Homogeneous CO Hydrogenation: Ligand Effects on the Lewis Acid ...

Table 3. Selected bond lengths [Å] and angles [°] for 11 (AJMM55) (CCDC 776949).
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Re(1)-C(1) 1.955(12)
Re(1)-C(4) 1.963(13)
Re(1)-C(3) 1.973(13)
Re(1)-C(2) 1.990(13)
Re(1)-C(9) 2.200(11)
Re(1)-P(1) 2.478(3)
Re(2)-C(8) 1.900(16)
Re(2)-C(5) 1.924(15)
Re(2)-C(6) 1.942(13)
Re(2)-C(7) 1.974(12)
Re(2)-C(32) 2.277(13)
Re(2)-P(2) 2.448(3)
C(1)-Re(1)-C(4) 95.5(5)
C(1)-Re(1)-C(3) 90.4(5)
C(4)-Re(1)-C(3) 173.8(5)
C(1)-Re(1)-C(2) 91.8(5)
C(4)-Re(1)-C(2) 87.5(5)
C(3)-Re(1)-C(2) 90.5(5)
C(1)-Re(1)-C(9) 177.6(4)
C(4)-Re(1)-C(9) 86.8(4)
C(3)-Re(1)-C(9) 87.3(4)
C(2)-Re(1)-C(9) 87.6(5)
C(1)-Re(1)-P(1) 92.8(3)
C(4)-Re(1)-P(1) 85.8(3)
C(3)-Re(1)-P(1) 95.8(3)
C(2)-Re(1)-P(1) 172.2(4)
C(9)-Re(1)-P(1) 88.1(3)
C(8)-Re(2)-C(5) 93.7(6)
C(8)-Re(2)-C(6) 90.5(6)
C(5)-Re(2)-C(6) 90.0(5)
C(8)-Re(2)-C(7) 88.8(5)
C(5)-Re(2)-C(7) 92.7(5)
C(6)-Re(2)-C(7) 177.2(6)
C(8)-Re(2)-C(32) 94.2(6)
C(5)-Re(2)-C(32) 172.1(6)
C(6)-Re(2)-C(32) 90.7(5)
C(7)-Re(2)-C(32) 86.7(5)
C(8)-Re(2)-P(2) 159.0(5)
C(5)-Re(2)-P(2) 106.6(5)
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