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GC COLUMNS | APPLICATION-SPECIFIC COLUMNSEnvironmentalTable of Contents forGC Chromatogramssee page 542Brominated Flame Retardants AnalysisRtx®-1614 Columns (fused silica)(5% phenyl methyl)• Optimized for PBDE analysis by EPA Method 1614.• Short column option resolves BDE-209 3 times faster, with less thermal breakdown.• Unique deactivation gives higher BDE-209 response, compared to DB-5HT<strong>columns</strong>, for greater analytical sensitivity.• Exceeds EPA Method 1614 resolution criteria for BDE-49 and BDE-71.ID df temp. limits 15-Meter 30-Meter0.25mm 0.10µm -60 to 330/360°C 10296 10295Brominated flame retardants on an Rtx®-1614 column.Get results 3 timesfaster with a shortcolumn method!GC_EV01025Column: Rtx ® -1614, 15m, 0.25mm ID, 0.10µm (cat.# 10296)Sample: 100-300ppb PBDE PAR Solution (cat.# EO-5113, CambridgeIsotope Laboratories Inc.), 500ppb decabromodiphenyl ether(cat.# BDE-209, Wellington Laboratories)Inj.:1µL splitless (hold 1 min.), 4mm cyclo double gooseneckliner (cat.# 20896)Inj. temp.: 340°CCarrier gas: helium, constant flowLinear velocity: 60cm/sec. @ 120°COven temp.: 120°C (hold 1 min.) to 275°C @ 15°C/min. to 300°C @5°C/min. (hold 5 min.)Detector temp.: µ-ECD @ 345°CGreat peak shapefor BDE 209!1. BDE-102. BDE-73. BDE-84. BDE-115. BDE-126. BDE-137. BDE-158. BDE-309. BDE-3210. BDE-1711. BDE-2512. BDE-2813. BDE-3314. BDE-3515. BDE-3716. BDE-7517. BDE-4918. BDE-7119. BDE-4720. BDE-6621. BDE-7722. BDE-10023. BDE-11924. BDE-9925. BDE-11626. BDE-11827. BDE-8528. BDE-15529. BDE-12630. BDE-15431. BDE-15332. BDE-13833. BDE-16634. BDE-18335. BDE-18136. BDE-19037. BDE-20838. BDE-20739. BDE-20640. BDE-20992 www.restek.comWebsite : www.chromtech.net.au E-mail : info@chromtech.net.au TelNo : 03 9762 2034 . . . in AUSTRALIA Mar 2011

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