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Pesticide Analyzer Reference - writeframeofmind.biz

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Configuring the GC/MS System for <strong>Pesticide</strong> Analysis<br />

TSQ Quantum GC Mass Spectrometer<br />

The TSQ Quantum GC mass spectrometer ships with the recommended configuration for pesticide analysis. It is equipped for easy ion volume exchange.<br />

The method settings for the TSQ Quantum GC will provide good results for all listed compounds. Adjustments can be made if the compound list changes or<br />

additional sensitivity is required.<br />

Table 22. TSQ Quantum GC Mass Spectrometer - Tuning Parameters<br />

AutoTune<br />

Setting<br />

Parameter<br />

Manual tune may be recommended for special mass range enhancements.<br />

Table 23. TSQ Quantum GC Mass Spectrometer - Source Parameters<br />

Setting<br />

Ionization Mode EI<br />

Emission Current 50 uA<br />

Ion Volume<br />

Closed EI Volume<br />

Source Temperature 250 °C<br />

Parameter<br />

Tip Even with a maximum GC oven temperature of 300 °C, a low transfer line temperature works well and prevents active<br />

sites created in a constantly high heated transfer line.<br />

44 <strong>Pesticide</strong> <strong>Analyzer</strong> <strong>Reference</strong> Thermo Scientific

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