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Maintain the Teflon lid clean. Large particles of dust on either side of the<br />

Teflon sheet, near the edge or in the corresponding recess in the main vessel,<br />

will cause solvent vapor leaks. A moist, soft paper towel or cloth will remove<br />

dust with a minimum of scratching.<br />

THE TEFLON FUNNEL AND SOLVENT INLET<br />

Set the funnel holder in a stand to place the stopcock 55 cm above bench<br />

level. Screw the inlet fully down into the holder in the Teflon lid and choose an<br />

inlet stopper stamped with a numeral (1, 2, or 4) corresponding to the sorbent<br />

layer thickness (in mm) to be used. The funnel height, together with the<br />

stainless steel capillary tubing in the inlet stopper, controls the solvent flow rate<br />

to that required for the particular sorbent layer thickness used. If for some<br />

special purpose the flow rate must be changed, adjust the funnel height.<br />

5

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