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General Catalogue Chemistry - BECO Internacional LTDA.

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667 320<br />

Dewar flask<br />

Silver finish, with protective casing, for<br />

maintaining a constant temperature, e.g. in<br />

calorific experiments.<br />

Capacity: 500 ml<br />

Diameter: 70 mm<br />

Height: 210 mm<br />

Weight: 1.0 kg<br />

667 319<br />

Dewar flask<br />

Silver finish, with protective casing,<br />

for experiments using the magnetic stirrer.<br />

Capacity: 500 ml<br />

Diameter: 70 mm<br />

Height: 210 mm<br />

Weight: 1.0 kg<br />

667 321<br />

Plastic lid<br />

With stirrer and borehole for a thermometer, fits<br />

the Dewar flasks (> 667 320 and<br />

> 667 319). The lid serves as a holder for a<br />

thermometer and reduces the exchange of<br />

heat energy with the surroundings.<br />

Diameter: 85 mm<br />

Weight: 0.2 kg<br />

All that is needed to conduct simple experiments<br />

in calorimetry is an insulating flask (Dewar<br />

flask) which reduces to a minimum the exchange<br />

of thermal energy with the environment,<br />

a plastic insert with a lid that holds the thermometer<br />

and the stirrer used for manual agitation.<br />

A magnetic stirrer may also be employed when<br />

using the special, flat-bottomed version of the<br />

Dewar flask.<br />

Application examples for a calorimeter which is<br />

assembled using > 667 321 along with<br />

> 667 319 or > 667 320 include:<br />

• Measuring the heat of solution<br />

• Measuring the heat of neutralization<br />

• Measuring the heat of reaction in solutions<br />

Stoichiometry<br />

The subject of stoichiometry deals with the<br />

quantitative description of chemical reactions.<br />

It is based on the realization that chemical elements<br />

will react one with another only in certain,<br />

constant proportions (law of constant proportions).<br />

Consequently the final product of the<br />

reaction - the chemical compound - always consists<br />

of a constant share of the initial substances,<br />

regardless of the quantities which were available.<br />

Based on this fundamental law, conclusions can<br />

be drawn regarding the relative masses of the<br />

reactants involved, allowing us, for instance,<br />

to calculate the yield factor for a reaction.<br />

One of the elementary experiments in stoichiometry<br />

is the quantitative synthesis of water, the<br />

complement to the water analysis experiments<br />

using Hofmann's electrolysis setup.<br />

This experiment demonstrates that the reactants,<br />

hydrogen and oxygen, join in a precise stoichiometric<br />

ratio of 2:1 to form water (H2O). Gravimetric<br />

examination of the water thus formed<br />

allows us to derive information on the molar<br />

mass of water.<br />

The reaction vessel for stoichiometry also permits<br />

the determination of the relative atomic<br />

mass and the valence of metals.<br />

668 802<br />

<strong>Chemistry</strong> demonstration experiments<br />

“<strong>General</strong> chemistry”<br />

216 pages, DIN A 4<br />

Demonstration experiments from the area of<br />

general chemistry based on the <strong>Chemistry</strong><br />

Panel System. The equipement list of the<br />

experiments also takes account of conventional<br />

stand material<br />

667 320<br />

664 097<br />

Stoichiometric reaction vessel<br />

Metals react with water or acids in the stoichiometric<br />

reaction vessel, developing hydrogen<br />

while doing so. The atomic weight and the chemical<br />

valence of the metal can be determined<br />

on the basis of the volume of the gas collected<br />

in a gas syringe and the preweighed metal<br />

mass. The lower portion of the vessel is first<br />

filled with water or acid, the vessel is then<br />

purged with a non-reactive gas (N 2 ) and, after a<br />

gas syringe has been attached to the reaction<br />

vessel, the reaction is started by lowering the<br />

plunger. The reaction then proceeds calmly,<br />

without flames being produced.<br />

Glass with lateral connection (GL 18) and<br />

three-way stopcock at the lower end<br />

Height: 225 mm<br />

Diameter: 60 mm<br />

Weight: 0.22 kg<br />

analysis methods<br />

Calorimetry<br />

667 321<br />

664 097<br />

LEYBOLD DIDACTIC · GENERAL CATALOGUE CHEMISTRY<br />

71

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