Chromatotron
Chromatotron
Chromatotron
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glue-bound layers 29<br />
gypsum-bound layers 24<br />
partition layers 31<br />
set-up for slow setting<br />
layers 31<br />
storage 29<br />
sample<br />
introducing and eluting 11, 12, 13<br />
loading 15<br />
low solubility 11, 13<br />
prepurification 10<br />
volume 13<br />
scraping sorbent layers 28<br />
series connection 19<br />
silica - gel glue layers 24, 29<br />
silica gel - gypsum layers 21 - 23<br />
solvent<br />
addition 11<br />
choice 10<br />
condensation 12, 38<br />
flow rates 11, 14<br />
maximum 14<br />
inlet 5<br />
interrupting flow 15<br />
leaks 38, 39<br />
pumps 6-8, 33, 38, 39<br />
surface flow 14<br />
solvent inlet 5<br />
sorbent<br />
clean-up 17<br />
layer thickness 9<br />
loose layers 37<br />
sorbents<br />
(list) 20<br />
coating rotors 20<br />
drying layers 26<br />
scraping layers 28<br />
storage of coated rotors 29<br />
surface flow 14<br />
tailing 10<br />
Teflon funnel 5<br />
Teflon lid 4, 34<br />
test mixture 41<br />
Troubleshooting 35<br />
vapor locks 12, 38<br />
wick 5, 6<br />
43
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