MD, Vincent Cirimele, PhD, Pascal Kintz, PharmD, PhD, and Bertrand Ludes, MD, PhD, Institut de Médecine Légale, 11 rue Humann, 67085 Strasbourg Cedex, France. Razatos, Gerasimos BS* and Curtis Caylor, BS, New Mexico Department Health, Toxicology Bureau, PO Box 4700, Albuquerque, NM 87196-4700 Reich, Richard F. MS*, University of Florida, PO Box 14044, Gainesville, FL 32604 Reichardt, Eva M. MSc*, Bournemouth University, Talbot Campus, Fern Barrow, Poole, BH12 5BB, UNITED KINGDOM; Dene Baldwin, PhD, Concateno, 92 Milton Park, Oxfordshire, Abingdon, OX14 4RY, UNITED KINGDOM; and Michael D. Osselton, Bournemouth University, Fern Barrow, Talbot Campus, Poole, BH12 5BB, UNITED KINGDOM Reidy, Lisa J. PhD*, Bernard W. Steele, MD, and H. Chip Walls, BS, Forensic Toxicology Laboratory, University of Miami, Department of Pathology, 12500 Southwest 152nd Street, Building B, Miami, FL 33177 Rieders, Michael F. PhD*, Kevin D. Ballard, MD, PhD, Francis X. Diamond, Loan T. Nguyen, Eric F. Rieders, PhD, and William E. Vickery, National Medical Services, Inc., 3701 Welsh Road, Willow Grove, PA 19090; Fredric Rieders, PhD, Fredric Rieders Family Renaissance Foundation, 2300 Stratford Avenue, Willow Grove, PA 19090 Rieders, Michael F. PhD*, Robert A. Middleberg, PhD, Eric F. Rieders, PhD, and Lee M. Blum, PhD, National Medical Services, Inc., 3701 Welsh Road, Willow Grove, PA 19090 Index 101 Case Report: Death Due to Snorting of Crushed Sustained-Release Morphine Tablets Purity of Street Ketamine Preparations Retrieved From Night Club Amnesty Bins in London 160 A Fast GC/MS Method for the Analysis of 84 Common Selective Serotonin Reuptake Inhibitors Determination of Alprazolam in Oral Fluid 146 Postmortem Analysis of Buprenorphine/ Norbuprenorphine From Whole Blood by GC/MS Detection of Cortisol and Cortisone in Human Hair Validation of Volatile Analysis Using Dual Column Capillary GC Quantitative Mass Spectrometric Imaging of Drugs of Abuse in Postmortem Human Brain Tissue Investigation of the Effect of Vinegar on Oral Fluid Drug Testing: Effects on Immunoassay Screening Screening of Anabolic Steroids in Suspected DUI Drivers in Miami - Dade Florida Using ELISA Kits A Review of Succinylmonocholine Concentrations in Body Fluids and Tissues Analyzed by LC-MS/MS Toxicological Testing of Emergency Responders Following the World Trade Center Attack 5 63 265 203 82 21 65 222 176
Rodriguez, April BS, University of Texas Health Science Center, San Antonio TX, Sandra Valtier, MS; Clinical Research Squadron, 59th Medical Wing, Lackland AFB, TX; and John T. Cody, PhD*, Academy of Health Sciences, Ft. Sam Houston, TX Rohde, Douglas E. MS*, Lake County Crime Laboratory, 235 Fairgrounds Road, Painesville, OH 44077; and Dwight Flammia, PhD, Department of Forensic Science, 700 North 5th Street, Richmond, VA 23219 Rohde, Douglas E. MS*, Lake County Crime Laboratory, 235 Fairgrounds Road, Painesville, OH 44077; Robert A. Malinowski, DO, Ashtabula County, 600 State Road, #108, Ashtabula, OH 44004-3933; and Andrea D. McCollom, MD, and Amanda J. Jenkins, PhD, Cuyahoga County Coroner’s Office, 11001 Cedar Road, Cleveland, OH 44106 Rohde, Douglas E. MS*, William Bligh-Glover, MD, and Salvatore G. Rizzo, MD, Lake County Coroner’s Office, 104 East Erie Street, Painesville, OH 44077; and David A. Engelhart, PhD, and Amanda J. Jenkins, PhD, Cuyahoga County Coroner’s Office, 11001 Cedar Avenue, Cleveland, OH 44106 Ropero-Miller, Jeri D. PhD*, and Cynthia Lewallen, MS, RTI International, 3040 Cornwallis Road, Building 3, 3040 Cornwallis Road, Research Triangle Park, NC 27709; Nichole D. Bynum, MS, Center for Forensic Sciences, RTI International, 3040 Cornwallis Road, Building 3, Research Triangle Park, NC 27709; Meredith Meaders, BS, RTI International, 3040 Cornwallis Road, Building 3, Research Triangle Park, NC 27709; Jordan N. Espenshade, MSFS, 1420 Centre Avenue, Apartment 103, Pittsburgh, PA 15282; and John M. Mitchell, PhD, Michael R. Baylor, PhD, and Peter R. Stout, PhD, Center for Forensic Sciences, RTI International, 3040 Cornwallis Road, Research Triangle Park, NC 27709 Ropero-Miller, Jeri D. PhD*, Peter R. Stout, PhD, Edward J. Minden Jr., BS, and Nichole D. Bynum, MS, RTI International, Center for Forensic Sciences, 3040 Cornwallis Road, Building 3, Research Triangle Park, NC 27709; John F. Casale, BS, Drug Enforcement Administration, Special Testing Laboratory, 22624 Dulles Summit Court, Dulles, VA 20166; Insook Kim, PhD, Jennifer Runkle, BS, Marilyn Past, PhD, and Buddha D. Paul, PhD, Armed Forces Institute of Pathology, 1413 Research Boulevard, Building 102, Rockville, MD 20850 Index 102 Amphetamine and Methamphetamine Excretion Following Administration of Multiple Doses of the Drug Gewodin® 236 Inhalant Abuse Involving Difluoroethane 161 The Controversy of Death Involving Drugs of Abuse and TASERs® Suicide by Acute Cyanide Ingestion in a 40- Year-Old Male Analysis of Cocaine Analytes in Human Hair II: Evaluation of Different Hair Color and Ethnicity Types Following Surface Contamination and Laboratory Decontamination Signature Analysis of 25 Illicit Cocaine Samples and a Comparison to Analysis by AccuTOF DART 119 200 21 87
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FORENSIC TOXICOLOGY Proceedings 200
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Forensic Toxicology iii
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Preface The American Academy of For
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Toxiclogy Board of Directors Repres
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Development & Accreditation; Tracie
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Analysis of Amphetamine on Swabs an
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Evaluation of Enzymatic Hydrolysis
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Identification of Markers of JWH-01
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Cannabinoid Concentrations in Daily
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Alcohol Elimination Rate Variabilit
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Preparation of Oral Fluid for Quant
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Postmortem Pediatric Toxicology Rob
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A Quick LC/MS/MS Method for the Ana
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Fatal Death of an 8-Year-Old Boy Fr
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Nine Xylazine Related Deaths in Pue
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Gas Chromatography of Postmortem Bl
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Specificity Characteristics of Bupr
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Disposition of MDMA and Metabolites
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Determination of Trace Levels of Be
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Whole Blood/Plasma Cannabinoid Rati
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Prevalence of Cocaine on Urban and
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Intoxilyzer® 8000 Stability Study
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The Role of the Forensic Expert in
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Clinical vs. Forensic Toxicology -
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Comparative Analysis of GHB and GHV
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Toxicology of Deaths Associated Wit
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Determination of Toxins and Alkaloi
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Bupropion and Its Metabolites in Tw
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Use of a Novel Large Volume Splitle
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Death Due to Ingestion of Tramadol
Page 62 and 63: A Multi-Drug Fatality Involving the
Page 64 and 65: Urinary Excretion of α-Hydroxytria
Page 66 and 67: Analysis of Barbiturates by Fast GC
Page 68 and 69: A Review of Postmortem Diltiazem Co
Page 70 and 71: Analysis of Drugs From Paired Hair
Page 72 and 73: Index by Presenting Author Author b
Page 74 and 75: Virginia Street, West, Charleston,
Page 76 and 77: Bévalot, Fabien MD*, Laboratoire L
Page 78 and 79: C. Bishop BS*, Sandra Bruce R. McCo
Page 80 and 81: Chen, Bud-gen BS, Fooyin University
Page 82 and 83: Couper, Fiona J. PhD*, and Rory M.
Page 84 and 85: Drees, Julia C. PhD*, Judy A. Stone
Page 86 and 87: Furton, Kenneth G. PhD, Internation
Page 88 and 89: Gray, Teresa R. MS*, National Insti
Page 90 and 91: Halphen, Aimee M. MS*, and C. Richa
Page 92 and 93: Huestis, Marilyn A. PhD, David A. G
Page 94 and 95: Jufer, Rebecca A. PhD*, Barry S. Le
Page 96 and 97: Kim, Nam Yee PhD*, National Institu
Page 98 and 99: Langman, Loralie J. PhD*, Provincia
Page 100 and 101: Li, Ling MD, and Xiang Zhang, MD*,
Page 102 and 103: Lougee, Kevin M. BS*, Amy L. Lais,
Page 104 and 105: Mercan, Selda MSc, Institute of For
Page 106 and 107: Miles, Harry L. JD*, Green, Miles,
Page 108 and 109: Negrusz, Adam PhD, DSc*, Bindu K. S
Page 110 and 111: Peters, DeMia E. MS*, Liqun L. Wong
Page 114 and 115: Ropero-Miller, Jeri D. PhD*, RTI In
Page 116 and 117: Sasaki, Tania A. PhD*, Applied Bios
Page 118 and 119: Shakleya, Diaa M. PhD*, West Virgin
Page 120 and 121: Staretz, Marianne E. PhD, Departmen
Page 122 and 123: Swofford*, Henry J. 4207 Coatsworth
Page 124 and 125: Wagner, Michael MS, PA*, Harold E.
Page 126 and 127: Winterling, Jill M. BS*, Richard T.
Page 128 and 129: Index 117
Page 130 and 131: ange of years studied, drugs appear
Page 132 and 133: K6 Simultaneous Detection of Psyche
Page 134 and 135: K10 Analysis of Hydrocodone, Hydrom
Page 136 and 137: A cleanup tip was developed that is
Page 138 and 139: Eurachem method. Validation results
Page 140 and 141: tetrathiocynates and further determ
Page 142 and 143: K26 An Investigation Into the Cellu
Page 144 and 145: important of quickly identifying th
Page 146 and 147: K33 Detection of Various Performanc
Page 148 and 149: K36 The Uncertainty of Hair Analysi
Page 150 and 151: Results: The Intercept® device col
Page 152 and 153: collected on days 22-31, 14.8% rema
Page 154 and 155: concentrations of glucose and lacta
Page 156 and 157: A 48-year-old male was found dead o
Page 158 and 159: TOXICOLOGY Seattle 2010 Seattle 201
Page 160 and 161: scientists, as well as the importan
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toxicology in suspected narcotic ov
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Blood * Presenting Author Oxycodone
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According to the routine screening
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particle) analytical column operate
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ventilated low-lying areas. Inhalat
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may be relevant to forensic toxicol
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and one case had combined caffeine
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(16.9%), flunitrazepam (15.7%) and
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end of the run. Comparison of the r
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K42 Melendez-Diaz and Other 6th Ame
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In developing a full panel of DFSA
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including equilibration time. MS/MS
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ng/ml. The upper limit of quantitat
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to 18-years-old. Ten of the samples
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to 200 mg/dL. Samples above the lin
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which is used to relieve moderate t
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lab for drug and alcohol screening.
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elated fatalities. Methamphetamine,
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explosion. Toxicological analyses w
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and GC-MS, plus drug class specific
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incidence of methamphetamine in all
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K42 Homicide by Propofol Martha J.
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K45 Common Heroin Adulterants in Pu
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K48 Evaluation of Alcohol Markers i
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The color formation with the ferric
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explored. Opioids were chosen for a
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including pharmaco-toxicokinetic da
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of compounds typically found in ill
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Discussion: When investigating a to
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qualifier ratios. Samples containin
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BG and some cross-reactivity toward
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concentrations, almost invariably t
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nitrogen. Qualitative analysis was
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LC/MS/MS for analysis of benzodiaze
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were analyzed with each batch of sa
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concentration will decrease signifi
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and the meprobamate. To explain thi
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plasma drug concentrations. Oral fl
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significant correlation existed bet
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to an increase in the frequency of
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matrix despite extensive mixing pri
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y SPE (Clean Screen ® ZSTHC020 ext
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0.18 mg/L in aortic blood and 2.1 m
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munoassay. Identification and quant
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The fluctuations in the child’s u
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AMP BZE OPI PCP THCA ADULT INV SUBS
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Table I. Postmortem Distribution of
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K9 Fatal Ephedrine Intoxication in
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without any chromatography, resulti
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In the “direct” application of
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K21 Evaluation of the Immunalysis®
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fibrillation (VF) induction using t
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K28 Driving Under the Influence (DU
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K31 Methadone and Impaired Driving
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of Criminal Procedure was likewise
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Case #1: A 12-year-old female was f
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As seen in the above data, there ha
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determination of methamphetamine fr
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K48 Rapid Analysis of THC and Metab
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(0.09 mg/L). The accused drove over
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necessity. Information pertaining t
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K6 Determination of 2-Chloracetophe
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K8 Simultaneous Determination of HF
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This presentation will impact the f
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K16 Fentanyl Concentrations in 23 P
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Table 2 - GC Results Analyte LOD LO
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In America, recent growth in the po
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to fully prosecute the case, negoti
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dictive for the time of use. The ti
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absence, or cursory forms, of such
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Atomoxetine can be considered non-t
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nickel catalyst and detected with a
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Sample ID Hair result (pg/mg) Urine
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prevalence was compared with the do
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K1 Determination of Toxins and Alka
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toxicological profiles of the deced
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ecords were reviewed for all deaths
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K15 Performance Characteristics of
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analyzed by GC/MS with separation o
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This presentation will provide a fu
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tubing ran from the container throu
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murder and is often initially misdi
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K35 Interpretation of Glucose and L
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K38 Drugs in Driving Fatalities in
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jDALLA Toxicology j2004 K1 Use of a
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manufacturer. Analysis of samples f
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K9 An Analytical Protocol for the I
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K13 Laboratory Analysis of Remotely
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K15 Postmortem Production of Ethano
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K18 The Effects of pH on the Oxidat
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directed into an electrospray ioniz
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K25 The Detection of Oxycodone in M
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Hair analysis revealed the presence
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K32 Detection of Ketamine in Urine
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Conversations with two MDMA / MDA c
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The concentrations of total ropivac
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clozapine and metabolite in the cas
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(except in exceptionally high doses
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y pulmonary edema and a rapid cardi
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Toxicology K1 Urinary Excretion of
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presumptive pneumonia, and administ
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K7 Optimizing HPLC Separation of An
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and quantitative determination of M
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with BSTFA. Quantitation was perfor
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compounds contained in the current
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Fast gas chromatography (GC) has th
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importance to law enforcement agenc
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tramadol, closely followed by amitr
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acid. Oxalic and formic acids are f
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interaction involves activation of
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intake. Also, the positive serum an
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K1 A Review of Postmortem Diltiazem
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The concentration of interferent re
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three principal media, viz., blood,
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Of the tricyclic antidepressants, a
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Table 1. Effect of reconstitution v
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corticosteroids: cortisol and corti
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Hair specimens aligned in a foil en
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eference solution of each olanzapin
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presented. In the first case, a 31-
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combination with alcohol. From 1997
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Urine specimens were spiked with th
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