Pike Technologies Comprehensive Catalog of FTIR ... - Madatec

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VeeMAX II with ATR – Variable Angle, Single Reflection ATR for Depth Profiling Studies F EATURES O F T HE V EEMAX II WITH ATR • Continuously variable set angle of incidence – 30 to 75 degrees • 0.4 to 46 micron depth of penetration – dependent on crystal material, angle of incidence, sample’s refractive index and wavelength of IR beam – ideal for depth profiling studies • High throughput for excellent quality spectra in a short time period • Optional, high-pressure clamp for sampling of films, coatings or powdered samples • Integrated position for optional manual or automated polarization • Motorized option with electronic control module and AutoPRO software for automated, high-precision experiments • VeeMAX II can be used as a variable angle of incidence specular reflection accessory • Sealed and purgeable optical design to eliminate water vapor and carbon dioxide interferences combination of large crystal diameter (20 mm) and slip-clutch pressure clamp provides sample to crystal contact without altering layered sample composition. The optional liquid retainer may be added to the crystal plate for analysis of liquid samples. Motorized control of angle of incidence via personal computer for automated data collection of depth profiling studies and ATR measurements is available as an option for the accessory. The motorized VeeMAX II option is ideal for depth profiling studies as it greatly speeds and improves the precision and reproducibility of the data collection process. VeeMAX with ATR optical layout Depth profiling study of layered polymer film. FTIR spectra collected using ZnSe crystal at set angles of incidence from 43 to 65 degrees. IR absorbance band at 1591 cm -1 clearly increases relative to other bands as we probe deeper into the sample. A TTENUATED T OTAL R EFLECTANCE – L IQUIDS, SOLIDS AND I N -BETWEEN PIKE Technologies announces the VeeMAX II, now with new variable angle single reflection attenuated total reflection (ATR) capability. The VeeMAX II with ATR now offers continuous variable angle of incidence and a variety of crystal plates to selectively control the depth of penetration of the IR beam into the sample. New ATR applications include the study of layered samples, coatings, release agents, monolayers on silicon and chemical migration studies. The VeeMAX II with ATR accessory provides exceptionally high throughput (over 50% with 45 degree ZnSe crystal) to minimize sampling time and enable detection of low concentration components in samples of complex composition. The flat plate crystals offered for the VeeMAX II are ideal for solid and layered samples and are designed for use with the optional pressure clamp. The AutoPRO Software control of VeeMax II angle of incidence (automated polarizer available) for automated depth profiling studies, angle of incidence and polarization angle can be set independently. 21
22 P IKE T ECHNOLOGIES WWW. PIKETECH. COM 608-274-2721 Analysis of monomolecular layer on silicon – VeeMAX II with 60 degree Ge crystal, pressure clamp with 7.8 mm tip and p polarization. VeeMax II Base Optics (must select, insert spectrometer model for XX) P ART N UMBER 013-10XX D ESCRIPTION VeeMax II Variable Angle Specular Reflectance Accessory Notes: VeeMax II includes specular reflectance masks (2", 5/8" and 3/8"), purge tubes, purge kit and spectrometer base mount. Please see the FTIR instrument code sheet. VeeMax II ATR Crystal Plates (must select 1 or more for ATR) P ART N UMBER D ESCRIPTION 013-4020 Flat Plate, ZnSe, 45° 013-4030 Flat Plate, ZnSe, 60° 013-4040 Flat Plate, Ge, 45° 013-4050 Flat Plate, Ge, 60° 013-4060 Flat Plate, Ge, 65° 013-4080 Flat Plate, Si, 45° 013-4070 Flat Plate, Si, 60° 013-4090 Flat Plate, ZnS, 45° 013-4095 Flat Plate, ZnS, 60° 013-3400 Liquid Retainer for VeeMAX II ATR crystals Notes: VeeMax II Crystal Plates are pre-aligned and pinned-in-place. Changing crystal plates is easy and fast to optimize sampling results. ZnS crystal plate is excellent for deepest penetration of IR beam. Si crystal plate is excellent for Far IR ATR. If you need a crystal not listed here, please contact us. Heated VeeMAX II ATR Crystal Plates (optional) P ART N UMBER D ESCRIPTION 013-4120 Heated Flat Plate, ZnSe, 45° 013-4130 Heated Flat Plate, ZnSe, 60° 013-4140 Heated Flat Plate, Ge, 45° 013-4150 Heated Flat Plate, Ge, 60° 013-4160 Heated Flat Plate, Ge, 65° 013-4170 Heated Flat Plate, Si, 60° 013-4180 Heated Flat Plate, Si, 45° 013-4190 Heated Flat Plate, ZnS, 45° 013-4195 Heated Flat Plate, ZnS, 60° 076-1410 PC Temperature Control Module (Single RTD) 076-1210 Digital Temperature Control Module (Single RTD) Notes: Heated VeeMAX crystal plates may be heated to 130 °C. A temperature controller must be selected. TempPRO software for graphical setup and control of kinetic measurements O RDERING I NFORMATION Specifications for Resistively Heated VeeMax ATR Plates Temperature Range: Ambient to 130 °C Accuracy: +/- 0.5% Voltage: Sensor Type: Controllers Digital: Digital PC: Input Voltage: Output Voltage: 24 VAC 3 wire Pt RTD (low drift, high stability) +/- 0.1% of set point +/- 0.1% of set point, graphical setup, up to 3 ramps, USB interface 110/220 V, switch able 10A/24 VAC VeeMax II Pressure Clamp (must select for solids, films or powder analysis) P ART N UMBER D ESCRIPTION 013-3100 VeeMax ATR Pressure Clamp 025-3094 7.8 mm Tip for VeeMAX ATR Pressure Clamp Notes: Pressure clamp supplied with 20 mm tip for polymer films. The 7.8 mm pressure tip is required for monolayers on silicon. The pressure clamp is required for solids, films, coatings and powdered samples. VeeMax II Sampling Options P ART N UMBER D ESCRIPTION 007-0300 PIKECalc Software 013-2800 Motorized Option for VeeMAX II 090-1000 Manual Polarizer, ZnSe 090-2000 Automated Polarizer, ZnSe Notes: PIKECalc software provides easy calculations of depth of penetration, effective angle of incidence and critical angle for ATR measurements. Motorized Option includes PIKE Technologies AutoPRO software and controller. Other polarizer options are found in the polarization section of this catalog. Replacement Parts P ART N UMBER D ESCRIPTION 013-4010 Mask Set for VeeMAX Heated crystal plates are available for the VeeMAX II for Temperature Studies
Page 2 and 3: FTIR Instrument Code XX ABB Bomem F
Page 4 and 5: TABLE O F C ONTENTS Pages 1 - 6 Pag
Page 6 and 7: Sampling Kits If you are not sure w
Page 8 and 9: Comprehensive Transmission Sampling
Page 10 and 11: Valu-Line - High Performance Set of
Page 12 and 13: Attenuated Total Reflectance Sampli
Page 14 and 15: Table 1: MIRacle Crystal Plate Spec
Page 16 and 17: MIRacle Base Optics (must select, i
Page 18 and 19: GladiATR Base Optics (must select,
Page 20 and 21: HATR Crystal Plate Choices PIKE Tec
Page 22 and 23: HATR and HATRPlus Pressure Clamp (m
Page 24 and 25: Optimized FTIR spectrum of polymer
Page 28 and 29: Classic VATR - Variable Angle ATR f
Page 30 and 31: Table 1 ATR Sampling ZnSe, Diamond
Page 32 and 33: Diffuse Reflectance Products Diffus
Page 34 and 35: DiffusIR - Research Grade Diffuse R
Page 36 and 37: UpIR - Upward Looking Diffuse Refle
Page 38 and 39: X, Y Autosampler - Transmission and
Page 40 and 41: Diffuse Reflectance - Theory and Ap
Page 42 and 43: Specular Reflectance Products Specu
Page 44 and 45: Changing the angle of incidence wit
Page 46 and 47: 80Spec - Grazing Angle Specular Ref
Page 48 and 49: 10Spec - Measures Sample Reflectanc
Page 50 and 51: Specular Reflectance - Theory and A
Page 52 and 53: Polarization Products Polarizers ma
Page 54 and 55: Infrared Polarizers - Theory and Ap
Page 56 and 57: Integrating Sphere Products Integra
Page 58 and 59: NIR IntegratIR - Integrating Sphere
Page 60 and 61: Integrating Spheres - Introduction
Page 62 and 63: Fiber Optic Sampling Products Fiber
Page 64 and 65: FlexIR - NIR Fiber Optic Accessory
Page 66 and 67: Microsampling Products Microsamplin
Page 68 and 69: Switching from transmission to refl
Page 70 and 71: Microsampling Tools - Compression C
Page 72 and 73: Beam Condensers - 4X and 6X Version
Page 74 and 75: Transmission Sampling Products Tran
Page 76 and 77:
RotatIR - Automated Rotating Sample
Page 78 and 79:
X, Y Autosampler - Transmission and
Page 80 and 81:
Demountable Liquid Cells - For Vers
Page 82 and 83:
Long-Path Quartz Liquid Cells - For
Page 84 and 85:
Demountable Liquid Cell Windows (mu
Page 86 and 87:
Bolt Press & Hydraulic Die - Low-Co
Page 88 and 89:
PIKE CrushIR - Digital Hydraulic Pr
Page 90 and 91:
Sample Preparation Accessories - Fo
Page 92 and 93:
Disks, Windows and Powders - For Tr
Page 94 and 95:
Disks, 41 mm Diameter 3 mm Thicknes
Page 96 and 97:
Short Path Gas Cells - For Samples
Page 98 and 99:
Long-Path Gas Cells - For Measureme
Page 100 and 101:
Transmission Sampling Techniques -
Page 102 and 103:
An alternate method for analysis of
Page 104 and 105:
Special Applications Products PIKE
Page 106 and 107:
MappIR and MAP300 - For Automated A
Page 108 and 109:
TGA/FTIR Accessory - Identification
Page 110 and 111:
Semiconductor Applications - FTIR S
Page 112 and 113:
Other Useful Products for Spectrosc
Page 114 and 115:
ATR spectra are somewhat different
Page 116 and 117:
ATR Spectral Data Bases - Optimize
Page 118 and 119:
Alphabetical Index A 10Spec, specul
Page 120 and 121:
T Teflon gaskets, demountable cell
Page 122 and 123:
022-5340 HATR Liquid Jacketed Troug
Page 124 and 125:
160-1007 25 x 2 mm ZnSe (6 pack) 88
Page 126 and 127:
162-1130 Press-On Demountable Liqui
Page 128:
We are PIKE Technologies, a small c
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Pike Technologies Comprehensive Catalog of FTIR ... - Madatec

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