Reaction vessels for vacuum and pressure

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20 Reaction vessels for vacuum and pressure Reaction vessels for vacuum and pressure, 30 litre nominal capacity N4 N5 N3 Internal height Internal diameter Fitted with stirrehead type 10312.00 N6 N2 ∅404 N1 425 mm 314 mm 855 443 N9 410 N7 N8 N1 Port, central, ∅48.5, with stirrerhead N2 Sightglass, DN48 N3 Port, M24x1.5, with pressure gauge N4 Port, M33x1.5, with plug N5 Port, M24x1.5, with excess pressure valve N6 Illumination glass, DN30 N7 Port, M24x1.5, with plug N8 Port, M33x1.5, with plug N9 Port, M24x1.5, with thermometer pocket PTFE Klingersil Weight Volume Pressure Heating jacket Cat. no. without heating jacket 10161.01 10161.04 81 kg 30.5 ltr 6 Bar Volume Pressure Cat. no. with heating jacket 10163.01 10163.04 87 kg 30.5 ltr 6 Bar 4.3 ltr 3 Bar ∅640 M30x1.5 1055
All information is for the standard vessel, gaskets and glasses are consumables Reaction vessels for vacuum and pressure Components of standard vessel – PTFE gaskets Description Vessel with Size No. Cat. no. Heating jacket 30.5 ltr 1 10163.01 Lid gasket ∅ 343 x ∅ 325 x 2 1 20345.31 Bolts M16 x 80 A2-70 15 Nuts M16 A2-70 15 Washers ∅ 17 A2 15 Drain plug M24 x 1,5 1 10334.00 Drain plug gasket ∅ 34 x ∅ 24 x 1 1 20337.21 Stirrerhead gasket ∅ 56 x ∅ 49 x 1 1 20337.41 Stirrerhead 1 10312.00 ‘O’ ring ∅ 15 x 4 2 20312.04 Double universal joint 8 x 8 1 20441.00 Shield 1 20447.00 Anchor stirrer 1 10315.70 Thermometer pocket, closed 1 20465.27 Gasket for M24 ports ∅ 30 x ∅ 24 x 1 4 20337.11 Adaptor M24 - 1/2" BSP 1 20461.11 Gasket, 1/2" BSP ∅ 18 x ∅ 12 x 1 1 20336.51 Excess pressure valve 6 Bar, 1/2" BSP 1 21453.06 Adaptor M24 - 1/4" BSP 1 20461.21 Gasket, 1/4" BSP ∅ 11 x ∅ 6 x 1,5 1 20336.13 Pressure gauge –1 to 5 Bar 1 20460.00 Plug, M24 ports M24 x 1,5 1 20463.21 Plug, M33 ports M33 x 1,5 2 20463.31 Gasket for M33 ports ∅ 40 x ∅ 34 x 2 2 20337.31 Illumination glass, DN30 ∅ 40 x 10 1 20466.47 Flange, DN30 1 20467.03 Gasket for DN30 flange ∅ 40 x ∅ 30 x 1 2 20336.71 Sightglass, DN48 ∅ 60 x 10 1 20466.67 Flange, DN48 1 20467.05 Gasket for DN48 flange ∅ 60 x ∅ 50 x 1 2 20337.61 Custom design with a second stirrerhead in the lid Klingersil gaskets The drawing shows a 5 litre vessel with a centrally mounted 16 Nm magnetic stirrerhead and a sloping mechanically sealed stirrerhead to one side. The magnetic stirrerhead is fitted with an anchor stirrer and the lateral stirrerhead is fitted with a dispersion disk. Both stirrers can be used simultaneously. Description Size Cat. no. Lid gasket ∅ 343 x ∅ 325 x 2 20345.34 Drain plug gasket ∅ 34 x ∅ 24 x 2 20337.24 Gasket for M24 ports ∅ 30 x ∅ 24 x 2 20337.14 Gasket for M33 ports ∅ 40 x ∅ 34 x 2 20337.34 Gasket, 1/2" BSP ∅ 18 x ∅ 12 x 2 20336.54 Gasket for DN30 flange ∅ 40 x ∅ 30 x 2 20336.74 Gasket for DN48 flange ∅ 60 x ∅ 50 x 2 20336.64 Stirrerhead gasket ∅ 56 x ∅ 49 x 1 20337.44 Gasket sets, options and accessories Description Size Cat. no. Set of 14 gaskets PTFE 20365.30 Set of 14 gaskets Klingersil 20360.30 Mechanically sealed stirrerhead M48 x 1,5 10309.50 Magnetic stirrerhead M48 x 1,5 10313.00 Double universal joint, stainless steel 8 x 8 20441.11 Vessel insulation 10163.90 Drain with ball valve* 15 ... 50 Drain valve, straight outlet M24 x 1,5 10333.1* Drain valve, lateral outlet M24 x 1,5 10335.0* Pt100 thermometer for closed pocket EL420 Thermometer holders 52009.50 - open with dip tube 20465.41 - open without dip tube 20465.51 Pt100 direct immersion thermometer EL375 52009.30 Bottom Pt100 thermometer mounted in vessel bottom* EL50 15009.00 Vycor glass, DN30 ∅ 40 x 10 20466.49 Vycor glass, DN38 ∅ 60 x 10 20466.69 * available only as original equipment The view from above the vessel shows the constrained layout. 21
Page 1: Reaction vessels for pressure and v
Page 4 and 5: 2 54470 Bernkastel-Kues Deliveries
Page 6 and 7: Dimensions 4 Reaction vessels for v
Page 8 and 9: 6 Cylindrical-conical pressure vess
Page 10 and 11: 8 Reaction vessels for vacuum and p
Page 12 and 13: PTFE Klingersil Weight Volume Press
Page 14 and 15: PTFE Klingersil Weight Volume Pessu
Page 20 and 21: 18 Reaction vessels for vacuum and
Page 26 and 27: 24 10 litre pressure vessel, rated
Page 30 and 31: 28 Custom and special purpose vesse
Page 32 and 33: 30 Reactor system with lifting stag
Page 38 and 39: 36 Accessories Fittings and spare p
Page 40 and 41: 38 Accessories Drain valves and acc
Page 42 and 43: Analogue pressure gauge Connection
Page 44 and 45: 42 Accessories Safety devices for v
Page 46 and 47: 44 Accessories Thermometers, thermo
Page 48 and 49: 46 Accessories Adaptors for ports i
Page 50 and 51: Lid gaskets for vessels 48 Accessor
Page 52 and 53: 50 Lifting jacks for vessels Fixed
Page 54 and 55: 52 Stirrer drives Stirrer drive wit
Page 56 and 57: 54 Torque measurement Torque measur
Page 58 and 59: 56 Stirrerheads ‘O’ and oil fil
Page 60 and 61: 58 Stirrerheads ’O’ ring sealed
Page 62 and 63: 60 Stirrerheads ’O’ ring sealed
Page 64 and 65: 62 Stirrerheads Mechanically sealed
Page 70 and 71: Stirrerhead Cat. no. Fixing B29 M24
Page 72 and 73:
Stirrerhead Cat. no. Fixing B45 M33
Page 74 and 75:
Stirrerhead Cat. no. Fixing M33 x 1
Page 76 and 77:
Stirrerheads Magnetically coupled s
Page 78 and 79:
76 Stirrer drive couplings and shie
Page 80 and 81:
78 Stirrers Anchor stirrers and sti
Page 82 and 83:
80 Stirrers Impeller stirrers and P
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82 Stirrers Sloped anchor stirrers
Page 86 and 87:
84 Conical joint stirrerheads Conic
Page 88 and 89:
86 Conical joint stirrerheads Stirr
Page 90 and 91:
88 Thermostats and accessories Conn
Page 92 and 93:
90 Thermostats and accessories Base
Page 94 and 95:
Cat. no. Male M18 x 1.5 Female M16
Page 96 and 97:
94 Thermostats and accessories Acce
Page 98 and 99:
96 Thermostats and accessories Spar
Page 100 and 101:
98 Thermostats and accessories Ther
Page 102 and 103:
100 Thermostats and accessories 9 k
Page 104 and 105:
102 Glass Flask Holders Universal h
Page 106 and 107:
104 Raction vessel built to GMP req
Page 108 and 109:
106 General information Materials:
Page 110 and 111:
108 Index T Tachometer ............
Page 112 and 113:
110 Transportable turnkey plant, ex
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Reaction vessels for vacuum and pressure

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