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Abstracts of the Academy of Dental Materials Annual ... - IsiRed

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e8 dental materials 26S (2010) e1–e84<br />

in vivo studies are needed to clarify <strong>the</strong> clinical performance<br />

<strong>of</strong> simplified adhesives.<br />

doi:10.1016/j.dental.2010.08.022<br />

15<br />

Effect <strong>of</strong> chlorhexidine on 6-months bond strength <strong>of</strong> resinglass-modified-ionomer<br />

to dentin<br />

E. Dursun, J.P. Attal<br />

University <strong>of</strong> Paris Descartes, France<br />

Objectives: The purpose <strong>of</strong> this study was to investigate<br />

<strong>the</strong> effect <strong>of</strong> chlorhexidine (CHX) on dentin bond strength <strong>of</strong><br />

resin-modified glass-ionomer (RMGI) after 24 h and 6 months<br />

<strong>of</strong> water storage.<br />

<strong>Materials</strong> and methods: 60 human teeth with a flat surface<br />

<strong>of</strong> dentin were embedded in blocks <strong>of</strong> resin. 60 cylinders<br />

<strong>of</strong> RMGI (Fuji LCII ® (GC)) were bonded on 60 teeth following<br />

various modalities: 30 after polyalkenoic acid (ac pol) treatment,<br />

30 after polyalkenoic acid treatment and an application<br />

<strong>of</strong> 0.05% chlorhexidine (CHX). One subgroup (n = 15) was tested<br />

after 24 h in water at 37 ◦ C and <strong>the</strong> o<strong>the</strong>r subgroup (n = 15)<br />

after 6-month storage in water. A shear bond strength (SBS)<br />

test was performed. The data (in MPa) were analyzed with<br />

ANOVA and Tukey tests (p < 0.05). The type <strong>of</strong> bond failure<br />

(mixed/adhesive/cohesive) was noted and analyzed with a chisquare<br />

test (p < 0.05).<br />

Results:<br />

Dentin treatment, material and time Dentin SBS (MPa)<br />

Ac Pol + RMGI 24 h 8 ± 1 (a)<br />

AcPol+Chx+RMGI24h 9 ± 3 (a)<br />

Ac Poly + RMGI 6 months 12 ± 4 (b)<br />

Ac Pol + Chx + RMGI 6 months 9 ± 3 (a)<br />

Letters in paren<strong>the</strong>ses = homogeneous subsets.<br />

After 24 h, <strong>the</strong>re were no significant differences on dentin<br />

SBS <strong>of</strong> RMGI with or without application <strong>of</strong> chlorhexidine.<br />

After 6 months, <strong>the</strong> dentin SBS increased in <strong>the</strong> samples that<br />

had not been treated with chlorhexidine, and did not increase<br />

in those that had been treated with chlorhexidine.<br />

No significant differences in debonding locations were<br />

found between <strong>the</strong> various groups tested with 100% <strong>of</strong> adhesive<br />

failures.<br />

Conclusions: Chlorhexidine application does not seem to<br />

disturb <strong>the</strong> dentin SBS <strong>of</strong> RMGI after 24 h. However, <strong>the</strong> dentin<br />

SBS <strong>of</strong> RMGI seems to increase after 6 months and application<br />

<strong>of</strong> chlorhexidine may inhibit this increase.<br />

doi:10.1016/j.dental.2010.08.023<br />

16<br />

Bonding effectiveness <strong>of</strong> all-in-one adhesives<br />

H.M. El-Damanhoury 1 , N.A. El-Sahn 2 , A.N. Habib 2 , K.B.<br />

Moore 3<br />

1 University <strong>of</strong> Sharjah, UAE<br />

2 Cairo University, Egypt<br />

3 Indiana University, IN, USA<br />

Objectives: To evaluate <strong>the</strong> bonding effectiveness <strong>of</strong><br />

six all-in-one adhesives to dentin by testing micro-tensile<br />

bond strength (�-TBS) and micrographic analysis <strong>of</strong> <strong>the</strong><br />

resin/adhesive interface.<br />

<strong>Materials</strong> and methods: Flat occlusal dentin was exposed<br />

in 128 extracted human molars. Teeth were equally divided<br />

into 16 groups (8 teeth each). Two groups were randomly<br />

assigned for each all-in-one adhesive and controls: Clearfil<br />

S3 (S3-kuraray); G-Bond (GB-GC dental); iBond (IB-Heraeus<br />

Kulzer); Xeno V (XB-Dentsply); Optibond All-in-one (OB-Kerr)<br />

and Adper Easy Bond (AEB-3M ESPE). Adper ScotchBond SE<br />

(ASE-3M ESPE) was used as two-bottle self-etch control and<br />

Adper Single Bond Plus (SB-3M ESPE) as etch-and-rinse control.<br />

Specimens were restored with Filtek Z250 Composite (3M<br />

ESPE). One group for each material was <strong>the</strong>rmocycled (TC). �-<br />

TBS to dentin was measured in a universal testing machine.<br />

Mode <strong>of</strong> failure <strong>of</strong> debonded beams was examined under SEM.<br />

Micrographic analysis <strong>of</strong> <strong>the</strong> bonded interface <strong>of</strong> demineralized/deproteinized<br />

samples was done using SEM. All data were<br />

analyzed by one-way ANOVA and multiple comparisons was<br />

done using Tukey’s test (p < 0.05).<br />

Results: SB presented <strong>the</strong> highest �-TBS (58.17 ± 10.1 MPa)<br />

and a reduction <strong>of</strong> 25.12% after TC, with resin tags >40 �m,<br />

while GB (53.40 ± 9.6 MPa) showed <strong>the</strong> least reduction in �-TBS<br />

after TC (14.71%). OB (48.40 ± 8.0 MPa) exhibited <strong>the</strong> highest<br />

reduction in �-TBS (31.16%) and resin tags >40 �m. XB presented<br />

<strong>the</strong> lowest �-TBS (25.88 ± 5.5 MPa) with reduction <strong>of</strong><br />

22.06% after TC. All-in-one adhesive showed mixed type <strong>of</strong><br />

failure, except for GB and XB, which failed cohesively within<br />

<strong>the</strong> adhesive layer.<br />

Conclusions: Etch and rinse adhesive systems remain as<br />

<strong>the</strong> gold standard for bonding to dentin, meanwhile some <strong>of</strong><br />

<strong>the</strong> all-in-one adhesives demonstrate promising results concerning<br />

<strong>the</strong> bond strength and durability after <strong>the</strong>rmocyclying.<br />

There is no direct relation between depth <strong>of</strong> infiltration in<br />

dentin and bond strength <strong>of</strong> adhesives.<br />

doi:10.1016/j.dental.2010.08.024<br />

17<br />

Influence <strong>of</strong> surface pretreatment on <strong>the</strong> short term bond<br />

strength <strong>of</strong> composite resin to a zirconia-based material<br />

G. Fazi, A. Vichi, M. Ferrari<br />

University <strong>of</strong> Siena, Italy<br />

Objectives: The purpose <strong>of</strong> <strong>the</strong> present study was to evaluate<br />

<strong>the</strong> influence <strong>of</strong> sandblasting zirconia before and after<br />

sintering on <strong>the</strong> bond strength between a zirconia core and a<br />

composite resin material.

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