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Preparing Samples 3. Cap the tube and vortex it for 30 seconds. 4. Remove the cap and pour the powder reagents poured slowly into the MeCN layer. Tighten the cap securely on the 50 mL extraction tube and vortex for 30 seconds until all of the powder reagents are mixed with the liquid layers. Thermo Scientific Pesticide Analyzer Reference 21
Preparing Samples 5. Place the tube on a mechanical shaker for 5 minutes and centrifuge it for 5 minutes at 3000 rpm. 6. Remove 11 mL of the top MeCN layer and transfer it to a 15 mL clean-up tube. 22 Pesticide Analyzer Reference Thermo Scientific
Page 1 and 2: Pesticide Analyzer Reference
Page 3 and 4: © 2009 Thermo Fisher Scientific In
Page 5 and 6: Contents 4 Pesticide Analyzer Refer
Page 7 and 8: Introduction Modern analytical meth
Page 9 and 10: About This Manual This manual also
Page 11 and 12: What is a Pesticide? Pesticide Chem
Page 13 and 14: What is a Pesticide? Table 2. Pesti
Page 23 and 24: Preparing Samples Preparing Samples
Page 25: Preparing Samples Extracting Sample
Page 29 and 30: Preparing Samples Exchanging Solven
Page 31 and 32: Preparing Samples 5. Centrifuge the
Page 33 and 34: Setting Up a Method 9. Now you can
Page 35 and 36: Configuring the GC/MS System for Pe
Page 53 and 54: List of Pesticide Compounds Table 2
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List of Pesticide Compounds Table 2
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SRM Method Library Table 27. Compou
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References References 1. Anastassia
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