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dissertation global and local fracture properties of metal matrix ...

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Section 4<br />

Table 4.1. Chemical composition <strong>of</strong> the Al-6061 alloy<br />

Si Fe Cu Mn Mg Zn Cr Ti<br />

0.4÷0.8 0.7 0.15÷0.4 0.15 0.8÷1.2 0.25 0.04÷0.35 0.15<br />

chemical composition <strong>of</strong> the <strong>matrix</strong> is given in Table 4.1. The mean alumina particle size is<br />

about 10 µm. Metallographic sectioning shows that the particles are distributed quite<br />

homogeneously in all composites, but a few particle clusters are observed, as well (Fig. 4.1).<br />

The particles have a shape <strong>of</strong> spheroids. The MMCs were supplied in the shape <strong>of</strong> bars with a<br />

section <strong>of</strong> 40x12.5 mm by AMAG (Austria).<br />

The materials were annealed at 560°C for 30 minutes, quenched in water, <strong>and</strong> kept at room<br />

temperature for 1 week [69]. To study the effect <strong>of</strong> the <strong>matrix</strong> <strong>properties</strong> on the composite<br />

behavior, the materials were subjected to different heat treatments:<br />

(1.) aging at room temperature;<br />

(2.) aging at 160°C for 8h;<br />

(3.) aging at 160°C for 24h;<br />

(4.) aging at 160°C for 200h.<br />

In the following, the investigated specimens are referred to by their volume percentage <strong>and</strong><br />

the heat treatment, e.g., Specimen Al2O3-10-RT or Specimen Al2O3-15-8h. The term<br />

“Increasing aging condition” will be used when specimens with the conditions RT, 160°C/8h,<br />

160°C/24h, 160°C/200h are compared.<br />

4.1.1.2. Tensile tests<br />

To determine the <strong>global</strong> material parameters, conventional tensile mechanical tests are<br />

performed. The tensile specimens have a cylindrical shape with a diameter <strong>of</strong> 3 mm <strong>and</strong> a<br />

gage length <strong>of</strong> 15 mm (Fig. 4.2). The tensile tests are conducted on a mechanical testing<br />

machine “ZWICK” at a loading rate <strong>of</strong> 5.6·10 -4 s -1 . The materials are assumed to follow a<br />

st<strong>and</strong>ard power-law work hardening behavior (Eq. 3.3). The strain hardening coefficient, N,<br />

<strong>and</strong> the coefficient, α, are determined from the log(ε/ε0) vs. log(σ/σ0) curves. The fit was<br />

taken so that it covers the better part <strong>of</strong> the stress-strain behavior (Fig. 4.3a). The results <strong>of</strong> the<br />

tensile tests are collected in Table 4.2. The mechanical <strong>properties</strong> <strong>of</strong> the <strong>matrix</strong> material in<br />

each considered aging condition are given in Table 3.3, as well.<br />

30

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