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Pike Technologies Comprehensive Catalog of FTIR ... - Madatec

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P IKE T ECHNOLOGIES WWW. PIKETECH. COM 608-274-2721<br />

MIRacle Digital Clamp<br />

Ideal for Controlled<br />

Pressure<br />

MIRacle Pressure Clamp Options<br />

MIRacle Pressure Clamps are Pinned-in-Place and Easily Upgraded<br />

MIRacle Rotating Clamp<br />

Ideal for Cleaning Tip<br />

<strong>of</strong> Debris<br />

MIRacle pressure clamps are pinned in place and easily changeable<br />

within seconds. A high-pressure clamp is recommended for<br />

most applications and is available in digital, rotating and viewing<br />

versions. All clamps (except the viewing clamp) include tips for<br />

hard, s<strong>of</strong>t and pellet shaped samples. High-pressure clamps are<br />

calibrated to deliver over 10,000 psi <strong>of</strong> pressure when used with<br />

the single reflection crystal plates.<br />

Ability to deliver high pressure is very important for achieving<br />

spectral quality. In the example below, we demonstrate spectral<br />

differences for a porous polymer sample measured with the<br />

micrometer clamp and the high-pressure clamp. Clearly the<br />

spectrum obtained using the high-pressure clamp is required<br />

for a high quality result.<br />

MIRacle high-pressure clamps utilize a slip-clutch mechanism<br />

to prevent excessive pressure from being applied to the crystal.<br />

Max. lbs. Crystal<br />

MIRacle Clamp Pressures Pressure Diameter, mm PSI<br />

High-Pressure Clamps 40<br />

Micrometer Pressure Clamp 8<br />

1.8 10,141<br />

6.0 913<br />

1.8 2,028<br />

6.0 183<br />

MIRacle Viewing Clamp<br />

Ideal for Placing Fibers<br />

or Crystals<br />

MIRacle High-Pressure<br />

Clamp – Ideal for Routine<br />

Sampling<br />

MIRacle Micrometer<br />

Clamp – OK for Low<br />

Pressure Applications<br />

MIRacle Sampling Options<br />

The MIRacle can be configured with optional resistively heated<br />

crystal plates using a PIKE temperature control module. Digital<br />

and digital with PC control versions are available. The PC control<br />

module includes TempPRO s<strong>of</strong>tware which provides a graphical<br />

user interface for temperature control and kinetic measurements.<br />

An optional water<br />

jacket for MIRacle ATR<br />

crystal plates provides<br />

the ability to cool or<br />

elevate ATR sampling<br />

temperature via a<br />

water circulator.<br />

TempPRO s<strong>of</strong>tware for<br />

graphical setup and<br />

control <strong>of</strong> kinetic<br />

measurements<br />

Note: All clamps except Micrometer are high pressure<br />

MIRacle with Optional Heated Crystal Plate, Flow Cell and PIKE<br />

Temperature Control Module<br />

Porous Polymer Sample Measured Using High and Low-Pressure Clamp<br />

MIRacle ATR Summary<br />

The MIRacle ATR accessory is a high performance <strong>FTIR</strong> sampling<br />

tool for solid, liquid, or polymer samples. Easily changeable crystal<br />

plates provide optimized spectral data for unique sample types.<br />

With options for single or three reflection crystal plates, several<br />

pressure clamp styles and heating or cooling the MIRacle is able<br />

to address a wide range <strong>of</strong> <strong>FTIR</strong> sampling applications.<br />

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