Pesticide Analyzer Reference - writeframeofmind.biz

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Configuring the GC/MS System for Pesticide Analysis TriPlus and AS 3000 II Autosamplers The recommended configuration for the TriPlus autosampler is as follows: • AS (liquid sampling only) or Duo (liquid and headspace sampling) configuration • One primary ambient tray for up to 150 vials of 1, 2, or 2.5 mL • Syringe holder for syringe needles: − − Syringe holder for 50mm needles in 5, 10, 100, 250 μL syringes Syringe holder for 80mm needles in 5, 10, 100, 250 μL syringes • 10 μL syringe (0.47/50/cone) with a fixed needle suitable for split injections (PN 365 00525) • 10 μL syringe (0.63/50/cone), which is compatible with a Merlin valve and suitable for split injections (PN 365 20060) • Standard 5x10 mL washing station The following autosampler upgrade options are recommended for analyzing pesticides: • AI 3000 II autoinjector (PN 25117552) or AS 3000 II autosampler (PN 25117562) • Secondary ambient for TriPlus tray with 151-300 labeling for 1, 2, 2.5 mL vials Thermo Scientific Pesticide Analyzer Reference 41
Configuring the GC/MS System for Pesticide Analysis • Cooled/heated trays for TriPlus: − − Primary cooled/heated tray with 1-96 labeling for 1, 2, 2.5 mL vials Secondary cooled/heated tray with 97-192 labeling for 1, 2, 2.5 mL vials • 2x100 mL washing station • 100 μl syringe (0.63/50/side hole) with removable needle suitable for PTV-LVI (PN 365 20050) • 100 μl syringe (0.63/50/cone) with removable needle suitable for LV-SL (PN 365 00495) The autosampler parameters are described in the following tables. Table 16. TriPlus AS or AS 3000 II Autosampler - Syringe Parameters Setting Needle Length 80 mm for SSL 50 mm for PTV Parameter Table 17. TriPlus AS or AS 3000 II Autosampler - Mode, Injector, Sync Parameters Setting Injection Mode Basic Injector Port Injector A (or B) Start Sync Mode Standard Parameter 42 Pesticide Analyzer Reference Thermo Scientific
Page 1 and 2: Pesticide Analyzer Reference
Page 3 and 4: © 2009 Thermo Fisher Scientific In
Page 5 and 6: Contents 4 Pesticide Analyzer Refer
Page 7 and 8: Introduction Modern analytical meth
Page 9 and 10: About This Manual This manual also
Page 11 and 12: What is a Pesticide? Pesticide Chem
Page 13 and 14: What is a Pesticide? Table 2. Pesti
Page 23 and 24: Preparing Samples Preparing Samples
Page 25 and 26: Preparing Samples Extracting Sample
Page 27 and 28: Preparing Samples 5. Place the tube
Page 29 and 30: Preparing Samples Exchanging Solven
Page 31 and 32: Preparing Samples 5. Centrifuge the
Page 33 and 34: Setting Up a Method 9. Now you can
Page 35 and 36: Configuring the GC/MS System for Pe
Page 45: Configuring the GC/MS System for Pe
Page 53 and 54: List of Pesticide Compounds Table 2
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List of Pesticide Compounds Table 2
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SRM Method Library Table 27. Compou
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References References 1. Anastassia
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