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Empower Gas Chromatography - Waters

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• Method parameters<br />

• Column type<br />

• Operating pressure<br />

• Carrier gas<br />

You might also be asked to provide the firmware versions of your GC instruments.<br />

To check the firmware version on the 5890, 6890, 6890 Plus or the 6890N GC, power on<br />

the instrument. The firmware version is displayed on the LCD.<br />

To check the firmware version on the injector towers and controllers:<br />

1. On the instrument keypad, press Options.<br />

2. Scroll down to Instrument Status and press Enter.<br />

3. Scroll down. The instruments are shown as follows:<br />

• Smplr:model&firmware<br />

• F inj:model&firmware<br />

• B inj:model&firmware<br />

4.1 <strong>Gas</strong> System Troubleshooting<br />

A poorly functioning gas system can cause problems in your <strong>Empower</strong> GC system. Before<br />

proceeding to Section 4.2, check these gas system components.<br />

Regulators<br />

To check the regulators, set the instrument for a constant pressure of 8 psi. Then use the<br />

manifold pressure (on the regulator, not the tank) to adjust the pressure to a constant flow<br />

at 8 psi.<br />

Tanks<br />

Ensure there is adequate pressure in the tanks. The lower the pressure in the tank, the<br />

more erratic the pressure and flow readings. As a rule, the tank should be replaced when<br />

its pressure falls below 100 psi. Follow your standard operating procedure for replacing the<br />

tank.<br />

4<br />

If you are using a split/splitless inlet, consider using the 6890 <strong>Gas</strong> Saver option, which<br />

reduces carrier gas consumption and allows you to reach pressures that may otherwise be<br />

difficult to achieve.<br />

Troubleshooting the GC System 44

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