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Configuring the GC/MS System for Pesticide Analysis Table 10. SSL Injector Parameters Setting Mode SSL splitless Temperature 250 °C Surge Pressure 250 kPa Parameter If SSL is used, a high-surge pressure is necessary for a quick and sample transfer. Liner Siltek deactivated, splitless (PN 20943-214.5) For easy setup of the SSL option in your TRACE GC Ultra, the following pre-column ready-to-use installation and consumable kits are available. Table 11. Pesticide Method GC Installation Kit for SSL (PN 60181-730) Quantity Kit Component Thermo Fisher Part Number 1 TR-Pesticide II 30 m x 0.25 mm x 0.25 μm with 5 m guard 26RD142F 1 Deactivated Silica Tubing ID 0.53 mm, 1 m (Siltek) 260G401P 2 SilTite SS Union with GLT (0.1-0.25 mm to 0.1-0.53 mm) 290MU498 1 SilTite Ferrules for 0.45-0.53 mm, Pkg of 10 290MF231 1 SSL Straight liner, Siltek Deact., Pkg of 5 453T2121 Thermo Scientific Pesticide Analyzer Reference 37
Configuring the GC/MS System for Pesticide Analysis Table 12. Pesticide Method GC Consumables Kit for SSL (PN 60181-732) Quantity Kit Component Thermo Fisher Part Number 2 TR-Pesticide II 30 m x 0.25 mm x 0.25 μm with 5 m guard 26RD142F 10 Deactivated Silica Tubing ID 0.53 mm, 1 m (Siltek) 260G401P 2 SilTite SS Union with GLT (0.1-0.25 mm to 0.1-0.53 mm) 290MU498 3 SilTite Ferrules for 0.45-0.53 mm, Pkg of 5 290MF231 3 SilTite Ferrules for 0.1-0.25 mm, Pkg of 5 290MF229 5 SSL Straight liner, Siltek Deact., Pkg of 5 453T2121 38 Pesticide Analyzer Reference Thermo Scientific
Page 1 and 2: Pesticide Analyzer Reference
Page 3 and 4: © 2009 Thermo Fisher Scientific In
Page 5 and 6: Contents 4 Pesticide Analyzer Refer
Page 7 and 8: Introduction Modern analytical meth
Page 9 and 10: About This Manual This manual also
Page 11 and 12: What is a Pesticide? Pesticide Chem
Page 13 and 14: What is a Pesticide? Table 2. Pesti
Page 23 and 24: Preparing Samples Preparing Samples
Page 25 and 26: Preparing Samples Extracting Sample
Page 27 and 28: Preparing Samples 5. Place the tube
Page 29 and 30: Preparing Samples Exchanging Solven
Page 31 and 32: Preparing Samples 5. Centrifuge the
Page 33 and 34: Setting Up a Method 9. Now you can
Page 35 and 36: Configuring the GC/MS System for Pe
Page 41: Configuring the GC/MS System for Pe
Page 53 and 54: List of Pesticide Compounds Table 2
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List of Pesticide Compounds Table 2
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SRM Method Library Table 27. Compou
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References References 1. Anastassia
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