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GC COLUMNS | PACKED/MICROPACKED COLUMNSSpecialty Packed ColumnsAromatics AnalysisfreeliteratureResolve Benzeneand Toluene inSpark Ignition FuelsContaining EthanolDownload your freecopy fromwww.restek.comlit. cat.# 580227D3606 Application Column (2 column set)• Complete separation of ethanol and benzene, with a resolution value > 3.00.• Accurate quantification of benzene and toluene.• Fully conditioned two column set—ready to use out of the box.• A chromatogram is provided with each column set demonstrating conformance tothe revised ASTM method.Conforms to the specifications established in ASTM method D3606-07 for the quantitationof benzene and toluene in spark ignition fuel containing ethanol.Description cat.#* priceD3606 Application Column (2 column set)**Column 1: 6' (1.8m), 1 /8" OD, 2.0mm ID, nonpolar Rtx-1Column 2: 16' (4.9m), 1 /8" OD, 2.0mm ID, proprietary packing material 83606-*Please add column instrument configuration suffix number to cat.# when ordering. See page 143.**The column set is designed to accommodate both valve injection and/or syringe injection. Column 1 isconfigured with a 2" inlet void to facilitate on-column injection. The inlet is identified on both column 1 andcolumn 2. Note: The inlet of column 2 is identified for proper orientation for connection to the valve.Gasoline containing ethanol on a D3606 Application Column set.1. ethanol2. benzene3. 2-butanol4. tolueneGC_PC01079Column: D3606 Application Column (2 column set, cat.# 83606-800)Column 1: nonpolar Rtx ® -1, 6' (1.8m), 1 /8" OD, 2.0mm IDColumn 2: proprietary packing material, 16' (4.9m), 1 /8" OD, 2.0mm IDSample: 1.5µL gasoline with internal standardInj.: 200°CBackflush: 3 min.Carrier gas: helium, constant flowFlow rate: 20mL/min.Oven temp.: 135°C, isothermalDet.: TCD @ 200°CChromatogram courtesy of Boguslaw Dudek, Conoco Phillips, Linden, NJ.128 www.restek.comWebsite : www.chromtech.net.au E-mail : info@chromtech.net.au TelNo : 03 9762 2034 . . . in AUSTRALIA Mar 2011
Light Hydrocarbon AnalysisSpecial Columns for Unsaturated Light Hydrocarbons• Faster separations of C1 to C4 hydrocarbons.• Res-Sil® packing replaces Porasil materials.n-Octane on Res-Sil® C Packed ColumnThis packed column has unique selectivity for resolving unsaturatedlight hydrocarbons (Figure 1).OPN on Res-Sil® C Packed ColumnThis column separates the light hydrocarbons, and baselineresolves cis-2-butene from 1,3-butadiene (Figure 2).2abc Refinery Gas Column SetThis 3-column set is finely tuned to resolve light hydrocarbons.When used in the proper valving system, it will elute C5+ hydrocarbonsahead of C1 through C4 hydrocarbons. (Figure 3)Description cat.#* pricen-Octane on Res-Sil C, 80/100 (20', 2.0mm ID,1/8" Silcosmooth OD) 80436-OPN on Res-Sil C, 80/100 (12', 2.0mm ID, 1 /8" Silcosmooth OD) 80437-2abc Refinery Gas Column Set (3 column set)** 88000-*Please add column instrument configuration suffix number to cat.# whenordering. See page 143.**This column set is for a valving system; therefore, packing material is filled toends of <strong>columns</strong>.Figure 1 n-Octane on Res-Sil® C packing has uniqueselectivity for unsaturated light hydrocarbons.142,3 5 78for more info6min. 0 2 4 691011121. methane2. ethane3. ethylene4. acetylene5. propane6. propylene7. isobutane8. n-butane9. 1-butene10. pentane11. isobutylene12. 1,3-butadiene13. 1-pentene14. trans-2-pentene15. cis-2-pentene16. 2-methylbutene-2n-octane 80/100 Res-Sil ® C20', 1 /8" OD x 2mm ID, SilcoSmooth ® tubing (cat. # 80436)Oven temp.: 60°CInj. temp.: 150°CDet. temp: 150°C FIDFlow rate: 30mL/min. HeSample: refinery gas C1-C5Sample size: 20µLSee page 135 for more information on Res-Sil® packing materials.1314158 10 12GC_PC0037216GC COLUMNS | PACKED/MICROPACKED COLUMNSSpecialty Packed ColumnsFigure 2 OPN on Res-Sil® C packing has uniqueselectivity for cis-2-butene and 1,3-butadiene.Retention1 2 4 536789101112Indices1. methane 1002. ethane/ethylene 2003. acetylene 2604. propane 3005. propylene 3216. propadiene 3457. isobutane 3868. butane 4009. 1-butene 42210. isobutylene/trans-2-butene 43411. cis-2-butene 44312. 1,3-butadiene 45413. isopentane 48814. pentane/3-methyl-1-butene 50315. 1-pentene 52216. trans-2-pentene 53317. cis-2-pentene 54018. 2-methyl-2-butene 5491314min. 0 5 10cis-2-butene/1,3-butadieneresolved to baseline15 16 17 18OPN on Res-Sil ® C, 80/100 mesh, 12' x 2mm ID x 1 /8" OD in SilcoSmooth ®tubing (cat.# 80437). 20µL on-column injection of refinery gas.Concentration: 0.1-6 absolute mole %Oven temp.: 50°CInj. & det. temp.: 200°CCarrier gas: heliumFlow rate: 30mL/minReference standard courtesy of AC Analytical Controls, Bensalem, PA.GC_PC00373Figure 3 Refinery gas calibration standard on a Restekrefinery gas packed column set.3,4 5216789101112131415161. C5=C6+2. methane3. ethane4. ethylene5. propane6. acetylene7. propylene8. cyclopropane9. isobutane10. propadiene11. n-butane12. 1-butene13. isobutene14. trans-2-butene15. cis-2-butene16. 1,3-butadiene17. isopentane18. n-pentanemin. 10 20 30 GC_PC003742abc Refinery Gas Column Set (cat.# 88000-875) (3 column set)Oven temp.: 60°CInj. temp.: 150°CDet. temp: 150°C FIDFlow rate: 30mL/min., heliumSample: refinery gasSample size: 1cc1718www.restek.com 129Website : www.chromtech.net.au E-mail : info@chromtech.net.au TelNo : 03 9762 2034 . . . in AUSTRALIA Mar 2011
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GC COLUMNSDetailed Table of Content
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GC COLUMNS | CAPILLARY COLUMNSSelec
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Columns by Application/IndustryRtx-
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GC COLUMNS | CAPILLARY COLUMNSGuard
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GC COLUMNS | CAPILLARY COLUMNSFused
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GC COLUMNS | CAPILLARY COLUMNSFused
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3-IN-1 TECHNOLOGYHighest Inertness
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GC COLUMNS | HIGH-PERFORMANCE RXI C
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Rxi®-1ms Columns (fused silica)(no
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GC COLUMNS | HIGH-PERFORMANCE RXI C
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NEW!GC COLUMNS | HIGH-PERFORMANCE R
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GC COLUMNS | GENERAL PURPOSE COLUMN
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Rt®-2330 Columns (fused silica)(hi
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GCxGC Second Dimension Selectivity
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Basic Compounds AnalysisRtx®-Volat
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Basic Compounds AnalysisRtx®-35 Am
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Acidic Compounds AnalysisStabilwax
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cis/trans FAMEsRt®-2560 Column (fu
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Flavor & Fragrance Compounds Analys
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PAHs in Foods AnalysisRxi®-17Sil M
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Detailed Hydrocarbon Analysis (DHA)
Page 61 and 62: Simulated Distillation (C5-C44) Ana
Page 63 and 64: GC COLUMNS | APPLICATION-SPECIFIC C
Page 65 and 66: Biodiesel Fuels AnalysisMXT®-Biodi
Page 67 and 68: Organic Volatile Impurities (OVI) A
Page 69 and 70: Organic Volatile Impurities (OVI) A
Page 71 and 72: Semivolatiles AnalysisRxi®-5Sil MS
Page 73 and 74: Chlorinated Pesticides AnalysisGC C
Page 75 and 76: Organophosphorus Pesticides Analysi
Page 77 and 78: PCB Congeners AnalysisRtx®-PCB Col
Page 79 and 80: Dioxin & Furan Congeners AnalysisRx
Page 81 and 82: Polycyclic Aromatic Hydrocarbon (PA
Page 83 and 84: Mineral Oil AnalysisRtx®-Mineral O
Page 85 and 86: Volatile Organics AnalysisRtx®-VRX
Page 87 and 88: Volatile Organics AnalysisRxi®-624
Page 89 and 90: Next Generation GC PLOT Columns•
Page 91 and 92: GC COLUMNS | PLOT COLUMNSPLOT Colum
Page 93 and 94: GC COLUMNS | PLOT COLUMNSMolecular
Page 95 and 96: GC COLUMNS | PLOT COLUMNSPorous Pol
Page 97 and 98: What is an MXT® column?MXT® colum
Page 99 and 100: GC COLUMNS | METAL (MXT®) CAPILLAR
Page 101 and 102: GC COLUMNS | METAL (MXT®) CAPILLAR
Page 103 and 104: Triglycerides in Foods AnalysisMXT
Page 105 and 106: Volatile Organics AnalysisMXT®-502
Page 107 and 108: Bonded Stationary PhasesWe combined
Page 109 and 110: Packed Column TubingRestek offers a
Page 111: GC COLUMNS | PACKED/MICROPACKED COL
Page 115 and 116: Sulfur AnalysisRt®-XLSulfur Packed
Page 117 and 118: Packed Column Inlet Adaptor Kits•
Page 119 and 120: Res-Sil® Packing Materials• Uniq
Page 121 and 122: GC COLUMNS | PACKED/MICROPACKED COL
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Page 125 and 126: Custom Packed ColumnsTo order, spec
Page 127: GC COLUMNS | PACKED/MICROPACKED COL
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