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Pike Technologies Comprehensive Catalog of FTIR ... - Madatec

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Long-Path Gas Cells –<br />

For Measurement <strong>of</strong> Low Concentration Vapor Components<br />

Long-Path Gas Cells<br />

2.4 M Meter Gas Cell<br />

F EATURES O F T HE L ONG-PATH G AS C ELLS<br />

• Long-path gas cells for measurements <strong>of</strong> vapor species to<br />

ppb levels<br />

• Fixed and variable pathlength versions<br />

• Heated versions available<br />

• For most <strong>FTIR</strong> spectrometers<br />

PIKE <strong>Technologies</strong> <strong>of</strong>fers several Long-Path Gas Cells for analysis<br />

<strong>of</strong> trace components in gas samples – typical concentrations may<br />

range from the percent to ppb levels. The long-path cells feature<br />

a folded path design providing an extended pathlength within a<br />

compact dimension. The <strong>FTIR</strong> beam enters the cell through an IR<br />

transparent window and reflects a number <strong>of</strong> times between the<br />

accessory mirrors before exiting to the detector. The number <strong>of</strong><br />

reflections is determined by the optical configuration <strong>of</strong> the cell<br />

and may be selected as a permanently aligned version or<br />

adjustable by the user (variable path cells). Typical applications<br />

<strong>of</strong> the long-path gas cells include air pollution studies, gas purity<br />

determinations, monitoring <strong>of</strong> industrial processes, exhaust gas<br />

analysis and many others.<br />

All long-path gas cells <strong>of</strong>fered by PIKE <strong>Technologies</strong> are<br />

manufactured by Infrared Analysis, Inc., pioneers in the<br />

development <strong>of</strong> gas analysis technology.<br />

Permanently aligned long-path gas cells. All cell assemblies<br />

include a heavy wall borosilicate glass tube mounted on a corrosionresistant<br />

anodized aluminum base. The base includes spectrometerspecific<br />

transfer optics allowing placement <strong>of</strong> the accessory in the<br />

sample compartment <strong>of</strong> the <strong>FTIR</strong>. Infrared transparent windows<br />

serve as beam entry and exit ports (windows are easily replaceable<br />

and different window materials are available). The top <strong>of</strong> the cell<br />

is enclosed by the valve/gauge assembly with all the valves made<br />

<strong>of</strong> stainless steel. The accessory mirrors are mounted permanently<br />

with chemically inert cement at the bottom <strong>of</strong> the cell and the<br />

facing part <strong>of</strong> the top enclosure. The gold coated mirrors have<br />

protected surfaces and the gas cells can be cleaned with detergent<br />

and water without loss <strong>of</strong> cell throughput or alignment.<br />

Variable-Path gas cells. The construction and main components<br />

<strong>of</strong> the variable-path gas cells are identical with those described<br />

above, with an exception <strong>of</strong> the internal mirror assembly. The cell<br />

has two adjustable mirrors located at the top <strong>of</strong> the enclosure<br />

(controlled with a calibrated dial) and one stationary mirror<br />

cemented to the cell base. Adjustments to mirror positions allow<br />

selection <strong>of</strong> different pathlengths supported by the cell.<br />

Some gas measurement applications require temperature<br />

control for higher precision or to prevent condensation <strong>of</strong> specific<br />

components. PIKE <strong>Technologies</strong> <strong>of</strong>fer heated versions <strong>of</strong> our fixed<br />

and variable path gas cells.<br />

2.4 m 10.0 m 22.0 m 33.0 m 1-16 m<br />

Fixed Fixed Fixed Fixed Variable<br />

Base Path 5" 10" 22" 22" 10"<br />

Body Material Glass Glass Glass Glass Glass<br />

Optics Coatings Gold Gold Gold Gold Gold<br />

Window Material KCI KCI KCI KCI KCI<br />

Window 37.5 x 4 mm 25 x 4 mm 25 x 4 mm 25 x 4 mm 25 x 4 mm<br />

Dimension<br />

# Window 1 2 2 2 2<br />

Cell Volume 0.1 liter 2.3 liter 8.5 liter 8.5 liter 2.3 liter<br />

Specifications for Long-Path Gas Cells from PIKE <strong>Technologies</strong><br />

T RANSMISSION S AMPLING P RODUCTS – A UTOMATED AND M ANUAL T ECHNOLOGIES<br />

93

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