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Pesticide Analyzer Reference - writeframeofmind.biz

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Configuring the GC/MS System for <strong>Pesticide</strong> Analysis<br />

Table 15. Column Parameters<br />

Setting<br />

Supplier<br />

Type<br />

Dimensions<br />

Pre-column<br />

Parameter<br />

Thermo Fisher Scientific<br />

Thermo Scientific TRACE TR-<strong>Pesticide</strong> (PN 26RF142F)<br />

30 m x 0.25 mm ID x 0.25 μm film with 5 m integrated guard column<br />

Tip Use the integrated guard column in the MS transfer line. The empty guard column in the transfer lines keeps the<br />

background low and guarantees optimum chromatographic integrity.<br />

1 m x 0.53 mm ID (optional) for easy exchange with dirty matrix samples<br />

For matrix samples (e.g. from QuEChERS sample prep), use an empty pre-column of Siltec deactivated silica tubing<br />

(PN 260G401P).<br />

Connectors SilTite Mini-Unions (PN 073550)<br />

Tip Mini-unions of low thermal mass are a durable and easy to handle connection. Check for leaks regularly if glass quick fit<br />

pieces are used.<br />

40 <strong>Pesticide</strong> <strong>Analyzer</strong> <strong>Reference</strong> Thermo Scientific

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