23 - Curriculum Development Centre, Kalamassery

SUBJECT TITLE : APPLIED CHEMISTRY LABSUBJECT CODE : PL 103PERIODS/WEEK : 2PERIODS/YEAR : 64TIME SCHEDULEUNIT TOPIC PERIODSI Introduction to volumetric analysis 6II Acidimetry and Alkalimetry 16III Permanganometry 16IV Iodimetry 10V Gravimetry 10VI Identification of simple organic compounds 6-----------Total 64====CONTENT DETAILS OF LABORATORY WORK IN APPLIED CHEMISTRY LAB1.0 Introduction to volumetric analysis1.1 Equivalent weights of compounds1.2 Concentration of solutions – Normality and molarity1.3 Preparation of standard solutions1.4 Principles of volumetric analysis1.5 Apparatus used the volumetric analysis2.0 Acidimetry and Alkalimetry2.1 Standardisation of NaOH using standard HCl2.2 Standardisation of HCl using standard NaOH Solution2.3 Estimation of KOH using standard Na 2 CO 3 Solution2.4 Estimation of H 2 SO 4 using standard Na 2 CO 3 solution2.5 Estimation of K 2 CO 3 using standard Na 2 CO 3 solution3.0 Permanganometry3.1 Standardisation KMnO 4 using Mohr’s salt solution3.2 Estimation of Ferrous iron using standard oxalic acid3.3 Estimation of NaOH using standard KMnO 4 solutions3.4 Estimation of calcium using standard oxalic acid solution4.0 Iodimetry4.1 Standardisation of Sodiumthiosulphate using standard pot dichromate solution4.2 Estimation of potassium dichromate4.3 Estimation of copper5.0 Gravimetry5.1 Estimation of Barium as BaSO 45.2 Estimation of Fe as ferric hydroxide6.0 Identification of simple organic compounds6.1 Reaction of Alcohol, Aldehyde, Acids, Esters, Amines etc6.2 Detection of elements like nitrogen, sulphur, halogens in organic compoundsREFERENCE BOOKS1. Practical Chemistry for B.Sc main – A.O. Thomas55