Homogeneous CO Hydrogenation: Ligand Effects on the Lewis Acid ...

Table 4. Bond lengths [Å] and angles [°] for 11 (AJMM55) (CCDC 776949).
_______________________________________________________________________________
Re(1)-C(1) 1.955(12)
Re(1)-C(4) 1.963(13)
Re(1)-C(3) 1.973(13)
Re(1)-C(2) 1.990(13)
Re(1)-C(9) 2.200(11)
Re(1)-P(1) 2.478(3)
Re(2)-C(8) 1.900(16)
Re(2)-C(5) 1.924(15)
Re(2)-C(6) 1.942(13)
Re(2)-C(7) 1.974(12)
Re(2)-C(32) 2.277(13)
Re(2)-P(2) 2.448(3)
P(1)-C(25) 1.809(13)
P(1)-C(18) 1.816(9)
P(1)-C(19) 1.840(10)
P(2)-C(39) 1.801(12)
P(2)-C(33) 1.830(11)
P(2)-C(31) 1.836(12)
O(1)-C(1) 1.161(12)
O(2)-C(2) 1.124(13)
O(3)-C(3) 1.164(13)
O(4)-C(4) 1.175(13)
O(5)-C(5) 1.162(15)
O(6)-C(6) 1.135(13)
O(7)-C(7) 1.147(12)
O(8)-C(8) 1.222(16)
O(9)-C(9) 1.328(14)
O(9)-C(32) 1.493(13)
O(10)-C(9) 1.248(11)
O(10)-B(1) 1.591(15)
B(1)-C(14) 1.592(17)
B(1)-C(18) 1.619(14)
B(1)-C(10) 1.650(14)
C(10)-C(17) 1.502(13)
C(10)-C(11) 1.551(16)
C(11)-C(12) 1.490(17)
C(12)-C(13) 1.583(14)
C(13)-C(14) 1.532(15)
C(14)-C(15) 1.530(14)
C(15)-C(16) 1.558(13)
C(16)-C(17) 1.553(15)
C(19)-C(20) 1.382(13)
C(19)-C(24) 1.412(12)
C(20)-C(21) 1.373(13)
C(21)-C(22) 1.373(14)
C(22)-C(23) 1.341(14)
C(23)-C(24) 1.376(14)
C(25)-C(26) 1.377(15)
C(25)-C(30) 1.397(15)
C(26)-C(27) 1.383(18)
C(27)-C(28) 1.404(16)
C(28)-C(29) 1.380(16)
C(29)-C(30) 1.426(17)
C(31)-C(32) 1.632(16)
S282