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PHYS01200804001 Sohrab Abbas - Homi Bhabha National Institute

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2<br />

(1)<br />

-(δk i .Δ i ) /2<br />

Γ (Δ) = e , (73)<br />

i=x,y,z<br />

is obtained. In this case, the wave vector distribution and coherence length i are related by<br />

Heisenberg uncertainty relation [95],<br />

δk Δ = 1/ 2 . (74)<br />

i<br />

i<br />

Diffraction from a macroscopic grating<br />

Diffraction of neutrons of wavelength for near normal incidence at a grating of period d>><br />

gives rise to a pattern with an angular separation ~ /d between successive intensity maxima. With<br />

a grating period of even a few microns, scattering angles become as small as a few arcsec for<br />

thermal and cold neutrons. A collimation of the incident neutron beam to within ~ arcsec is<br />

therefore necessary to record a well resolved diffraction pattern. Our super collimated beam<br />

facilitated measurement of the diffraction pattern from a large-period grating and determination<br />

therefrom of the transverse coherence length of the beam.<br />

A grating of ~ 200 μm period, made by winding a steel wire of 100 μm diameter tightly on a 50x50<br />

mm 2 aluminium frame (inset of Fig.44), was mounted between the monochromator and analyser<br />

for near normal neutron incidence. SUSANS (Super Ultra-Small Angle Neutron Scattering) spectra<br />

recorded with and without the grating in the mount are depicted in Fig.47. The two peaks in the<br />

grating pattern are considerably broadened due to multiple scattering and refraction in the<br />

cylindrical wires, and modulated by clearly resolved diffraction oscillations corresponding to the<br />

grating period [154]. The average peak broadening on transmission through the steel wires in the<br />

grating was least-square fitted to a Gaussian angular profile of standard deviation equal to about<br />

0.41 arcsec, by deconvoluting each peak from that in the no-grating SUSANS pattern. At a<br />

82

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