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Biennial Report 2016/2017

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<strong>Report</strong>s<br />

Reactive Ion Beam Etching for Ultraprecise Fabrication of Optical<br />

Elements: A Progress <strong>Report</strong><br />

R. Fechner, A. Finzel, G. Dornberg, M. Mitzschke, S. Görsch, A. Nickel, F. Frost<br />

in collaboration with<br />

F. Koch, D. Lehr, O. Schönbrodt, T. Glaser, Carl Zeiss Jena GmbH, Microstructured Optics, Germany<br />

Introduction<br />

(Reactive) ion beam etching ((R)IBE) becomes<br />

more and more a versatile and indispensable<br />

technology step in the fabrication chain of high<br />

precision optical elements. An example for the<br />

crucial importance of RIBE is the pattern transfer<br />

of 3D resist or metal masks into hard optical<br />

materials, especially for the fabrication of highend<br />

optical diffraction gratings [1,2].<br />

Today gratings can be manufactured using<br />

various sophisticated techniques, e. g.,<br />

interference lithography, mechanical ruling,<br />

volume holography, laser direct writing<br />

lithography, electron-beam writing, and Talbot<br />

lithography. While for some applications the resist<br />

grating is sufficient, the vast majority of<br />

applications demands grating patterns to be<br />

transferred into glass, silicon, metals, or other<br />

substrate materials. Due to the very high flexibility<br />

and degree of freedom RIBE is predestined for<br />

this. Thus, due to process optimized gas mixture<br />

used for etching, the selectivity (ratio of the etch<br />

rates of the substrate material related to the etch<br />

rate of the mask material) can be varied over<br />

several orders of magnitude making it possible to<br />

compress or stretch surface profiles during the<br />

pattern transfer, according to the respective<br />

optical application. Owing to the spatial separation<br />

of ion generation and substrate, RIBE steps at<br />

non-normal ion incidence additionally offers a<br />

targeted alteration of the surface profile, e. g., the<br />

implementation of undercut patterns or lanted<br />

gratings or the realization of blazed gratings<br />

starting with symmetrical mask profiles. Moreover,<br />

RIBE is a key step in the ion beam planarization<br />

technique, for example, for smoothing of diamond<br />

turned metal surfaces with sub-nm roughness<br />

values [3].<br />

In this report research activities in the core area<br />

Ion Beam assisted Technologies will be<br />

summarized. The work focused mainly on<br />

improvement of technical infrastructure, the<br />

integration and further optimization of in-situ<br />

measurement techniques, the implementation of<br />

sophisticated processing algorithms, which allow<br />

a RIBE processing of workpieces larger than the<br />

extension of the ion beam and the development of<br />

RIBE processing steps for high-end diffraction<br />

gratings.<br />

Technical Infrastructure<br />

The improvement in the technical infrastructure<br />

was one of the key issue in recent years. Thanks<br />

to the funding provided by BMBF within the<br />

SHAPION project [4] and with the additional help<br />

of European Regional Development funding and<br />

funding from the Free State of Saxony a total of<br />

three new RIBE facilities (ISA 200, SHAPION,<br />

RIBE 450) could be taken into operation recently.<br />

All RIBE systems are equipped with Kaufmantype<br />

ion sources (grid apertures of 180 mm),<br />

configured for Fluorine-based etching gases, and<br />

were partially upgraded with different optical and<br />

mass spectroscopic in-situ measurement<br />

technologies which guarantee for a high process<br />

stability and reliability. All machines allow a base<br />

pressure of 1 × 10 -7 mbar and are able to execute<br />

process variable user defined recipes. Both ISA<br />

200 as well as the SHAPION RIBE plant enable<br />

the processing of workpieces up to 245 mm in<br />

diameter. With the former also a defined ion beam<br />

sputter deposition of, e.g. metals, during etching<br />

is possible in order to investigate ion beam driven<br />

self-organized pattern formation processes with<br />

and without co-deposition. Within the extended<br />

research infrastructure a new state-of-the-art<br />

Figure 1: View in the RIBE 450 plant with 5-axis-motion<br />

system for workpieces up to 450 mm diameter.<br />

18

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