03.10.2016 Views

SIM0216

You also want an ePaper? Increase the reach of your titles

YUMPU automatically turns print PDFs into web optimized ePapers that Google loves.

ELECTRON MICROSCOPY<br />

Stemming Unwanted Interference<br />

Resolution Improvement by Incoherent Imaging with ISTEM<br />

Florian Krause<br />

In Transmission Electron Microscopy (TEM) spatially incoherent image formation can have significant<br />

advantages regarding attainable resolution by removing unwanted interference effects. This<br />

has been exploited in the scanning TEM mode, which is incoherent but limited by other factors.<br />

Combining a scanning beam with the conventional TEM imaging mode can overcome these limitations.<br />

This method called ISTEM gives access to the advantages of both modes and facilitates an increase<br />

in resolution.<br />

From Traditional TEM to ISTEM<br />

High resolution Transmission Electron<br />

Microscopy (TEM) is one of the most important<br />

tools for the investigations of nanoscale<br />

structures. Historically, it has<br />

mostly been divided into two modes:<br />

For Conventional TEM (CTEM) the<br />

specimen is illuminated with a plane<br />

electron wave and then the image is<br />

formed by the objective lens of the microscope.<br />

For modern field emission sources<br />

the image formation is almost completely<br />

coherent here. Because a large area is illuminated,<br />

CTEM is influenced neither by<br />

the positioning precision of the incoming<br />

beam nor by aberrations of the probe<br />

forming lenses. Another advantage is the<br />

fact that though the size of the electron<br />

source has an influence on the images, it<br />

is not the factor limiting the resolution.<br />

Due to the coherence however, highresolution<br />

CTEM images can show complex<br />

interference patterns and hence be<br />

difficult to interpret. The high coherence<br />

also causes a strong dependence of the<br />

image pattern on the energy of the incident<br />

electrons. Chromatic aberration is<br />

therefore the limiting factor for resolution<br />

in CTEM.<br />

In the Scanning TEM (STEM) mode,<br />

the electron beam is focused onto the<br />

specimen. Then the intensity in a specific<br />

area of the diffraction pattern is<br />

recorded with an extended, usually circular<br />

or annular, detector. The image is<br />

formed by scanning over an area of the<br />

specimen. It can be shown that STEM is<br />

effectively an incoherent imaging mode<br />

due to the universal principle of reciprocity<br />

[1]. Therefore it is much more ro-<br />

40 • G.I.T. Imaging & Microscopy 2/2016

Hooray! Your file is uploaded and ready to be published.

Saved successfully!

Ooh no, something went wrong!