Accela Pump Hardware Manual

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CAUTION Symbol CAUTION Electric Shock: This instrument uses high voltages that can cause personal injury. Before servicing, shut down the instrument and disconnect the instrument from line power. Keep the top cover on while operating the instrument. Do not remove protective covers from PCBs. Chemical: This instrument might contain hazardous chemicals. Wear gloves when handling toxic, carcinogenic, mutagenic, or corrosive or irritant chemicals. Use approved containers and proper procedures to dispose waste oil. Heat: Before servicing the instrument, allow any heated components to cool. Fire: Use care when operating the system in the presence of flammable gases. Eye Hazard: Eye damage could occur from splattered chemicals or flying particles. Wear safety glasses when handling chemicals or servicing the instrument. General Hazard: A hazard is present that is not included in the above categories. Also, this symbol appears on the instrument to refer the user to instructions in this manual. When the safety of a procedure is questionable, contact your local Technical Support organization for Thermo Fisher Scientific San Jose Products.
Contents Thermo Scientific Accela Pump Hardware Manual ix C Preface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xiii Related Documentation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xiii Safety and Special Notices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xiii Special Precautions for the Accela Pump. . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xiv Good Laboratory Practices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . xv Contacting Us . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . xvii Chapter 1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Functional Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Vacuum Degasser Assembly. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Liquid Displacement Assembly (LDA) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Purge Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Pulse Dampening Assembly. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Dynamic Mixer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 Status LEDs. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Specifications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 Chapter 2 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9 Installation Checklist. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10 Unpacking and Inspecting the Instrument . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Making the Initial Instrument Preparations. . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 Making the Initial Back Panel Connections. . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 Connecting the Power Cable . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 Connecting the USB Cable . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 Connecting the System Interconnect Cable . . . . . . . . . . . . . . . . . . . . . . . . . . 15 Connecting the Low-Pressure Solvent Lines . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 Assembling the Solvent Reservoir Bottles. . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 Installing the Super Flangeless Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 Connecting the Pump to the Autosampler. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22 Powering On for the First Time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24 Chapter 3 Data System Instrument Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25 Adding the Pump to the Xcalibur Instrument Configuration . . . . . . . . . . . . . . 25 Configuring the Signal Polarity for the Accela AS in Xcalibur . . . . . . . . . . . . . . 28 Configuring an Accela Instrument in ChromQuest. . . . . . . . . . . . . . . . . . . . . . 30
Page 1 and 2: Accela Pump Hardware Manual 60157-9
Page 3 and 4: Regulatory Compliance Thermo Fisher
Page 5 and 6: WEEE Compliance This product is req
Page 7: CAUTION Symbol CAUTION VORSICHT ATT
Page 11: Baseline Noise at Low Pressures. .
Page 14 and 15: Preface Special Precautions for the
Page 16 and 17: Preface Solvent Requirement Many ch
Page 19 and 20: Introduction The Accela Pump is a m
Page 21 and 22: The following topics describe the m
Page 23 and 24: Pulse Dampening Assembly 1 Introduc
Page 25 and 26: Status LEDs 1 Introduction Function
Page 27 and 28: Installation This chapter provides
Page 29 and 30: Unpacking and Inspecting the Instru
Page 31 and 32: Making the Initial Back Panel Conne
Page 33 and 34: Connecting the System Interconnect
Page 35 and 36: Connecting the Low-Pressure Solvent
Page 37 and 38: Installing the Super Flangeless Fit
Page 39 and 40: d. Unscrew the swaged fitting and v
Page 41 and 42: Figure 18. Connection between the p
Page 43 and 44: Data System Instrument Configuratio
Page 45 and 46: Figure 20. Thermo Foundation Instru
Page 47 and 48: 3 Data System Instrument Configurat
Page 49 and 50: The Instrument Configuration dialog
Page 51 and 52: 6. Configure the Accela Pump option
Page 53: 3 Data System Instrument Configurat
Page 56 and 57: 4 Preparing the Pump for Operation
Page 58 and 59:
4 Preparing the Pump for Operation
Page 61 and 62:
Diagnostics Use the following proce
Page 63 and 64:
Using ChromQuest to Monitor the Pum
Page 65 and 66:
5 Diagnostics Testing the Pump Prop
Page 67 and 68:
Determining the Delay Volume of the
Page 69:
5 Diagnostics Determining the Delay
Page 72 and 73:
6 Maintenance Flushing the Piston G
Page 74 and 75:
6 Maintenance Minimizing Pump Pulsa
Page 76 and 77:
6 Maintenance Cleaning the LDA Comp
Page 78 and 79:
6 Maintenance Removing the LDA from
Page 80 and 81:
6 Maintenance Removing the LDA from
Page 82 and 83:
6 Maintenance Disassembling the LDA
Page 84 and 85:
6 Maintenance Disassembling the LDA
Page 86 and 87:
6 Maintenance Replacing the Primary
Page 88 and 89:
6 Maintenance Assembling the Liquid
Page 90 and 91:
Page 92 and 93:
Page 94 and 95:
6 Maintenance Connecting the LDA to
Page 96 and 97:
6 Maintenance Servicing the Proport
Page 98 and 99:
6 Maintenance Replacing a Fuse Repl
Page 100 and 101:
7 Troubleshooting General System Tr
Page 102 and 103:
7 Troubleshooting Pump Troubleshoot
Page 104 and 105:
7 Troubleshooting Pump Troubleshoot
Page 106 and 107:
7 Troubleshooting Baseline Noise at
Page 108 and 109:
7 Troubleshooting Irreproducible Re
Page 110 and 111:
8 Accessories and Replacement Parts
Page 112 and 113:
Page 114 and 115:
Page 116 and 117:
Page 119 and 120:
Discontinued Versions of the Accela
Page 121 and 122:
Figure 74. Installing the PEEK film
Page 123:
A Discontinued Versions of the Acce
Page 126 and 127:
Index: E delay volume determining 4
Page 128:
Index: T steel compression ring 20
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