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dissertation global and local fracture properties of metal matrix ...

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Section 4<br />

4.3.2. The relation between the particle location with respect to the crack tip <strong>and</strong> the CODvi-<br />

values<br />

As seen from Figures 4.18 - 4.20, the scatter <strong>of</strong> the CODvi-values is still high in all<br />

investigated specimens, but less than those <strong>of</strong> the CODi-values. The maximum CODvi-values<br />

seem to decrease with increasing aging conditions <strong>and</strong> with increasing particle volume<br />

fraction, leading to a narrowing <strong>of</strong> the scatter. Only for the cast MMCs, the CODi-values for<br />

the Specimens 160°C-200h are slightly higher in comparison with Specimens 160°C-24h.<br />

Contrary to the CODi-values, a slight tendency to decreasing CODvi-values with increasing<br />

particle location angle, θ, can be noted for the cast MMCs (Fig. 4.18). Whereas small CODvi-<br />

values appear at large angles between θ = 50 <strong>and</strong> 70° in the RT-condition, they are more<br />

equally distributed for the materials aged at 160°C.<br />

Very interesting are the crack pr<strong>of</strong>iles through alumina particles in cast MMCs with large<br />

particle location angle θ. For such particles, a step appears on both <strong>fracture</strong> surfaces, <strong>and</strong> the<br />

CODvi- <strong>and</strong> CODi-values are measured as the height differences <strong>of</strong> the two steps. Figure 4.21<br />

presents an example <strong>of</strong> the pr<strong>of</strong>iles through Particle 7 <strong>of</strong> the Specimen Al2O3-10-RT, located<br />

at θ = 47°. Here, void initiation <strong>and</strong> <strong>fracture</strong> initiation occur simultaneously at a very low<br />

value <strong>of</strong> CODvi ≈ CODi ≈ 0. One can conclude that Particle 7 <strong>fracture</strong>s at a low external<br />

loading, <strong>and</strong> the crack immediately extends.<br />

No dependency <strong>of</strong> the CODvi-values on the distance to the crack tip, r, is observed in both the<br />

cast <strong>and</strong> PM MMCs. The CODvi vs. r curves show a scatter similar to those <strong>of</strong> Figures 4.16,<br />

4.17a (Figs. 4.19, 4.20a). It should be noted that no near-zero CODvi-values are observed for<br />

the PM MMCs in comparison with the cast MMCs. What might be a reason for such different<br />

effect <strong>of</strong> the angle θ on the CODvi-values in different materials?<br />

It is plausible that the void initiation might be strongly influenced by plastic straining.<br />

Therefore, it can suggested that this finding has to do with the shape <strong>of</strong> the plastic zone which<br />

has its maximum extension at an angle <strong>of</strong> about θ = 70° with respect to the crack plane (Fig.<br />

4.22). For plane strain conditions, the plastic zone size in that direction, ω70, is by a factor 4.4<br />

larger than in the crack plane [73, 74]. As was shown in [74], ω70 can be determined directly<br />

from the COD as<br />

2<br />

K<br />

J E<br />

ω70 =<br />

0.<br />

157 ≈ 0.<br />

16 ≈<br />

σ<br />

σ<br />

2<br />

y<br />

51<br />

2<br />

y<br />

0.<br />

16<br />

d<br />

N<br />

E σ COD<br />

o<br />

2<br />

y<br />

σ<br />

(4.2)

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