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PHYS01200804001 Sohrab Abbas - Homi Bhabha National Institute

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III. High precision determination of neutron coherent scattering<br />

In Chapter 5, a proposal for high-precision determination of the neutron coherent scattering length<br />

is described. With this proposal, the neutron coherent scattering length and refractive index for Si<br />

become determinable to within a few parts per million and a few parts per trillion respectively, for<br />

slow neutrons. When such ultra high precision is achieved, the refraction correction at the ambientsample<br />

interface becomes mandatory. We have derived the correct formula for the phase and b c . In<br />

a proof-of-principle measurement, we used a dual non-dispersive sample to measure the largest<br />

non-dispersive phase (911 interference orders) to date, to within 1 ppm and the Si b c value of<br />

4.1479 0.0023 fm was arrived at after adding a correction of 0.009137 fm for ambient air. The<br />

major part of the b c error arose from the 10 μm error in the 18 mm sample thickness. The<br />

correction of –1.01x10 -5 fm to b c due to refraction at air-sample interfaces was too small in<br />

comparison.<br />

A repeat experiment with a better polished sample, to within 1 μm, yielded a Si b c value of<br />

4.15195 0.00011 fm after correcting for all possible sources of errors. Thus, Si b c could be<br />

determined to within 27 parts per million.<br />

By further reducing mechanical vibrations and thermal variations of the IFM set-up and using a<br />

sample polished to better flatness, the proposed ppm precision in bc<br />

determination is achievable.<br />

Rauch et al.’s [126] nondispersive sample configuration afforded precise interferometric<br />

determination of neutron coherent scattering lengths and Ioffe et al. [127] improved the precision<br />

further by an order of magnitude by alternating the sample between the two paths of the<br />

interferometer. We have presented here a dual nondispersive sample which is more nondispersive<br />

than the single “nondispersive” sample by several orders of magnitude. This advantage will be<br />

especially interesting for cold neutron interferometry. The dual sample generates double the phase<br />

122

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