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An Introduction to Neutron Scattering - Spallation Neutron Source

An Introduction to Neutron Scattering - Spallation Neutron Source

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X-Ray Reflectivity<br />

Polarized <strong>Neutron</strong> Reflectivity<br />

10 0<br />

10 -1<br />

10 -2<br />

10 -3<br />

10 -4<br />

10 -5<br />

10 -6<br />

10 0<br />

10 -1<br />

10 -2<br />

10 -3<br />

10 -4<br />

Structure, Chemistry & Magnetism of Fe(001) on MgO(001)*<br />

0 0.1 0.2 0.3 0.4 0.5<br />

Q [Å -1 ]<br />

R ++ (obs)<br />

R ++ (fit)<br />

R -- (obs)<br />

R -- (fit)<br />

R SF (obs)<br />

R SF (fit)<br />

10 -5<br />

0.00 0.02 0.04 0.06<br />

Q [Å<br />

0.08 0.10 0.12<br />

-1 ]<br />

X-Ray<br />

<strong>Neutron</strong><br />

*Data courtesy of M. Fitzsimmons (LANSCE)<br />

Co-Refinement<br />

α-FeOOH (1.8µ B )<br />

Fe(001) (2.2µ<br />

B<br />

)<br />

fcc Fe (4µ B )<br />

H<br />

X-Ray<br />

β = 3.9(3)<br />

β = 5.2(3)<br />

β = 4.4(2)<br />

β = 3.1(3)<br />

1.9(2)nm<br />

10.7(2)nm Fe<br />

2.1(2)nm<br />

0.20(1)nm<br />

a-FeOOH<br />

0.44(2)nm<br />

0.07(1)nm<br />

interface<br />

0.03(1)nm<br />

MgO<br />

TEM<br />

<strong>Neutron</strong><br />

β = 4.4(8)<br />

β = 8.6(4)<br />

β = 6.9(4)<br />

β = 6.2(5)<br />

H

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