Homogeneous CO Hydrogenation: Ligand Effects on the Lewis Acid ...

Table 4. Bond lengths [Å] and angles [°] for [1-M 2][BAr F
4] (AJMM43) (CCDC 768445).
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Re(1)-C(1) 1.974(2)
Re(1)-C(2) 1.988(2)
Re(1)-C(4) 2.005(2)
Re(1)-C(3) 2.018(2)
Re(1)-P(2) 2.4509(5)
Re(1)-P(1) 2.4521(5)
P(1)-C(11) 1.820(2)
P(1)-C(17) 1.824(2)
P(1)-C(5) 1.825(2)
P(2)-C(32) 1.820(2)
P(2)-C(38) 1.820(2)
P(2)-C(26) 1.829(2)
O(1)-C(1) 1.141(3)
O(2)-C(2) 1.137(3)
O(3)-C(3) 1.130(3)
O(4)-C(4) 1.135(3)
C(5)-C(10) 1.394(3)
C(5)-C(6) 1.397(3)
C(6)-C(7) 1.389(3)
C(7)-C(8) 1.392(3)
C(8)-C(9) 1.375(3)
C(9)-C(10) 1.389(3)
C(11)-C(12) 1.390(3)
C(11)-C(16) 1.399(3)
C(12)-C(13) 1.385(3)
C(13)-C(14) 1.377(3)
C(14)-C(15) 1.383(3)
C(15)-C(16) 1.387(3)
C(17)-B(1) 1.596(3)
B(1)-C(18) 1.525(3)
B(1)-C(22) 1.600(3)
C(18)-C(19) 1.538(3)
C(18)-C(25) 1.589(3)
C(19)-C(20) 1.508(3)
C(20)-C(21) 1.498(3)
C(21)-C(22) 1.546(3)
C(22)-C(23) 1.520(3)
C(23)-C(24) 1.539(3)
C(24)-C(25) 1.493(3)
C(26)-C(31) 1.378(3)
C(26)-C(27) 1.393(3)
C(27)-C(28) 1.392(3)
C(28)-C(29) 1.380(4)
C(29)-C(30) 1.384(4)
C(30)-C(31) 1.391(3)
C(32)-C(33) 1.390(3)
C(32)-C(37) 1.402(3)
C(33)-C(34) 1.391(3)
C(34)-C(35) 1.385(3)
C(35)-C(36) 1.385(4)
C(36)-C(37) 1.386(3)
C(38)-B(2A) 1.568(3)
B(2A)-C(39A) 1.524(3)
B(2A)-C(43A) 1.603(3)
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