NNR IN RAPIDLY ROTATED METALS By - Nottingham eTheses ...
NNR IN RAPIDLY ROTATED METALS By - Nottingham eTheses ...
NNR IN RAPIDLY ROTATED METALS By - Nottingham eTheses ...
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-103-<br />
results obtained at a temperature of 301 K in an applied field<br />
of 1.45 T are listed in Table 7.2. The errors quoted refer only<br />
TABLE 7.2. EXPERIMENTAL ZEEMAN AND DIPOLAR RELAXATION TIMES<br />
POWDER SAMPLE<br />
TjZ TID a<br />
ms ms<br />
99.995% pure sprayed (a) 6.12 ± 0.04 2.96 ± 0.05 2.07 ± 0.05<br />
99.999% pure filed (c) 6.09 ± 0.04 2.88 ± 0.06 2.12 ± 0.06<br />
99.5% pure sprayed (b) 6.04 ± 0.03 2.70 ± 0.05 2.24 ± 0.05<br />
to the spread of values in each case and not to any possible instrun-<br />
ental error or error in processing the data. The measurements were<br />
recorded within a short space of time of each other and an accurate<br />
comparison of the Tlz values could be made. Although the error<br />
limits rule out any definite conclusion, the values quoted would<br />
seem to indicate that the pure filed powder (c) had a slightly<br />
shorter Tlz than that prepared by spraying pure wire. The short-<br />
est Tlz values occurred for the sample (b) considered to be the<br />
least pure of the three.<br />
7.5.2 DIPOLAR RELAXATION TIME (TID)<br />
The dipolar relaxation times of samples (a), (b) and (c)<br />
were measured with the Jeener and Brockaert pulse sequence (see<br />
Section 5.8) in identical conditions to those existing for the TlZ<br />
measurements. The results are included in Table 7.2 together with