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SRM Method Library Table 27. Compounds For GCMS Positive Electron Ionization (EI) SRM Detection (Organized by Compound Name), continued Compound Vamidothion Nominal Mass 287 — Exact Mass 287.0416 — M Defect 15 15 Precursor Ion (m/z) 145.02 145.02 Product Ion (m/z) 112.02 87.01 Collision Energy (eV) 10 10 Comments — Vinclozolin 285 — — — — 284.9961 — — — — -1 -1 -1 -1 -1 285.00 287.00 285.00 232.00 212.00 212.00 214.00 178.00 110.00 172.00 15 15 15 15 15 — XMC 179 — 179.0947 — 53 53 122.06 122.06 122.06 107.06 10 10 Degrades in GC injector, as all carbamates do Xylylcarb 179 — 179.0947 — 53 53 122.06 107.06 107.06 77.04 10 10 Degrades in GC injector, as all carbamates do Zoxamide 335 — 335.0249 — 7 7 187.01 258.02 159.01 187.01 15 15 — Zoxamide Metabolite — — — — — — 187.00 242.00 159.00 214.00 15 15 — Thermo Scientific Pesticide Analyzer Reference 175
References References 1. Anastassiades, M.; Lehotay, S.; Stajnbaher, D.; Schenck, F.; J. AOAC lnternational 2003, No. 86, 412-431. 2. Carson, Rachel, Silent Spring; Houghton Mifflin: Boston, MA, 1962. 3. Codex Alimentarius. http://www.codexalimentarius.net (accessed March 2009). 4. COMMISSION DECISION of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results (notified under document number C(2002) 3044) 5. Compendium of Pesticide Common Names. http://www.alanwood.net (accessed April 8, 2005). 6. European Commission; Quality Control Procedures for Pesticide Residues Analysis; Document No SANCO/10232/2006; 24/March/2006. 7. Hemmerling, C. Multirückstandsmethoden in der Pestizidanalytik; Lebensmittelchemie, 2007; 61; 4-6. 8. Klein J.; Alder L.; J. AOAC International 2003, No. 86, 1015-1037. 9. PAN Pesticide Database. http://www.pesticideinfo.org. 10. Steiniger, D.; Butler, J.; Phillips, E. Quick Start-Up for a Modified QuEChERS Multi-residue Pesticide Analysis in Lettuce by GC/MSn, Thermo Fisher Scientific Technical Note: 10236, 2008. 11. The Role of Chemistry in History. http://itech.dickinson.edu/chemistry/?page_id=353. 12. Tomlin, C.D.S., Ed.; The Pesticide Manual, 11th ed.; British Crop Protection Council: Farnham, Surrey, UK, 1997. 13. US EPA: About Pesticides. http://134.67.99.207/pesticides/about/index.htm. 14. Ware, G.; Whitacre, D. The Pesticide Book, 6th ed.; Meister Media: Willoughby, OH, 2004. 15. Zimdahl, R. Agriculture’s Ethical Horizon; Academic Press: Burlington, MA, 2006. 176 Pesticide Analyzer Reference Thermo Scientific
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Pesticide Analyzer Reference
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© 2009 Thermo Fisher Scientific In
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Contents 4 Pesticide Analyzer Refer
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Introduction Modern analytical meth
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About This Manual This manual also
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What is a Pesticide? Pesticide Chem
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What is a Pesticide? Table 2. Pesti
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Preparing Samples Preparing Samples
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Preparing Samples Extracting Sample
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Preparing Samples 5. Place the tube
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Preparing Samples Exchanging Solven
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Preparing Samples 5. Centrifuge the
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Setting Up a Method 9. Now you can
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Configuring the GC/MS System for Pe
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List of Pesticide Compounds Table 2
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